Download Semester 4 - Vaal University of Technology

VAAL UNIVERSITY OF TECHNOLOGY
FACULTY OF
APPLIED AND COMPUTER SCIENCES
DEPARTMENT OF CHEMISTRY
LOGBOOK: WORK INTEGRATED LEARNING
&
UNIVERSITY TRAINING
ANALYTICAL CHEMISTRY
FOREWORD
1.
TO THE EMPLOYER
Thank you for your indispensable share as training partner in this important area of
cooperate educations.
You are undoubtedly aware of the fact that a student must have completed six months of
applicable work integrated learning plus the two and a half years prescribed university
training before the National Diploma: Analytical Chemistry (3215035) is awarded to
him/her.
To ensure the effectiveness of the work integrated learning period the employer and must
cooperate as equal partners.
Against this background the friendly request that employers should ensure that the
logbook is kept up to date and is periodically submitted to the applicable school of the
applicable Department of the University for evaluation.
2.
TO THE STUDENT
To qualify for the National Diploma: Analytical Chemistry (3215035) a six month period
of suitable work integrated learning as well as the prescribed University training must be
successfully be completed.
To assist the University in assessing the progress of your work integrated learning, you
have to report on a continuing basis to the Head of Department: Chemistry
The attached logbook makes it easy to keep a permanent record of all your activities
during your work integrated learning period. Your tutor/mentor must certify that you
satisfactorily performed the work reported.
In the event of a change of employer during this period, have your logbook brought up to
date before leaving. The logbook will inform your new employer about you training
programs and activities.
For the period of work integrated learning you must also complete the required
registration form at the Department of the University concerned.
On completion of your work integrated learning program, this logbook and other
documents which may be required must be submitted with your application for the issuing
of your National Diploma.
DR E.B. NAIDOO
HEAD OF DEPARTMENT: CHEMISTRY
TEL: (016) 950 9603
FAX: (016) 950 9794
2
RECORD OF TRAINING OF STUDENT
SURNAME
FIRST NAMES
I. D. NR.
DATE OF BIRTH
SEX
MALE
TITLE
MR
FEMALE
X
X
MRS
MISS
OTHER
STUDENT NUMBER
COURSE
N. DIP: ANALYTICAL CHEMISTRY (3215035)
PERIODS OF
UNIVERSITY TRAINING
S1
S2
S3
S4
S5
PERIODS OF WORK
INTEGRATED
LEARNING
FROM
TO
FROM
TO
FULL-TIME
PART-TIME
EMPLOYER
OFFICIAL STAMP OF EMPLOYER/COMPANY
3
GUIDELINES FOR WORK INTEGRATED LEARNING
AIM OF WORK INTEGRATED LEARNING (WIL):
WIL is an integral part of the training and, together with University Training, form a co-operative
training unit. It is therefore the aim of WIL to compel the students in his/her work situation, to be
actively engaged in the broadening of his/her knowledge and analytical skills. It is also important
that the students be exposed to the industrial world and his/her occupational ethics.
The outline for WIL has been drawn up in order that the prescribed requirements can, where
possible, fit in with the working environment of each students and his employer.
DURATION OF COURSE:
Five semester University training and one semester applicable work integrated learning for a total
minimum duration of three years. Students enroll for WIL by registering for one semester for the
subject “Chemical Industry: Practical P1”.
Students may register for “Chemical Industry: Practical P1” during any semester, even for the
semester immediately preceding full-time study.
WHERE IS WORK INTEGRATED LEARNING DONE?
“Chemical Industry: Practical P1” must be completed by the student at an accredited employer.
GUIDELINES FOR WORK INTEGRATED LEARNING:
1.
REGISTRATION FOR WORK INTEGRATED LEARNING:
It is the responsibility of the student to register at the University for work integrated
learning. No students will be registered without proof of employment. Registration takes
place at the same time as registration for full-time and part-time students during January
and July each year or soon after the student is employed Registration takes place by the
completion of an application to register that is available at the Head of Department:
Chemistry.
2.
REPORTS ON WORK INTEGRATED LEARNING:
The student and his/her employer (training institution) organize his/her work integrated
learning according to aspects referred to in this logbook. The employer may appoint a
mentor for the student. At the end of the training period the student reports to his/her
mentor. The mentor evaluates the report and, using the prescribed form in the logbook,
reports to the University.
