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VAAL UNIVERSITY OF TECHNOLOGY FACULTY OF APPLIED AND COMPUTER SCIENCES DEPARTMENT OF CHEMISTRY LOGBOOK: WORK INTEGRATED LEARNING & UNIVERSITY TRAINING ANALYTICAL CHEMISTRY FOREWORD 1. TO THE EMPLOYER Thank you for your indispensable share as training partner in this important area of cooperate educations. You are undoubtedly aware of the fact that a student must have completed six months of applicable work integrated learning plus the two and a half years prescribed university training before the National Diploma: Analytical Chemistry (3215035) is awarded to him/her. To ensure the effectiveness of the work integrated learning period the employer and must cooperate as equal partners. Against this background the friendly request that employers should ensure that the logbook is kept up to date and is periodically submitted to the applicable school of the applicable Department of the University for evaluation. 2. TO THE STUDENT To qualify for the National Diploma: Analytical Chemistry (3215035) a six month period of suitable work integrated learning as well as the prescribed University training must be successfully be completed. To assist the University in assessing the progress of your work integrated learning, you have to report on a continuing basis to the Head of Department: Chemistry The attached logbook makes it easy to keep a permanent record of all your activities during your work integrated learning period. Your tutor/mentor must certify that you satisfactorily performed the work reported. In the event of a change of employer during this period, have your logbook brought up to date before leaving. The logbook will inform your new employer about you training programs and activities. For the period of work integrated learning you must also complete the required registration form at the Department of the University concerned. On completion of your work integrated learning program, this logbook and other documents which may be required must be submitted with your application for the issuing of your National Diploma. DR E.B. NAIDOO HEAD OF DEPARTMENT: CHEMISTRY TEL: (016) 950 9603 FAX: (016) 950 9794 2 RECORD OF TRAINING OF STUDENT SURNAME FIRST NAMES I. D. NR. DATE OF BIRTH SEX MALE TITLE MR FEMALE X X MRS MISS OTHER STUDENT NUMBER COURSE N. DIP: ANALYTICAL CHEMISTRY (3215035) PERIODS OF UNIVERSITY TRAINING S1 S2 S3 S4 S5 PERIODS OF WORK INTEGRATED LEARNING FROM TO FROM TO FULL-TIME PART-TIME EMPLOYER OFFICIAL STAMP OF EMPLOYER/COMPANY 3 GUIDELINES FOR WORK INTEGRATED LEARNING AIM OF WORK INTEGRATED LEARNING (WIL): WIL is an integral part of the training and, together with University Training, form a co-operative training unit. It is therefore the aim of WIL to compel the students in his/her work situation, to be actively engaged in the broadening of his/her knowledge and analytical skills. It is also important that the students be exposed to the industrial world and his/her occupational ethics. The outline for WIL has been drawn up in order that the prescribed requirements can, where possible, fit in with the working environment of each students and his employer. DURATION OF COURSE: Five semester University training and one semester applicable work integrated learning for a total minimum duration of three years. Students enroll for WIL by registering for one semester for the subject “Chemical Industry: Practical P1”. Students may register for “Chemical Industry: Practical P1” during any semester, even for the semester immediately preceding full-time study. WHERE IS WORK INTEGRATED LEARNING DONE? “Chemical Industry: Practical P1” must be completed by the student at an accredited employer. GUIDELINES FOR WORK INTEGRATED LEARNING: 1. REGISTRATION FOR WORK INTEGRATED LEARNING: It is the responsibility of the student to register at the University for work integrated learning. No students will be registered without proof of employment. Registration takes place at the same time as registration for full-time and part-time students during January and July each year or soon after the student is employed Registration takes place by the completion of an application to register that is available at the Head of Department: Chemistry. 