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1 ACOUSTO-OPTICAL CHARACTERIZATION OF A CONTACT BETWEEN A TIP AND A PLATE J.P. Nikolovski CEA LIST : Laboratoire des Interfaces Sensorielles 18, route du Panorama, 92265 Fontenay aux Roses, France. Email : [email protected] tip Abstract The local strain perturbation induced by the contact between a tip and a plate is investigated with an optical heterodyne interferometer as symmetric S0 and antisymmetric A0 Lamb waves are propagated in the bulk of the plate. Elasto-optic disturbance analysis is carried out for each mode and comparison between both modes is made to best characterize the contact. Two and three wave optical interference analysis is used to explain the presence of fringes of equal thickness disturbances. The S0 Lamb mode turns out to magnify optical effects of the mechanical contact. 1. Introduction Ultrasonic testing of solid materials may require probing very small areas of a material. This can be done by coupling flat ultrasonic shear wave transducers to conical tips1. In many cases implying simultaneous detection of shear and longitudinal components, it can be very difficult to detect selectively one component from the other particularly when sub-wavelength contacts interactions are concerned. At the same time, the nature of the contact between the probed material and the tip should be characterized. The purpose of this work is to use the selectivity of an optical interferometer which has local access to the normal displacement of the matter to describe both experimentally and analytically the optical effects of a sub-wavelength mechanical contact between a free surface and a tip. sz z Cr-Au glass plate sz x AIR +sz -sz optical probe beam A0 Lamb mode S0 Lamb mode Figure 1 - Local perturbation caused by the tip in contact with a sample. The sample is here a glass plate which propagates S0 and A0 Lamb modes. Fig. 2 shows in schematics the optical probe. A He-Ne laser beam is modulated by an acousto-optic modulator of frequency f0. The laser beam has a circular polarization as it goes through the plate. The reflected beam is modulated at the frequency f of the Lamb waves. It is then received by a photodiode and demodulated. Dove's prism fL PZT /4 LASER beam fL + f 0 AOM f0 S 0,A fL fL + f 0 mod f R S The tip is a conically or parabolically tapered rod made with Duralumin. The length of the tip, typically 100 mm long, is large compared to the wavelength. Local perturbation induced by the tip can be visualized with an optical heterodyne interferometer2 trough a transparent sample as shown in fig.1. In the following case the sample is a glass plate of thickness 1 mm coated on one face with a Cr-Au layer. The plate propagates the symmetrical Lamb mode S0 and the antisymmetrical Lamb mode A0. Going through the plate to see the local disturbance caused by the tip is not a very convenient way to proceed because in that case, the optical path of the probe beam is modified both by surface displacement of the Cr-Au layer and by the variation of the refraction index n of the glass plate as Lamb waves goes by. We nevertheless proceedeed that way because a first C-scan made on the side opposite to the side of the contact area revealed no signal variations. f ANALYSER f0 mod f PHOTODIODE t Low pass s (t) filter Filter 2. Local perturbation induced by the tip Tip (f 0) 90° f0 90° Figure 2 -The optical heterodyne interferometer: a laser beam is modulated by an acousto optic modulator (AOM) of frequency f0. The optical path of the modulated beam is modified by the propagation of the Lamb modes at the frequency f. The light beam passing through the plate has a circular polarization. Fig. 3 represents a C-scan over a surface of 70 µm x 70 µm around the contact area in the configuration of fig. 1 for the S0 Lamb mode. A 2 cm focal length was used giving a spot of approximately 7 µm of diameter. The pictures shows regions where the signal is much smaller in amplitude, by 30 dB, than the signal of undisturbed regions as well as regions where the signal is stronger than the signal of undisturbed regions 2 Figure 3 - C-Scan on S0 over a surface of 70 µm x 70 µm. Multiple contacts can be seen. Phase inversions min 2 air 2s z0 2nc ec with n c n0 n e 2 1 n ndz e e 2 e c e0 2s z0 max 2 air 2s z0 n d ed n d n0 n 0 e d e0 2s z The circular polarization has an x and y component. The variation of the refraction index due to the travelling wave are along theses axes: n3 n x p11S xx p12 S zz and n x n0 n x 2 n3 n y p21 S xx S zz and n y n0 n y 2 where p11 and p12 are components of the elasto-optic tensor, and Sxx and Szz are components of the strain tensor. The displacement components of the S0 Lamb mode at 1 MHz are approximately 3: Figure 4 - B-scan on the line y = 25 µm of fig.20. Signal phase inversions are clearly visible. Regions of strong signals are very close to regions of weak signals. It can also be noticed that around these regions phase inversion of the signal occurs as it is showed more clearly on a B-scan at the position y = 25 µm of fig. 4. These effects are obviously due to the presence of the tip and reveal multiple contacts. The following theoretical analysis will help understand why inversion of the signal occurs in regions of strong interactions. 