3.
GENERAL
University staff will attempt to visit the student during his/her work integrated learning
period Employers are requested to make contact with the department if they experience
any problems or if they want to make any changes to the training programme.
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NATIONAL DIPLOMA: ANALYTICAL CHEMISTRY (3215035)
1.
Admission Requirements
Senior Certificate to its equivalent. (A pass in Mathematics and Physical Science is
recommended).
2.
Duration of course
Full-time: Five semesters of class attendance at a University and one semester applicable
in-service training. The minimum total of duration is three years and no award will be
considered until the complete course (theory and work integrated learning) has been
satisfactorily completed.
Part-time: Over a minimum period of three to four years for persons who are employed in
order that the required work integrated learning may be completed.
3.
Curriculum
Semester 1
Analytical Chemistry I (150413512)
Chemistry I (150417112)
Module 1: Theory
Module 2: Practical
Physics I (150710512)
Mathematics I (160404012)
Communication Skills I (129900612)
AAACA 1B
AACHC 1A
AACHX 1A
AACHY 1A
APFSA 1C
AMISS 1C
HKKVA 1C
Semester 2
Analytical Chemistry II (150416622)
Analytical Chemistry: Practical II (150400622)
Inorganic Chemistry II (150416822)
Physical Chemistry II (150413722)
Organic Chemistry II (150413822)
AAACA 2
AAACP 2A
AAICA 2C
AAFCA 2B
AAOCA 2B
Semester 3
Inorganic Chemistry II (150414203)
Physical Chemistry III (150414303)
Organic Chemistry III (150414103)
Computer Skills I (060205512)
AAICA 3B
AAFCA 3B
AAOCA 3B
AEREV 1B
Semester 4
Analytical Chemistry III (150414503)
Analytical Chemistry: Practical III (150414603)
Chemical Quality Assurance (150416722)
AAACA 3B
AAACP 3B
AACKV 2A
5
Semester 5
Chemical Process Industries II (080506822)
Entrepreneurial Skills (040927512)
Physics II (150710922)
Industrial Chemical Analysis (150417522)
Mathematics II (160404122)
AACPA 2B
BBENT 1A
APFSA 2A
AAIAC 2A
AMISK 2C
Semester 6
Chemical Industry: Practical P1
AACNP 1A
Remarks:
(1)
(2)
4.
Compulsory instructional offerings:
All instructional offerings are compulsory
Prerequisite instructional offerings:
Chemistry I for Inorganic Chemistry II,
Physical Chemistry II and Organic Chemistry II
Syllabuses
Semester 1
ANALYTICAL CHEMISTRY I
AAACA 1B
CONTENTS
THEORY:
1.
Introduction to analytical chemistry.
2.
Laboratory practice and safety.
3.
Calculations in analytical chemistry.
4.
Elementary statistics, including significant figures, precision and accuracy.
5.
Sampling and sample handling.
6.
Introduction to classical analysis.
7.
Technical report writing.
6
CHEMISTRY I
AACHC 1A
MODULE 1: CHEMSITRY: THEORY I
AACHX 1A
CONTENTS
1.
2.
3.
4.
5.
6.
7.
8.
Matter and energy: Atomic structure
Periodic table
Chemical bonding
Nomenclature of inorganic compounds
Chemical equations and stoichiometry
Solutions
Acids, bases and slats
Chemical equilibrium
Electrochemistry and redox theory
Introduction to inorganic chemistry
Introduction to organic chemistry
MODULE 2: CHEMISTRY: PRACTICAL I
AACHY 1A
CONTENTS
1.
2.
3.
4.
5.
6.
Heating techniques
Separation techniques
Cation and anion analysis
Gravimetric analysis
Titrimetric analysis
Redox titrations
PHYSICS 1
APFSA 1C
SECTION A: THEORY
CONTENTS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
Introduction to vectors
Equilibrium of a particle
Motion in a straight line
Newton’s second law
Motion in a plane
Work and energy
Impulse and momentum
Equilibrium moment of a force
Rotation
Elasticity
Fluid statics
Fluid dynamics
Temperature and expansion
Quantity of heat
7
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
29.
30.
31.