2. REPORTS ON WORK INTEGRATED LEARNING: The student and his/her employer (training institution) organize his/her work integrated learning according to aspects referred to in this logbook. The employer may appoint a mentor for the student. At the end of the training period the student reports to his/her mentor. The mentor evaluates the report and, using the prescribed form in the logbook, reports to the University. 3. GENERAL University staff will attempt to visit the student during his/her work integrated learning period Employers are requested to make contact with the department if they experience any problems or if they want to make any changes to the training programme. 4 NATIONAL DIPLOMA: ANALYTICAL CHEMISTRY (3215035) 1. Admission Requirements Senior Certificate to its equivalent. (A pass in Mathematics and Physical Science is recommended). 2. Duration of course Full-time: Five semesters of class attendance at a University and one semester applicable in-service training. The minimum total of duration is three years and no award will be considered until the complete course (theory and work integrated learning) has been satisfactorily completed. Part-time: Over a minimum period of three to four years for persons who are employed in order that the required work integrated learning may be completed. 3. Curriculum Semester 1 Analytical Chemistry I (150413512) Chemistry I (150417112) Module 1: Theory Module 2: Practical Physics I (150710512) Mathematics I (160404012) Communication Skills I (129900612) AAACA 1B AACHC 1A AACHX 1A AACHY 1A APFSA 1C AMISS 1C HKKVA 1C Semester 2 Analytical Chemistry II (150416622) Analytical Chemistry: Practical II (150400622) Inorganic Chemistry II (150416822) Physical Chemistry II (150413722) Organic Chemistry II (150413822) AAACA 2 AAACP 2A AAICA 2C AAFCA 2B AAOCA 2B Semester 3 Inorganic Chemistry II (150414203) Physical Chemistry III (150414303) Organic Chemistry III (150414103) Computer Skills I (060205512) AAICA 3B AAFCA 3B AAOCA 3B AEREV 1B Semester 4 Analytical Chemistry III (150414503) Analytical Chemistry: Practical III (150414603) Chemical Quality Assurance (150416722) AAACA 3B AAACP 3B AACKV 2A 5 Semester 5 Chemical Process Industries II (080506822) Entrepreneurial Skills (040927512) Physics II (150710922) Industrial Chemical Analysis (150417522) Mathematics II (160404122) AACPA 2B BBENT 1A APFSA 2A AAIAC 2A AMISK 2C Semester 6 Chemical Industry: Practical P1 AACNP 1A Remarks: (1) (2) 4. Compulsory instructional offerings: All instructional offerings are compulsory Prerequisite instructional offerings: Chemistry I for Inorganic Chemistry II, Physical Chemistry II and Organic Chemistry II Syllabuses Semester 1 ANALYTICAL CHEMISTRY I AAACA 1B CONTENTS THEORY: 1. Introduction to analytical chemistry. 2. Laboratory practice and safety. 3. Calculations in analytical chemistry. 4. Elementary statistics, including significant figures, precision and accuracy. 5. Sampling and sample handling. 6. Introduction to classical analysis. 7. Technical report writing. 6 CHEMISTRY I AACHC 1A MODULE 1: CHEMSITRY: THEORY I AACHX 1A CONTENTS 1. 2. 3. 4. 5. 6. 7. 8. Matter and energy: Atomic structure Periodic table Chemical bonding Nomenclature of inorganic compounds Chemical equations and stoichiometry Solutions Acids, bases and slats Chemical equilibrium Electrochemistry and redox theory Introduction to inorganic chemistry Introduction to organic chemistry MODULE 2: CHEMISTRY: PRACTICAL I AACHY 1A CONTENTS 1. 2. 3. 4. 5. 