2 0 x( mm) sx ( t , x , z ) 5sz cos t 0 2s 2 sz ( t , x , z ) z z sin t x( mm) e nx and ny components are independent from the z component. Therefore the average variation of the refraction index in the thickness of the plate is equal to the local variation at a particular position in the thickness. e 2 3. Two wave interferences In the experimental configuration of fig. 1 and 2, we assume that there is only one reflected beam from the CrAu layer. Let us calculate the minimum and maximum optical path length. We call air the optical path length in air 0 when the plate is at rest; s z is the z component amplitude of the S0 Lamb wave mechanical displacement at the surface of the plate, nc and nd are the average refraction indexes of the glass plate when its thickness (e) is respectively minimum (ec), and maximum (ed), whereas n0 is the refraction index of the plate at rest. e 2 1 1 n i n i dz n i dz ni e e e e 2 2 0 Numerical estimations: at 1 MHz and for s z =15 Å we have: S xx (x, t ) 5ks z0 sin(t kx ) 108 . 10 -6 sin(t kx ) S zz (x, t ) 2s z0 sin(t kx ) 81 . 10 -6 sin(t kx ) e n 15 . p11 0121 . p12 0.270 n x ( x , t ) n03 p11S xx p12 S zz 0.45 10 6 sin(t kx ) 2 n y ( x , t ) n03 p21S xx p12 S zz 2.68 10 6 sin(t kx ) 2 We have now to calculate the electrical field, reflected back from the Cr-Au layer: The x and y components of the field are: 2 0 E S x E0 cos 0 t s ( 2 4n0 ) 2e0n x sin(t kx ) S 0 z 2 0 y E0 sin 0 t s z ( 2 4n0 ) 2e0n y sin(t kx ) S 0 3 reference beam. At the output of the photodiode, the alternative part of the photocurrent is proportional to the following expression: ny Emsint nz Emcost circular polarization nx Figure 5 - Projection of the circular polarization vector entering the glass plate on the x and y unity vectors The beam has then to go back again through the /4 plate that has its eigen vectors at 45° from the x and y axis. At the exit, the electrical field is approximately linear and can be approximated by the expression: 0 t nx n y ES 2x E0 sin 2 0 sz (2 4n0 ) 2e0 2 0 1 cos 0 t k 2s z0 sin(t kx ) S1 R 0 0 n n x y 0 2 i( t ) 2 E0 1 2 cos 0 t k s z 4n0 2e0 sin(t ) 2kn0 e S 2 S 2 2 0 n x 0 n y cos t k s 0 ( 2 4n ) 2e sin( t ) 2 kn e 0 0 0 S2 R z 0 2 2 Cr-Au S0 Lamb mode sin(t kx ) S 4 S1 S2 We see that the total phase fluctuations of the laser beam due to variations of the refraction index along x and y is the average of the x and y refraction indexes variations. Figure 6 - Three wave interferences can be obtained experimentally by changing the position of the glass plate according to the focusing lens. If the total phase fluctuations are much smaller than 2, the signal spectrum is composed of a central carrier frequency f0, and lateral frequency rays, the amplitude of which are given by Bessel functions. The alternative part of the photocurrent can be developed as follows: n x0 n 0y ( x, t ) sz0 ( 2 4n0 ) 2e0 2 sin(t kx ) Numerical application: If we take: n0 = 1.5 s z0 = 15 Å n x ( x , t ) n y ( x , t ) 1.57 10 6 sin ( t kx ) 2 e0 = 1 mm (x, t) = (-6. 10 -9 - 3.1 10 -9 )sin ( t - kx + ) = -3.1* 2 s z sin ( t - kx + ) As a first conclusion, when the laser beam goes through the plate the signal is 3.1 times larger and opposite in sign to the signal that would be obtained if the laser beam was simply reflected at the surface of the plate. The expression of the optical signal path shows also that by strongly blocking the back surface of the plate with the tip, it is possible to diminish or even change the sign of the optical length path. This explains the phase inversions of the signal in the regions of strong interactions. 