Heat transfer
The first law of thermodynamics
Gas law
Electrostatics
Ohm’s law
Resistance and circuits
The magnetic field
The magnetic field of a current
Induced electromotive force
The nature and propagation of light
Images formed by a single surface
Lenses
Refraction through prisms
Illumination
Interference and diffraction
Photon’s, electrons and atoms
Nuclear physics
SECTION B: PRACTICAL
1.
2.
3.
4.
5.
Electricity
Nuclear physics
Optics
Mechanics
Heat
MATHEMATICS I
AMISS 1C
CONTENTS
1.
2.
3.
4.
5.
6.
7.
Calculations
Algebra
The Binomium
Trigonometry
Graphs
Differential calculus
Integral calculus
COMMUNICATION SKILLS
HKKVA 1C
Semester 2
ANALYTICAL CHEMISTRY
1.
2.
3.
4.
5.
6.
AAACA 2C
Gravimetric analysis
Precipitation titrations
Neutralization titrations
Non-aqueous titrations
Complexiometric titrations
Redox titrations
8
7.
8.
Analytical separations
Refractometry and polarimetry
ANALYTICAL CHEMSITRY: PRACTICAL II
AAACP 2A
CONTENTS
Section A: Wet chemical analysis
1.
Revision
2.
Sampling
3.
Gravimetry
4.
Volumetry
5.
Total analysis of complex materials
Section B: Basic instrumental analysis
1.
Chromatography
2.
Potentiometry
3.
Refractometry
4.
Polarimetry
INORGANIC CHEMISTRY II
AAAICA 2C
CONTENTS
THEORY
1.
2.
3.
4.
Introduction to chemical bonding and an advanced study of ionic bonding.
Chemical reactions in an aqueous and non-aqueous solution
Redox chemistry: Derivation of oxidation state diagrams
Descriptive inorganic chemistry
4.1
Hydrogen
4.2
Group IA (Li, Na, K)
4.3
Group IIA (Mg, Ca)
4.4
Group IIIA (B, A1)
4.5
Group IVA (C, Si, Ge, Sn, Pb)
4.6
Group VA (N, P, As, Sb, Bi)
4.7
Group VIA (O, S)
4.8
Group VIIA (F, Cl, Br, I)
PRACTICAL
1.
2.
3.
4.
Group IV (C, Si)
Group V (N)
Group VI (O, S)
Group VII (Halogens)
9
PHYSICAL CHEMISTRY II
AAFCA 2B
CONTENTS
THEORY
1.
2.
3.
4.
5.
6.
7.
Gases: ideal and non-ideal
Liquids: surface tension, viscosity, additive properties
Chemical kinetics
Chemical equilibrium
Colloids
Colligative properties of solutions
Electrochemsitry
PRACTICAL
Practical physical chemistry
ORGANIC CHEMISTRY II AAOCA 2B
CONTENTS
THEORY
1.
2.
3.
4.
5.
6.
7.
8.
9.
Introduction
Aliphatic hydrocarbons
Benzene
Alkyl and aryl halides
Alkanols and alkoxyalkanes
Phenols
Alkanals and alkanones
Carboxylix acids and derivatives
Amines
PRACTICAL
1.
2.
3.
4.
Quantitative analysis
Qualitative analysis
Separation and extraction
Elementary techniques (distillation and recrystallisation)
Semester 3
INORGANIC CHEMISTRY III
AAICA 3B
CONTENTS
THEORY
1.
Chemical bonding
10
1.1
1.2
1.3
Theories of covalent bonding
Coordination chemistry
Crystal field and Ligand field theories
2.
Descriptive chemistry of the transition elements
2.1
Extraction and uses
2.2
The first transition series (Sc to Ni)
2.3
Group IB (Cu, Ag, Au)
2.4
Group IIB (Zn, Cd, Hg)
3.
Nuclear chemistry
PRACTICAL
1.
2.
3.
4.
5.
Preparation and study of complexes
Spectroscopic study of transition metal compounds
Preparation of inorganic complexes
Electroplating of metals
Extraction of metals
PHYSICAL CHEMISTRY III
AAFCA 3B
CONTENTS
THEORY
1.
2.
3.
4.
5.
6.
7.
