Download Industrial Extraction

Associate professor, PhD, Ostvald Roman
Tomsk Polytechnic University, Institute of Physics and Technology
Chair of Rare, Scattered and Radioactive Elements Applied Chemistry
Tomsk 2011
Write a Russian equivalent for the
next phrases
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driving force,
flow rate,
surface of contact,
heat transfer
3
Draw up a table for the material
balance of a rectification column
in that process of separation
hydrofluoric acid and water is
produced.
Starting composition is given as
HF – 25 mole; H2O – 35 mole.
Requirements to quality of
product (final composition):
content of HF in water – 1 mole,
and purity of hydrofluoric acid
are the theoretical absolute.
4
What is a driving force for the
mass transfer process?
5
Draw up a table for the heat balance of a device to produce
sulfuric acid from oleum and water. Considerations must be
given to the quantity of heat which is forming at production
acid and equal 3.25 k.J per day. Looses for a heating in
surroundings are equal 0.40 k.J per day. The heat to warm
up the constructive materials of the device is 1.15 k.J per day
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What is a driving force for the heat
transfer process?
7
Draw up a table for the heat balance of the
desublimator in which process of recovery of
hexafluoride of uranium is produced, if the
condensation heat of UF6 is equal 2.5 k.J/day,
looses for heating in
surroundings are equal
0.3 k.J/day, heat to warm up
the constructive materials
of desublimator is 1 k.J/ day
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Write a Russian equivalent for the
next phrases
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mass transfer,
material balance,
flow rate,
surface of contact
9
Draw up a table for material
balance of the sorption column
in which process of separation
of threefluoride of bromine and
pentafluoride of iodine is
produced.
Starting composition:
IF5 – 0.65 mole; BrF3 – 0.74 mole.
Requirements to quality of
product: content of BrF3 in IF5 –
0.1 mole, and contamination of
BrF3 by IF5 can be 0.14 mole.
10
Write Russian equivalent for the
next phrases
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flux equations,
transverse velocity,
multidimensional,
creeping flow
11
Draw up a table for the material balance
of the extraction column in which process
of separation substances of uranium and
thorium is produced. Starting flow rate
(recalculated on UO22+ and ThO22+):
UO2(NO3)2 – 2.15 k.mole/day; ThO2(NO3)2
– 1.22 k.mole/day. Flow rate of ThO2… in
stream i is 1.15 k.mole/day, flow rate of
UO2… in stream j is 2.0 k.mole/day
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What is the term
“extraction” mean?
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Try to fined some examples of the
extraction using process in chemical
technology.
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What kind of extraction do you know?
14
Read the text about laboratory extraction
and try to explain words in bold
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separatory
funnel
figure
out
liquids will form two layers
when mixed together
vinegar
plug, bung
immiscible
liquid
stopper
stopcocks
ground
glass
lodge
crane, flow block
mechanism
acetum
special kind of compression
for laboratory installations
some equipment for extraction
carrying out in laboratory
calculate,
recognize
get stuck
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snugly
disadvantage
stem
stalk, tip of smth
trouble
ringstand
cushion
back shelves
elastic tubing
vigorously
shaking
tightly
flexible pipe
intensive, active shook of smth
resilient laying, softener
clamp,
claw
holder, rack, stand, tripod
17
Look the video about lab extraction and
discuss the extraction process
18
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What does it mean the
liquid-liquid extraction?
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What equipment uses to realize liquid-liquid
extraction?
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What does it mean the immiscible liquids?
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What factors influence on location of
immiscible layers, what liquid locate in upper
part of funnel and what in lower part of
funnel?
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What types of design
separatory funnels are uses in modern
chemical labs?
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How to realize the liquid-liquid extraction in
chemical laboratory? (general steps of the
process).
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How separation of the immiscible layers does
realized?
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Text for reading (extraction in
laboratory).
English literature review about your
scientific research.
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Associate professor, PhD, Ostvald Roman
Tomsk Polytechnic University, Institute of Physics and Technology
Chair of Rare, Scattered and Radioactive Elements Applied Chemistry
Tomsk 2011