6. Heating techniques Separation techniques Cation and anion analysis Gravimetric analysis Titrimetric analysis Redox titrations PHYSICS 1 APFSA 1C SECTION A: THEORY CONTENTS 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. Introduction to vectors Equilibrium of a particle Motion in a straight line Newton’s second law Motion in a plane Work and energy Impulse and momentum Equilibrium moment of a force Rotation Elasticity Fluid statics Fluid dynamics Temperature and expansion Quantity of heat 7 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. Heat transfer The first law of thermodynamics Gas law Electrostatics Ohm’s law Resistance and circuits The magnetic field The magnetic field of a current Induced electromotive force The nature and propagation of light Images formed by a single surface Lenses Refraction through prisms Illumination Interference and diffraction Photon’s, electrons and atoms Nuclear physics SECTION B: PRACTICAL 1. 2. 3. 4. 5. Electricity Nuclear physics Optics Mechanics Heat MATHEMATICS I AMISS 1C CONTENTS 1. 2. 3. 4. 5. 6. 7. Calculations Algebra The Binomium Trigonometry Graphs Differential calculus Integral calculus COMMUNICATION SKILLS HKKVA 1C Semester 2 ANALYTICAL CHEMISTRY 1. 2. 3. 4. 5. 6. AAACA 2C Gravimetric analysis Precipitation titrations Neutralization titrations Non-aqueous titrations Complexiometric titrations Redox titrations 8 7. 8. Analytical separations Refractometry and polarimetry ANALYTICAL CHEMSITRY: PRACTICAL II AAACP 2A CONTENTS Section A: Wet chemical analysis 1. Revision 2. Sampling 3. Gravimetry 4. Volumetry 5. Total analysis of complex materials Section B: Basic instrumental analysis 1. Chromatography 2. Potentiometry 3. Refractometry 4. Polarimetry INORGANIC CHEMISTRY II AAAICA 2C CONTENTS THEORY 1. 2. 3. 4. Introduction to chemical bonding and an advanced study of ionic bonding. Chemical reactions in an aqueous and non-aqueous solution Redox chemistry: Derivation of oxidation state diagrams Descriptive inorganic chemistry 4.1 Hydrogen 4.2 Group IA (Li, Na, K) 4.3 Group IIA (Mg, Ca) 4.4 Group IIIA (B, A1) 4.5 Group IVA (C, Si, Ge, Sn, Pb) 4.6 Group VA (N, P, As, Sb, Bi) 4.7 Group VIA (O, S) 4.8 Group VIIA (F, Cl, Br, I) PRACTICAL 1. 2. 3. 4. Group IV (C, Si) Group V (N) Group VI (O, S) Group VII (Halogens) 9 PHYSICAL CHEMISTRY II AAFCA 2B CONTENTS THEORY 1. 2. 3. 4. 5. 6. 7. Gases: ideal and non-ideal Liquids: surface tension, viscosity, additive properties Chemical kinetics Chemical equilibrium Colloids Colligative properties of solutions Electrochemsitry PRACTICAL Practical physical chemistry ORGANIC CHEMISTRY II AAOCA 2B CONTENTS THEORY 1. 2. 3. 4. 5. 6. 7. 8. 9. Introduction Aliphatic hydrocarbons Benzene Alkyl and aryl halides Alkanols and alkoxyalkanes Phenols Alkanals and alkanones Carboxylix acids and derivatives Amines PRACTICAL 1. 2. 3. 4. Quantitative analysis Qualitative analysis Separation and extraction Elementary techniques (distillation and recrystallisation) Semester 3 INORGANIC CHEMISTRY III AAICA 3B CONTENTS THEORY 1. Chemical bonding 10 1.1 1.2 1.3 Theories of covalent bonding Coordination chemistry Crystal field and Ligand field theories 2. Descriptive chemistry of the transition elements 2.1 Extraction and uses 2.2 The first transition series (Sc to Ni) 2.3 Group IB (Cu, Ag, Au) 2.4 Group IIB (Zn, Cd, Hg) 3. Nuclear chemistry PRACTICAL 1. 2. 3. 4. 5. Preparation and study of complexes Spectroscopic study of transition metal compounds Preparation of inorganic complexes Electroplating of metals Extraction of metals PHYSICAL CHEMISTRY III AAFCA 3B CONTENTS THEORY 1. 2. 3. 4. 5. 6. 7. Chemical thermodynamics: First, Second and Third Law Changing of phase: phase diagrams Electrochemistry: conductivity, transfer number, eletrolysis Reaction kinetics: orders, Arrhenius equations, compound mechanisms, catalyses Quantum chemistry: atomic spectra, emission and absorption spectra, rotational spectra, Raman, vibrational and electronic spectra The solid state: crystal lattices, planes, indices, X-ray diffraction, structure of crystals Surface chemistry: adsorption isotherms, surface reactions PRACTICAL 1. 2. 3. 4. 