Chemical thermodynamics: First, Second and Third Law
Changing of phase: phase diagrams
Electrochemistry: conductivity, transfer number, eletrolysis
Reaction kinetics: orders, Arrhenius equations, compound mechanisms, catalyses
Quantum chemistry: atomic spectra, emission and absorption spectra, rotational spectra,
Raman, vibrational and electronic spectra
The solid state: crystal lattices, planes, indices, X-ray diffraction, structure of crystals
Surface chemistry: adsorption isotherms, surface reactions
PRACTICAL
1.
2.
3.
4.
5.
6.
7.
8.
Conductometry
Coulometry and electrolysis
Reaction kinetics
Simple thermodynamic determinations
Surface chemistry
Elementary crystallography
Quantum chemistry
Physical properties of gasses and liquids
11
ORGANIC CHEMISTRY III
AAOCA 3B
CONTENTS
THEORY
1.
2.
Introduction
Stereochemistry and conformational analyses
3.
4.
5.
6.
7.
8.
9.
10.
Strength of acids and bases
Nucleophilic reactions and unsaturated carbons
Nucleophilic substitution at saturated carbons
Elimination reactions
Aromatic chemistry
Natural and synthetic polymers
Carbohydrates and related biological compounds
Determination of organic structures
PRACTICAL
1.
2.
3.
Preparation, isolation and purification of organic compounds
Library/laboratory project
Qualitative instrumental analyses of organic compounds
COMPUTER SKILLS 1
AEREV 1B
Semester 4
ANALYTICAL CHEMISTRY III
AAACA 3B
CONTENTS
1.
2.
3.
4.
5.
Data handling
Introduction to absorption and emission spectroscopy
Molecular spectroscopy
3.1
Ultraviolet and visible: Instrumentation
3.2
Ultraviolet and visible: Methods
3.3
Infrared
Atomic spectroscopy
4.1
Flame emission and atomic absorption spectrometry
4.2
Atomic emission spectroscopy
4.3
X-ray methods
Chromatographic methods
5.1
General principles
5.2
Quantitative analyses
5.3
Gas chromatography
5.4
Liquid chromatography
12
6.
7.
Electrometric methods of analysis
6.1
Potentiometry
6.2
Polarography
6.3
Electrogavimetry and coulometry
Thermal analysis
ANALYTICAL CHEMISTRY: PRACTICAL III
AACAP 3B
CONTENTS
1.
2.
3.
4.
5.
6.
Flame atomic spectrometry
1.1
Flame photometry
1.2
Atomic absorption spectrometry
Molecular spectroscopy
2.1
Colorimetry
2.2
UV visible spectrometry
2.3
Infrared spectroscopy
Chromatography
3.1
Gas chromatography
3.2
Liquid chromatography
Electro-analytical methods
4.1
Potentiometry
4.2
Polarography
4.3
Electrogravimetry and coulometry
Atomic emission spectrometry and X-ray methods
5.1
X-ray method
5.2
Atomic emission spectrometry
Thermal analysis
CHEMICAL QUALITY ASSURANCE
AACKV 2A
CONTENTS
1.
2.
3.
4.
5.
Advanced statistical treatment of data in Analytical Chemistry
Optimization and calibration of analytical instruments
Quality assurance systems
Laboratory accreditation
Research methods and techniques
Semester 5
CHEMICAL PROCESS INDUSTRIES II
ACCPA 2B
CONTENTS
Note: Compulsory subjects are points 1, 2, 8 and 9, choice of any three other subjects from lsit.
A minimum of 7 subjects must be covered.
1.
Coal processing
Compulsory
13
2.
Petroleum refining
3.
Synthetic rubber
4.
Plastics
5.
Paper and pulp
6.
Sugar refining
7.
8.
Agrochemicals
Iron and steel
Compulsory
9.
Heavy chemicals
Compulsory
ENTREPRENEURIAL SKILLS
Compulsory
BBENT 1A
CONTENTS
1.
2.
3.
4.
5.
Evaluating opportunity and developing the business concept
Assessing and acquiring necessary resources
Acquiring and existing business
Managing the enterprise and harvesting value
Project
PHYSICS II
APFSA 2A
CONTENTS
SECTION A: ATOMIC PHYSICS (OR QUANTUM PHYSICS)
1.
