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Radiation Sensors Zachariadou K. | TEI of Piraeus Radiation Sensors Part-V Semiconductor Sensors Part-V Semiconductor Sensors The course is largely based on : G. F. Knoll, “Radiation detection and measurement” ; 3rd ed., New York, Wiley, 2000 Gordon Gilmore & John D. Hemingway, “ Practical Gamma-Ray Spectrometry”; Willey , 21008 Types of detectors Gas detectors Gas-filled detectors consist of a volume of gas between two electrodes Scintillators the interaction of ionizing radiation produces UV and/or visible light Solid state detectors crystals of silicon, germanium, or other materials to which trace amounts of impurity atoms have been added so that they act as diodes Other , Cerenkov etc… Semiconductor Detectors Semiconductor Detectors They work on same principle as gas-filled detectors: Gas-filled detectors: production of ion pair Semiconductors: production of electron-hole pairs Advantages Drawbacks Only 3eV are required for ionization compared to about 30eV required to create an ion pair in typical gas filled detectors Limitation to small sizes Good stability Radiation-induced damage Thin entrance windows Need for cooling (thermal noise) Simplicity in operation High Energy resolution Compact size Fast timing characteristics Variable effective thickness to match the requirements of the application Band structure-Carriers in an Electric Field Insulators: Eg>5eV Conduction Band - - + + - + Valence Band Semiconductors: Eg~1eV Eo + Eg Air: >35eV EF Scintillators~15eV Eo Thermal excitation: A valence electron gains sufficient thermal energy to be elevated to the conduction band 0 Probability per unit time for thermal excitation: P(T ) Eg 2 KT CT 3 2 e Depends on the ratio of Eg over the absolute temperature Materials with large Eg have low thermal excitation probability Migration in an electric field At low to moderate values of the electric field intensity: The drift velocity is proportional to the electric field v h h E v e e E In Gases: mobility of free electrons >> mobility of positive ion In Semiconductors: mobility of electrons ~ mobility of holes 7 At higher electric field: the drift velocity rises slowly with the field and reaches a saturation velocity: Saturation velocity : v e ~ 10 cm s Time to collect the carriers over typical dimensions (0.1cm) : t 10 ns Semiconductors are among the fastestresponding radiation detectors Semiconductors basics Ionization energy Unbiased p-n junction If it functions as a detector This detector would very poor performance n e- Charge carriers migrate across the junction p + + o - Conduction electrons in the pside will combine with holes vice versa - Accumulated space charges create an electric field that opposites the conduction carriers migration Depletion region The space charges do not contribute to conductivity. The depletion region has very high resistivity electron-holes pairs created by the passage of radiation will be swept out their motion is an electrical signal. p n e- + - + - o eND (x) eNA d 2 (x) ρ(x) dt 2 a x0 0 xb (x) ε The thickness of the depletion region is small E(x) d E dx Contact potential :~1V V(x) V The electric field is not enough to make the charge carriers to move fast incomplete charge collection -a 0 b biased p-n junction p n + - e- o + Forward bias The contact potential is reduced by bias V Large currents are conducted p n Reverse bias + - e- o + - The contact potential is increased by bias V The minority carriers are attracted across the junction. The reverse current is very low + e- - + eND eNA o (x) - d 2 (x) ρ(x) dt 2 (x) ε a x0 0 xb d (-a) d (b) 0 dt dt eN D x a a x 0 d E dx eN A x b 0 x b E(x) Reverse bias V (a) V (b) 0 V(x) V -a 0 b eND 2 x a V a x 0 2 ( x) eNA x b 2 0 x b 2 e- For x=0: + - + - V o eND 2 eNA 2 a b 2 2 d ab b N D a N Ab if 2V d eN N D N A Resistivity : where μ is the mobility of the majority carrier eND 2 2 x a V a x 0 ( x) eNA x b 2 0 x b 2 1 N= dopant concentration 2V d μρ High resistivity(ρ) large depletion region (d) (detecting region) e- + - + - o d Higher reverse bias The capacitance per unit area decreases Small capacitance means less electronic noise resulting to better energy resolution 2V μρ Thicker depletion region C ε Ne d 2V We use largest possible voltage up to fully deplete the junction Semiconductor Radiation sensors The module is reverse-biased-->a depletion region is set up with an electric-field that sweeps charge-carriers to the electrodes. When a charged particle passes across the silicon strip electron-hole pairs are created. The electric field in the depletion region sweeps the new electron-hole pairs to the electrodes where they are collected The time taken for collection decreases as the bias voltage is increased. In a silicon detector 300 m thick, electrons are collected in about 10 ns and holes in about 25 ns. Semiconductor Radiation sensors Germanium need for cryogenics Energy to create +- pair = 2.9 eV Silicon can be used at room temperature. Energy needed to create +- pair= 3.6 eV Less performance for energetic radiation such as rays (it s a light material : atomic number 14) CdTe is the most often used because it combines heavy materials (atomic numbers 48 and 52) with relatively high bandgap energies. Why Ge over Si ? ZGe > ZSi (32 vs 14) photo-electric effect x 60 Compton scattering x 2 Semiconductor detectors Operational characteristics Leakage current Noise and Energy