5. 6. 7. 8. Conductometry Coulometry and electrolysis Reaction kinetics Simple thermodynamic determinations Surface chemistry Elementary crystallography Quantum chemistry Physical properties of gasses and liquids 11 ORGANIC CHEMISTRY III AAOCA 3B CONTENTS THEORY 1. 2. Introduction Stereochemistry and conformational analyses 3. 4. 5. 6. 7. 8. 9. 10. Strength of acids and bases Nucleophilic reactions and unsaturated carbons Nucleophilic substitution at saturated carbons Elimination reactions Aromatic chemistry Natural and synthetic polymers Carbohydrates and related biological compounds Determination of organic structures PRACTICAL 1. 2. 3. Preparation, isolation and purification of organic compounds Library/laboratory project Qualitative instrumental analyses of organic compounds COMPUTER SKILLS 1 AEREV 1B Semester 4 ANALYTICAL CHEMISTRY III AAACA 3B CONTENTS 1. 2. 3. 4. 5. Data handling Introduction to absorption and emission spectroscopy Molecular spectroscopy 3.1 Ultraviolet and visible: Instrumentation 3.2 Ultraviolet and visible: Methods 3.3 Infrared Atomic spectroscopy 4.1 Flame emission and atomic absorption spectrometry 4.2 Atomic emission spectroscopy 4.3 X-ray methods Chromatographic methods 5.1 General principles 5.2 Quantitative analyses 5.3 Gas chromatography 5.4 Liquid chromatography 12 6. 7. Electrometric methods of analysis 6.1 Potentiometry 6.2 Polarography 6.3 Electrogavimetry and coulometry Thermal analysis ANALYTICAL CHEMISTRY: PRACTICAL III AACAP 3B CONTENTS 1. 2. 3. 4. 5. 6. Flame atomic spectrometry 1.1 Flame photometry 1.2 Atomic absorption spectrometry Molecular spectroscopy 2.1 Colorimetry 2.2 UV visible spectrometry 2.3 Infrared spectroscopy Chromatography 3.1 Gas chromatography 3.2 Liquid chromatography Electro-analytical methods 4.1 Potentiometry 4.2 Polarography 4.3 Electrogravimetry and coulometry Atomic emission spectrometry and X-ray methods 5.1 X-ray method 5.2 Atomic emission spectrometry Thermal analysis CHEMICAL QUALITY ASSURANCE AACKV 2A CONTENTS 1. 2. 3. 4. 5. Advanced statistical treatment of data in Analytical Chemistry Optimization and calibration of analytical instruments Quality assurance systems Laboratory accreditation Research methods and techniques Semester 5 CHEMICAL PROCESS INDUSTRIES II ACCPA 2B CONTENTS Note: Compulsory subjects are points 1, 2, 8 and 9, choice of any three other subjects from lsit. A minimum of 7 subjects must be covered. 1. Coal processing Compulsory 13 2. Petroleum refining 3. Synthetic rubber 4. Plastics 5. Paper and pulp 6. Sugar refining 7. 8. Agrochemicals Iron and steel Compulsory 9. Heavy chemicals Compulsory ENTREPRENEURIAL SKILLS Compulsory BBENT 1A CONTENTS 1. 2. 3. 4. 5. Evaluating opportunity and developing the business concept Assessing and acquiring necessary resources Acquiring and existing business Managing the enterprise and harvesting value Project PHYSICS II APFSA 2A CONTENTS SECTION A: ATOMIC PHYSICS (OR QUANTUM PHYSICS) 1. Interaction of radiation with matter - Electromagnetic spectrum - Electromagnetic radiation of waves (General nature, diffraction, scattering, polarization, reflection, interference, etc) 2. Quantum mechanical properties of radiation - Wave particle duality Photo electric effect Absorption, emission, etc Quantum theory (Rydberg, etc) Selection Rules Stark, Zeeman and Doppler effect SECTION B: OPTICS 1. Lasers 2. Diffraction gratings and spectrometers 14 3. Detectors for spectroscopy – basic principles (Photo-tubes, silicon diodes, vidicons, CCD, CTD, CID, heat detectors) 4. Fibre optics 5. Multiple designs (Fourier Transform, etc) SECTION C: ELECTRONICS 1. Solid state physics (diodes, semi-conductors, transistors, microchip technology) 2. Basic electronics (operational amplifiers and their uses, integration, etc) 3. Digital electronics (analog/digital signals, binary numbers, microprocessors, basic digital circuit components) 4. Signal and noise (S/N ration, sources of noise, S/N enhancement) SECTION