Interaction of radiation with matter
- Electromagnetic spectrum
- Electromagnetic radiation of waves
(General nature, diffraction, scattering, polarization, reflection, interference, etc)
2.
Quantum mechanical properties of radiation
-
Wave particle duality
Photo electric effect
Absorption, emission, etc
Quantum theory (Rydberg, etc)
Selection Rules
Stark, Zeeman and Doppler effect
SECTION B: OPTICS
1.
Lasers
2.
Diffraction gratings and spectrometers
14
3.
Detectors for spectroscopy – basic principles
(Photo-tubes, silicon diodes, vidicons, CCD, CTD, CID, heat detectors)
4.
Fibre optics
5.
Multiple designs (Fourier Transform, etc)
SECTION C: ELECTRONICS
1.
Solid state physics (diodes, semi-conductors, transistors, microchip technology)
2.
Basic electronics (operational amplifiers and their uses, integration, etc)
3.
Digital electronics (analog/digital signals, binary numbers, microprocessors, basic digital
circuit components)
4.
Signal and noise (S/N ration, sources of noise, S/N enhancement)
SECTION D: MAGNETIC FORCES AND FIELDS
-
Motion of charged particle in magnetic field
Mass spectrometer
Magnetic flux
Magnetic flux density (KMR)
SECTION E: FLOW DYNAMICS
-
Viscosity
Bernoulli’s principle
Laminar and turbulent flow
SECTION F: NUCLEAR PHYSICS
-
Basic principles of radioactivity
Detectors
Applications
INDUSTRIAL CHEMICAL ANALYSIS
AAIAC 2A
CONTENTS
1.
Chemical analysis in complex matrices: an introduction. The analytical approach
2.
Drug analysis in biological fluids.
Introduction – analytical methods in drug analysis
Sample preparation – solid phase extraction
Practical considerations in biopharmaceutical analysis
15
3.
Analysis in the brewing industry.
Introduction – the brewing process
Instrumental methods – criteria
Applications for spectrometric methods
Applications for chromatographic methods
Servo chem. Automatic beer analyzer
Flow injection analysis
4.
Analytical lab in the speciality sealants/adhesives industry.
Introduction – composition and chemical behaviour of sealants/adhesives
Case histories involving problem solving
Useful analytical techniques
5.
Air pollution analysis
Introduction – air pollution system
Gas concentration
Gas sampling techniques
Gas collection devices
Choice of analytical methods
6.
Chemical analysis of animal feed and human food
Introduction – sampling and sample pretreatment
Compositional analysis, nutritional analysis, residence analysis
Agrochemicals and food safety
7.
Water analysis
8.
Metallurgical analysis
9.
Polymer analysis
10.
Sugar analysis
11.
Flow injection and automated analysis
MATHEMATICS II AMISK 2C
CONTENTS
1.
Differentiation
2.
Integration
3.
First order differential equations
4.
Matrix algebra
16
Semester 6
CHEMICAL INDUSTRY: PRACTICAL P1
AACNP 1A
SYLLABUS:
(Proposed study scheme)
Semester 1: University training
Analytical Chemistry I
AAACA 1B
Chemistry I
AACHC 1A
Physics I
APFSA 1C
Mathematics I
AMISS 1C
Communication Skills 1
HKKVA 1C
Semester 2: University training
Analytical Chemistry III
AAACA 2C
Analytical Chemistry: Practical II
AAACP 2A
Inorganic Chemistry II
AAICA 2C
Physical Chemistry
AAFCA 2B
Organic Chemistry
AAOCA 2B
Semester 3: University training
Inorganic Chemistry III
AAICA 3B
Physical Chemistry III
AAFCA 3B
Organic Chemistry III
AAOCA 3B
Computer Skills I
AEREV 1B
Semester 4: Work integrated learning
Aspects in which students
should receive training
SECTION A: GENERAL LABORATORY PRACTICE
Both modules are compulsory.
1.
General laboratory techniques
1.1
Correct sampling techniques
1.2
Sample preparation
1.3
Preparation of standards
1.4
Safety in the laboratory
2.
Laboratory organisation and management
2.1
General laboratory organisation and management
2.2
Preparation of laboratory reports
2.3
Data handling
2.4
Mathematical treatment of results
2.5
Quality assurance
2.6
Laboratory budget
2.7
Handling of chemical literature
2.8
Meeting procedures
SECTION B: WET CHEMICAL ANALYSIS
Both modules are compulsory.