Resolution Bias voltage Pulse rise time Radiation damage Channeling Entrance window Energy calibration Pulse height defect Leakage current Deteriorates energy resolution Bulk leakage current Minority carrier current – Mostly small thermal generation of electron-hole pairs in the depletion region– Need for cooling Silicon resistivity : 50,000Ωcm For bulk 1cm2 R=5000Ω Leakage current I=0.1A If V=500V The current is of the order of 10-6A by a pulse of 105 radiation induced carriers Surface leakage current The Leakage current must not exceed 10-9A Contamination of the surfaces clean techniques Detector noise For silicon diode detectors 3 contributions to noise are most significant: Fluctuations in the bulk generated leakage current Parallel noise Fluctuations in the surface leakage current Poor electrical contacts series noise Detector Bias Voltage Incomplete charge collection. Low Bias Voltage & electric field: Sufficiently high Bias Voltage for complete charge collection saturation region Higher Bias Voltage multiplication region The pulse height rises with applied voltage Corresponds to the region of ion saturation in a gas-filled ion detector The electrons liberated by the incident radiation gain enough energy from the electric field to create further electron-hole pairs . Basis of the operation of silicon avalanche detectors` Pulse rise time Semiconductors are among the fastest radiation detectors. Pulse rise time of the order of 10ns or less The rise time of the output pulse limited by the time required for complete migration of the electrons-holes created by the incident radiation from their point of formation to the opposite extremes of the depletion region The time is minimized with High electric field Small depletion width Dead layer Energy loss before the particle reaches the active volume of the detector The dead layer =metalic electrode + thickness of silicon beneath the electrode in which charge collection is inefficient. The dead layer can be a function of the applied voltage Radiation damage The energy that goes to the creation of electron-hole pairs leads to fully reversible processes BUT the Non-ionizing energy transferred to the atoms cause irreversible changes Increase in leakage current Loss in energy resolution of the detector Channeling In crystalline materials: The rate of energy loss of a charged particle may depend on the orientation of its path with respect to the crystal axes. Particles traveling parallel to crystal plane show lower energy loss The energy deposition depends on the crystal orientation Channeled particles penetrate farther in the crystal To minimize the channeling, detectors are fabricated from silicon cut so that the (111) orientation is perpendicular to the wafer surface Energy calibration The response of semiconductor diode radiation detectors when applied on the measurement of fast electrons, protons, alphas: is Linear The energy calibration obtained for one particle type is very close to that obtained using a different radiation type Most common calibration source: 241-Am Pulse Height defect Response of semiconductor detectors to very heavy ions (fission fragments) Pulse height defect: The pulse height observed is substantially less than that observed for a light ion of the same energy is the difference between the true energy of the heavy ion and its apparent energy (as determined from an energy calibration of the detector obtained using alpha particles) Applications of Semiconductor sensors Charged particle spectroscopy Heavy ion and Fission Fragment Particle identification (Energy loss) (For particle identification through dE/dx we choose detectors thin compared with the particle range) X ray spectroscopy with silicon p-i-n diode Germanium detectors for Gamma-ray spectroscopy For gamma ray detection large depletion region is needed 2V d eN Using Silicon or Germanium depletion beyond 2-3 mm are difficult to achieve. For depletion voltage V<1000V d~10mm and N=1010 atoms/cm3 A. Reduce impurity concentration to achieve large depletion regions B. Reduce impurity concentration by Lithium ion drifting High Purity Germanium (HPGe) or intrinsic germanium : ultra pure Germanium Ge(Li) detectors HPGe type is now in favor because they don’t need permanent cooling as Ge(Li) while detection efficiency and energy resolution are essentially identical Ge-detectors CONFIGURATIONS larger depleted volume more efficient detection Ultra-pure Ge (HPGe) impurity concentration: ~109-1010 cm-3 ! (Ge concentration ~ 1022 cm-3) -HV p+ n Planar Configuration n+ signal Coaxial Configuration p+ n n+ maximization of the sensitive volume (diameter ~8 cm, length ~7-8 cm) p+ n n+ -HV signal Ge Energy resolution Excellent energy resolution in gamma ray spectroscopy The energy resolution: combination of 3 factors: FWHM: 2 WT 2 WD 2 WX Inherent statistical spread in the number of charge carriers WD2 (2.35) 2 FE For F=0.08 E=1333MeV ε=2.96eV WD=1.32KeV 2 WE Contributions of electronic noise Variations in the charge collection efficiency Most significant in detectors with large volumes and low average electric field F=Fano Factor value ε=value necessary to create an electron-hole pair E=incident gamma-ray energy Ge Energy resolution Comparative pulse height spectra recorded by NaI (Tl) and a Ge(Li) detector Silicon detectors and the CMS experimentmore by Caio Laganá (http://www.academia.edu/1680843/Silicon_detectors_and_the_CMS_experiment