D: MAGNETIC FORCES AND FIELDS - Motion of charged particle in magnetic field Mass spectrometer Magnetic flux Magnetic flux density (KMR) SECTION E: FLOW DYNAMICS - Viscosity Bernoulli’s principle Laminar and turbulent flow SECTION F: NUCLEAR PHYSICS - Basic principles of radioactivity Detectors Applications INDUSTRIAL CHEMICAL ANALYSIS AAIAC 2A CONTENTS 1. Chemical analysis in complex matrices: an introduction. The analytical approach 2. Drug analysis in biological fluids. Introduction – analytical methods in drug analysis Sample preparation – solid phase extraction Practical considerations in biopharmaceutical analysis 15 3. Analysis in the brewing industry. Introduction – the brewing process Instrumental methods – criteria Applications for spectrometric methods Applications for chromatographic methods Servo chem. Automatic beer analyzer Flow injection analysis 4. Analytical lab in the speciality sealants/adhesives industry. Introduction – composition and chemical behaviour of sealants/adhesives Case histories involving problem solving Useful analytical techniques 5. Air pollution analysis Introduction – air pollution system Gas concentration Gas sampling techniques Gas collection devices Choice of analytical methods 6. Chemical analysis of animal feed and human food Introduction – sampling and sample pretreatment Compositional analysis, nutritional analysis, residence analysis Agrochemicals and food safety 7. Water analysis 8. Metallurgical analysis 9. Polymer analysis 10. Sugar analysis 11. Flow injection and automated analysis MATHEMATICS II AMISK 2C CONTENTS 1. Differentiation 2. Integration 3. First order differential equations 4. Matrix algebra 16 Semester 6 CHEMICAL INDUSTRY: PRACTICAL P1 AACNP 1A SYLLABUS: (Proposed study scheme) Semester 1: University training Analytical Chemistry I AAACA 1B Chemistry I AACHC 1A Physics I APFSA 1C Mathematics I AMISS 1C Communication Skills 1 HKKVA 1C Semester 2: University training Analytical Chemistry III AAACA 2C Analytical Chemistry: Practical II AAACP 2A Inorganic Chemistry II AAICA 2C Physical Chemistry AAFCA 2B Organic Chemistry AAOCA 2B Semester 3: University training Inorganic Chemistry III AAICA 3B Physical Chemistry III AAFCA 3B Organic Chemistry III AAOCA 3B Computer Skills I AEREV 1B Semester 4: Work integrated learning Aspects in which students should receive training SECTION A: GENERAL LABORATORY PRACTICE Both modules are compulsory. 1. General laboratory techniques 1.1 Correct sampling techniques 1.2 Sample preparation 1.3 Preparation of standards 1.4 Safety in the laboratory 2. Laboratory organisation and management 2.1 General laboratory organisation and management 2.2 Preparation of laboratory reports 2.3 Data handling 2.4 Mathematical treatment of results 2.5 Quality assurance 2.6 Laboratory budget 2.7 Handling of chemical literature 2.8 Meeting procedures SECTION B: WET CHEMICAL ANALYSIS Both modules are compulsory. 1. Gravimetric analysis 2. Titrimetric analysis 17 SECTION C: INSTRUMENTAL ANALYSIS Any ONE of the following. 1. Spectroscopic techniques 2. Chromatography 3. Electroanalytical techniques 4. Thermal analysis SECTION D: GENERAL CHEMISTRY Any ONE of the following. 1. Physical test (viscosity, density, etc.) 2. Physical chemistry (surface studies, kinetics, etc.) 3. Organic chemistry (synthesis of compounds) 4. Inorganic Chemistry (synthesis of compounds) 5. Process chemistry and chemical plant 6. Water chemistry Semester 5: University training Analytical Chemistry III AAACA 3B Analytical Chemistry: Practical III AAACP 3B Chemical Quality Assurance AACKV 2A Physics II APFSA 2A Semester 6: University training Chemical Process Industries II ACCPA 2B Entrepreneurial Skills BBEMT 1A Industrial Chemical Analysis AAIAC 2A Mathematics II AMISK 2C 18 RECORD OF UNIVERSITY TRAINING 19 RECORD OF UNIVERSITY TRAINING (S1) VAAL UNIVERSITY OF TECHNOLOGY PERIOD OF ATTENDANCE: ……………………………………………………………………. SUBJECTS Exam Number Exam % Exam. Results …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. Subjects Rewritten Exam Number Exam % Exam. Results ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. Analytical Chemistry I Chemistry: Theory I AAACA 1B AACHX 1A Chemistry: Practical I Physics I AACHY 1A APFSA 1C Mathematics I AMISS 1C Communication Skills HKCOM 1A % Class Attendance PASSED / FAILED REMARKS: ……………………………………………………………………………………… …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. SIGNED: ………………………………………… UNIVERSITY OFFICIAL 20 RECORD OF UNIVERSITY TRAINING (S2) VAAL UNIVERSITY OF TECHNOLOGY PERIOD OF ATTENDANCE: ……………………………………………………………………. SUBJECTS Exam Number Exam % Exam. Results …………. …………. …………. …………. Analytical Chemistry: Practical II AAACP 2A …………. …………. …………. …………. AAICA 2C …………. …………. …………. …………. Physical Chemistry II AAFCA 2B …………. …………. …………. …………. Organic Chemistry II AAOCA 2B …………. …………. …………. …………. …………. …………. …………. …………. Subjects Rewritten Exam Number Exam % Exam. Results ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. Analytical Chemistry II Inorganic Chemistry II AAACA 2C ……………………………………………. % Class Attendance PASSED / FAILED REMARKS: ……………………………………………………………………………………… …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. SIGNED: ………………………………………… UNIVERSITY OFFICIAL 21 RECORD OF UNIVERSITY TRAINING (S3) VAAL UNIVERSITY OF TECHNOLOGY PERIOD OF ATTENDANCE: ……………………………………………………………………. SUBJECTS Exam Number Exam % Exam. Results AAICA 3B …………. …………. …………. …………. Physical Chemistry III AAFCA 3B …………. …………. …………. …………. Organic Chemistry III AAOCA 3B …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. …………. Subjects Rewritten Exam Number Exam % Exam. Results ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. Inorganic Chemistry III Computer Skills I AEREV 1B ……………………………………………. % Class Attendance PASSED / FAILED REMARKS: ……………………………………………………………………………………… …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. SIGNED: ………………………………………… UNIVERSITY OFFICIAL 22 RECORD OF UNIVERSITY TRAINING (S4) VAAL UNIVERSITY OF TECHNOLOGY PERIOD OF ATTENDANCE: ……………………………………………………………………. SUBJECTS Exam Number Exam % Exam. Results …………. …………. …………. …………. Analytical Chemistry: Practical AAACP 13B …………. …………. …………. …………. Chemical Quality Assurance AACKV 2A …………. …………. …………. …………. Physics II …………. …………. …………. …………. Subjects Rewritten Exam Number Exam % Exam. Results ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. Analytical Chemistry III AAACA 3B APFSA 2A % Class Attendance PASSED / FAILED REMARKS: ……………………………………………………………………………………… …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. SIGNED: ………………………………………… UNIVERSITY OFFICIAL 23 RECORD OF UNIVERSITY TRAINING (S5) VAAL UNIVERSITY OF TECHNOLOGY PERIOD OF ATTENDANCE: ……………………………………………………………………. SUBJECTS Exam Number Exam % Exam. Results Chemical Process Industries II ACCPA 2B …………. …………. …………. …………. Entrepreneurial Skills …………. …………. …………. …………. Industrial Chemical Analysis AAIAC 2A …………. …………. …………. …………. Mathematics II …………. …………. …………. …………. Subjects Rewritten Exam Number Exam % Exam. Results ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. BBENT 1A AMISK 2C % Class Attendance PASSED / FAILED REMARKS: ……………………………………………………………………………………… …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. SIGNED: ………………………………………… UNIVERSITY OFFICIAL 24 RECORD OF UNIVERSITY TRAINING (S6) FIRM: ………..……………………………………………………………………………………. PERIOD OF ATTENDANCE: ……………………………………………………………………. SUBJECTS Exam Number Exam % Exam. Results …………. …………. …………. Subjects Rewritten Exam Number Exam % Exam. Results ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. ……………………………………….…… …………. …………. …………. Chemical Industry: Practical P1 AACNP 1A % Class Attendance …………. PASSED / FAILED REMARKS: ……………………………………………………………………………………… …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. …………………………………………………………………………………………………….. SIGNED: ………………………………………… UNIVERSITY OFFICIAL 25 REPORT OF WORK INTEGRATED LEARNING 26 WORK INTEGRATED LEARNING Only a brief summary is here required. Nature of Activity Time period in (Condensed description) performed, e.g. 1.1.2003 – 30.6.2003 ORIENTATION Supervisory Official 1.1 Information programme …………………….. …………………….. 