1.
Gravimetric analysis
2.
Titrimetric analysis
17
SECTION C: INSTRUMENTAL ANALYSIS
Any ONE of the following.
1.
Spectroscopic techniques
2.
Chromatography
3.
Electroanalytical techniques
4.
Thermal analysis
SECTION D: GENERAL CHEMISTRY
Any ONE of the following.
1.
Physical test (viscosity, density, etc.)
2.
Physical chemistry (surface studies, kinetics, etc.)
3.
Organic chemistry (synthesis of compounds)
4.
Inorganic Chemistry (synthesis of compounds)
5.
Process chemistry and chemical plant
6.
Water chemistry
Semester 5: University training
Analytical Chemistry III
AAACA 3B
Analytical Chemistry: Practical III
AAACP 3B
Chemical Quality Assurance
AACKV 2A
Physics II
APFSA 2A
Semester 6: University training
Chemical Process Industries II
ACCPA 2B
Entrepreneurial Skills
BBEMT 1A
Industrial Chemical Analysis
AAIAC 2A
Mathematics II
AMISK 2C
18
RECORD OF UNIVERSITY TRAINING
19
RECORD OF UNIVERSITY TRAINING (S1)
VAAL UNIVERSITY OF TECHNOLOGY
PERIOD OF ATTENDANCE: …………………………………………………………………….
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Analytical Chemistry I
Chemistry: Theory I
AAACA 1B
AACHX 1A
Chemistry: Practical I
Physics I
AACHY 1A
APFSA 1C
Mathematics I
AMISS 1C
Communication Skills
HKCOM 1A
% Class
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PASSED / FAILED
REMARKS: ………………………………………………………………………………………
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UNIVERSITY OFFICIAL
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RECORD OF UNIVERSITY TRAINING (S2)
VAAL UNIVERSITY OF TECHNOLOGY
PERIOD OF ATTENDANCE: …………………………………………………………………….
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AAICA 2C
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Physical Chemistry II
AAFCA 2B
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Organic Chemistry II
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Analytical Chemistry II
Inorganic Chemistry II
AAACA 2C
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UNIVERSITY OFFICIAL
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RECORD OF UNIVERSITY TRAINING (S3)
VAAL UNIVERSITY OF TECHNOLOGY
PERIOD OF ATTENDANCE: …………………………………………………………………….
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Results
AAICA 3B
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Physical Chemistry III
AAFCA 3B
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Organic Chemistry III
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Inorganic Chemistry III
Computer Skills I
AEREV 1B
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RECORD OF UNIVERSITY TRAINING (S4)
VAAL UNIVERSITY OF TECHNOLOGY
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AAACP 13B
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Chemical Quality Assurance
AACKV 2A
………….
………….
………….
………….
Physics II
………….
………….
………….
………….
Subjects Rewritten
Exam
Number
Exam
%
Exam.
Results
……………………………………….……
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………….
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Analytical Chemistry III
AAACA 3B
APFSA 2A
% Class
Attendance
PASSED / FAILED
REMARKS: ………………………………………………………………………………………
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SIGNED: …………………………………………
UNIVERSITY OFFICIAL
23
RECORD OF UNIVERSITY TRAINING (S5)
VAAL UNIVERSITY OF TECHNOLOGY
PERIOD OF ATTENDANCE: …………………………………………………………………….
SUBJECTS
Exam
Number
Exam
%
Exam.
Results
Chemical Process Industries II
ACCPA 2B
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………….
Entrepreneurial Skills
………….
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………….
Industrial Chemical Analysis
AAIAC 2A
………….
………….
………….
………….
Mathematics II
………….
………….
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………….
Subjects Rewritten
Exam
Number
Exam
%
Exam.
Results
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………….
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BBENT 1A
AMISK 2C
% Class
Attendance
PASSED / FAILED
REMARKS: ………………………………………………………………………………………
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SIGNED: …………………………………………
UNIVERSITY OFFICIAL
24
RECORD OF UNIVERSITY TRAINING (S6)
FIRM: ………..…………………………………………………………………………………….
PERIOD OF ATTENDANCE: …………………………………………………………………….