4. Three wave interferences We consider now the case where, the laser beam is partially reflected at the front and back faces of the plate. This corresponds to a case of interferences with three beams. Fig. 6 illustrates the experimental situation. After front and back reflections as well as going through the /4 plate, the electrical fields attached to the optical beams are: ES1 1E0 exp i 0t k 2sz0 sin(t ) S1 0t 0 sz ( 2 4n0 ) ES 2 2 E0 exp i 0 nx 0 n y k 2e0 2 E R E0 exp i R sin(t ) 2kn0e S 2 where 1 and 2 are constants characterizing the intensity of the reflected beam compared to the intensity of the 1 cos 0t S R 1 2 cos 0t S S 2kn0e 2 2 2 i( t ) 2 cos 0t S 2 R 2kn0e 0 s k cos t 0 S2 R 1z 0 0 nx n y 0 1 2 k sz 2n0 e0 cos 0 t S 2 S 2 2kn0e 2 0 0 nx n y k s0 (1 2n ) e cos t 2 kn e 2 z 0 0 0 S R 0 2 2 0 1sz k cos 0 t S 2 R 0 0 nx n y 0 1 2 k sz 2n0 e0 cos 0 t S 2 S 2 2kn0e 2 0 0 nx n y k s0 (1 2n ) e cos 0 t S 2 R 2kn0e 0 0 2 z 2 The sum of the three terms at frequency f0 has an amplitude A and a phase given by the following expression: 1 cos 0t S R 1 2 cos 0t S S 2kn0e 2 2 2 A cos( 0t ) 2 cos 0t S 2 R 2kn0e with 1 cos R S 2kn0e cos S S 2kn0e 2 2 1 A2 12 12 22 22 21 2 cos 2 S 2 4kn0e S1 R 2 2 sin R S 2kn0e tan 1 cos R S 12 cos2kn0e S 2 cos R S 2kn0e 1 sin R S2 12 sin 2kn0e S2 S2 2 2 2 S2 2 We do the same treatment for the three terms at lateral frequency f0 + f: 4 0 1sz k cos 0 t S 2 R 0 0 nx n y 0 1 2 k sz 2n0 e0 cos 0 t S 2 S 2 2kn0e 2 0 0 nx n y k s0 (1 2n ) e cos t 2 kn e 0 0 0 S2 R 0 2 z 2 A cos( 0t ) with tan 2 the fringe is moved up fringes of equal thickness A2 12 s2 k 2 12 22 k 2 2ns en 22 k 2 2ns en s 1s2ns en cos R S 2 2kne 21 2 k 2 s s1 2n en cos S 2 S1 2kne 2 s2ns en 2ns en2 cos 2 S 4kn0e S R 2 1 2 This leads to the same periodicity between minima. Fig. 8 presents two C-scans with a glass plate having a 1.1 mrd wedge. The perturbation caused by the tip is clear. Fringes are moved toward the crest. 2n i optical probe beam Figure 7 - Three wave interferences; fringes of equal thickness; glass plate with a 1.1 mrd wedge. 1sk sin R S 2 1 2 k 2ns en sin 2kn0e S 2 S 2 1sk cos R S 2 1 2 k 2ns en cos 2kn0e S 2 S 2 2 k s1 2n en sin R S 2 2kn0e 2 k s1 2n en cos R S 2 2kn0e From the ratio of the central and lateral frequency amplitudes discloses some information on the acoustic signal. r2 A2 A2 1 cos R S 2 kn0 e cos S S 2 kn0 e 2 2 1 12 22 12 22 21 2 2 cos 2 S 2 4kn0 e S1 R 12 s 2 k 2 22 k 2 2ns en s 2 12 22 k 2 2ns en 2 1s2ns en cos R S 2 2kne 21 2 k 2 s s1 2 n en cos S 2 S1 2 kne 2 s2ns en 2ns en 2 cos 2 S 4kn0 e S R 2 1 Numerical application: let us take 1 = 2 = 0.1, and s = 15 Å: 2. 01 0. 2 cos R S2 2 kne 2 cos S2 S1 2 kne k 2r 2 k 2 A2 A2 0. 2 cos 2 S2 4 kne S1 R 2286 180 cos R S2 2 kne 1350 cos S2 S1 2 kne 540 cos 2 S2 4 kn0 e S1 R The signal at the output of the interferometer is inversely proportional to this ratio: The signal is strong when the following condition is verified: cos S2 S1 2 kne 1 which leads to : 2kne 2 i.e. e = 2n Consequently, every time the thickness of the plate is increased by a value of /2n, the signal increases in amplitude. If the faces of the glass plate are not really parallel but have a wedge angle =1.1 mrd as illustrated with fig.7, fringes of equal thickness appear with the following periodicity between two maxima: 0. 632 m i 185 m 2 n 2 1.1 mrd 1.5 On the other way, the signal becomes very small when the following condition is satisfied. cos S2 S1 2 kne 1 Figure 8 - C-scan on the S0 Lamb mode. Disturbance caused by the tip to the fringes of equal thickness. The lower picture of fig. 8 shows that the parabolic tip has little effect on the position of two neighbouring fringes. This gives an idea of the disturbed area: a region of approximately 100 µm around the contact area. The interesting point is to see how far (about 80 µm) a fringe can be displaced by the presence of the tip. As a matter of fact, we know that the free surface vertical displacement is approximately 15Å (i.e. 0.7% of /2n); without any effect on the refraction indexes, the lateral displacement of the fringe should be of the order of 0.7% of the fringe period i.e. close to 1.3 µm instead of 80 µm. We see here how 5 refraction index variations mechanical disturbances. help investigate small 8. Conclusion The strain disturbance caused by a metallic tip in contact with a glass plate can experimentally be seen with an optical interferometric probe by propagating a S0 Lamb wave in the region of the contact. The refraction index variations reveals the regions stressed by the tip. Acknowledgments Author is thankful to D. Royer and D. Fournier (ESCPI, Paris) for helpful discussions. 1 Nikolovski J.P., Royer D., « Local and selective detection of acoustic waves at the surface of a material ». IEEE ultrasonics symposium proceedings. (1997) 699-703. 2 Royer D., Dieulesaint, E.,"Mesures optiques de déplacements d'amplitude 10-4 à 10-2 Angström. Application aux ondes élastiques". Revue Phys. Appl. 24 (1989) 833-846. 3 Nikolovski J.P. "Détecteur à ondes de Lamb de la Position d'un stylet", thèse de doctorat, Université Paris VI, 2 Feb. 1995.