1.2 Brief survey on the origin and growth of firm …………………….. …………………….. 1. SAMPLING TECHNIQUES ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. ……………………. 2. SAMPLE PREPARATION 3. PREPARATIONS OF STANDARDS 4. SAFETY IN THE LABORATORY 5. GENERAL LABORATORY ORGANISATION AND MANAGEMENT 27 Nature of Activity (Condensed description) Time period in performed, e.g. 1.1.2003 – 30.6.2003 Supervisory Official ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. ……………………. 6. PREPARING OF LABORATORY REPORTS ……………………………………………. ……………………………………………. ……………………………………………. 7. DATA HANDLING 8. MATHEMATICAL TREATMENT OF RESULTS 9. QUALITY ASSURANCE 10. LABORATORY BUDGET 11. HANDLING OF CHEMICAL LITERATURE 28 Nature of Activity (Condensed description) Time period in performed, e.g. 1.1.2003 – 30.6.2003 Supervisory Official ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. 12. MEETING PROCEDURES 13. WET CHEMICAL ANALYSIS GRAVIMETRIC ANALYSIS TITRIMETRIC ANALYSIS 14. INSTRUMENTAL ANALYSIS SPECTROSCOPIC TECHNIQUES 29 Nature of Activity (Condensed description) Time period in performed, e.g. 1.1.2003 – 30.6.2003 Supervisory Official ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. Viscosity …………………….. …………………….. Density …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. CHROMATOGRAPHY ELECTRO-ANALYTICAL TECHNIQUES THERMOMETRIC ANALYSIS 15. GENERAL CHEMISTRY PHYSICAL TESTS PHYSICAL CHEMISTRY 30 Nature of Activity (Condensed description) Time period in performed, e.g. 1.1.2003 – 30.6.2003 Supervisory Official ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. ……………………………………………. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. …………………….. .................................. …………………….. ORGANIC CHEMISTRY INORGANIC CHEMISTRY PROCESS CHEMISTRY AND CHEMICAL PLANT WATER CHEMISTRY ……………………………………………. ……………………………………………. ……………………………………………. ……………………………………………. ……………………………………………. ……………………………………………. ……………………………………………. 31 EVALUATION REPORT Excel-lent 1. Dexterity 2. Knowledge of techniques, Good Acceptable Insufficient Weak procedures and materials 3. Safety awareness 4. Willingness to learn new skills 5. Initiative 6. Human relations 7. Attitude 8. Efficiency as employee/ Standard of work 9. Neatness 10. Proficiency ……………………………………….. SIGNATURE ……………………… DATE RANK/DESIGNATION: ………………………………………………………………………… OFFICIAL STAMP OF EMPLOYER/COMPANY 32 DECLARATION BY EMPLOYER I, ……………………………………………………………………………………………………. associated with …………………………………………………………………………………….. in the capacity of …………………………………………………………………………………... hereby certifies that (name of student) ……………………………………………………………. Was a permanent employee of the company/concern for the past semester and performed the practical training as required by the University. I further certify that the work performed by the above mentioned person, was to the benefit of the company/concern. Finally I declare that the accompanying report, carrying my signature, is the student’s own as well as the work set out therein. ……………………………………….. SIGNATURE ……………… DATE 33 RECOMMENDATION BY EMPLOYER RE WORK INTEGRATED LEARNING Candidate ………………………………………………………………………………………… successfully/unsuccessfully completed his/her work integrated learning. Mark allocated for Chemical Industry: Practical P1 AACNP 1A: …………… % ………………………………………. TRAINING OFFICIAL OFFICIAL STAMP OF EMPLOYER …………………………….. DATE 34 RECOMMENDATION BY UNIVERSITY RE ISSUING OF DIPLOMA Candidate ………………………………………………………………………………………… successfully completed his/her Chemical Industry: Practical P1. It is recommended that the National Diploma: Analytical Chemistry is issued to him/her with effect from ………………………………………… 20…… …………………………………………….. HEAD OF DEPARTMENT: CHEMISTRY …………………………….. DATE 35