SUBJECTS
Exam
Number
Exam
%
Exam.
Results
………….
………….
………….
Subjects Rewritten
Exam
Number
Exam
%
Exam.
Results
……………………………………….……
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………….
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………….
………….
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………….
Chemical Industry: Practical P1
AACNP 1A
% Class
Attendance
………….
PASSED / FAILED
REMARKS: ………………………………………………………………………………………
……………………………………………………………………………………………………..
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SIGNED: …………………………………………
UNIVERSITY OFFICIAL
25
REPORT OF WORK INTEGRATED LEARNING
26
WORK INTEGRATED LEARNING
Only a brief summary is here required.
Nature of Activity
Time period in
(Condensed description)
performed, e.g.
1.1.2003 – 30.6.2003
ORIENTATION
Supervisory
Official
1.1 Information programme
……………………..
……………………..
1.2 Brief survey on the origin and growth of firm
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1. SAMPLING TECHNIQUES
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2. SAMPLE PREPARATION
3. PREPARATIONS OF STANDARDS
4. SAFETY IN THE LABORATORY
5. GENERAL LABORATORY
ORGANISATION AND MANAGEMENT
27
Nature of Activity
(Condensed description)
Time period in
performed, e.g.
1.1.2003 – 30.6.2003
Supervisory
Official
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6. PREPARING OF LABORATORY REPORTS
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7. DATA HANDLING
8. MATHEMATICAL TREATMENT OF
RESULTS
9. QUALITY ASSURANCE
10. LABORATORY BUDGET
11. HANDLING OF CHEMICAL
LITERATURE
28
Nature of Activity
(Condensed description)
Time period in
performed, e.g.
1.1.2003 – 30.6.2003
Supervisory
Official
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12. MEETING PROCEDURES
13. WET CHEMICAL ANALYSIS
GRAVIMETRIC ANALYSIS
TITRIMETRIC ANALYSIS
14. INSTRUMENTAL ANALYSIS
SPECTROSCOPIC TECHNIQUES
29
Nature of Activity
(Condensed description)
Time period in
performed, e.g.
1.1.2003 – 30.6.2003
Supervisory
Official
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Viscosity
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Density
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CHROMATOGRAPHY
ELECTRO-ANALYTICAL TECHNIQUES
THERMOMETRIC ANALYSIS
15. GENERAL CHEMISTRY
PHYSICAL TESTS
PHYSICAL CHEMISTRY
30
Nature of Activity
(Condensed description)
Time period in
performed, e.g.
1.1.2003 – 30.6.2003
Supervisory
Official
…………………………………………….
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ORGANIC CHEMISTRY
INORGANIC CHEMISTRY
PROCESS CHEMISTRY AND CHEMICAL
PLANT
WATER CHEMISTRY
…………………………………………….
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31
EVALUATION REPORT
Excel-lent
1.
Dexterity
2.
Knowledge of techniques,
Good
Acceptable Insufficient Weak
procedures and materials
3.
Safety awareness
4.
Willingness to learn new skills
5.
Initiative
6.
Human relations
7.
Attitude
8.
Efficiency as employee/
Standard of work
9.
Neatness
10. Proficiency
………………………………………..
SIGNATURE
………………………
DATE
RANK/DESIGNATION: …………………………………………………………………………
OFFICIAL STAMP OF EMPLOYER/COMPANY
32
DECLARATION BY EMPLOYER
I, …………………………………………………………………………………………………….
associated with ……………………………………………………………………………………..
in the capacity of …………………………………………………………………………………...
hereby certifies that (name of student) …………………………………………………………….
Was a permanent employee of the company/concern for the past semester and performed the
practical training as required by the University.
I further certify that the work performed by the above mentioned person, was to the benefit of the
company/concern.
Finally I declare that the accompanying report, carrying my signature, is the student’s own as
well as the work set out therein.
………………………………………..
SIGNATURE
………………
DATE
33
RECOMMENDATION BY EMPLOYER RE WORK INTEGRATED LEARNING
Candidate …………………………………………………………………………………………
successfully/unsuccessfully completed his/her work integrated learning.
Mark allocated for Chemical Industry: Practical P1 AACNP 1A: …………… %
……………………………………….
TRAINING OFFICIAL
OFFICIAL STAMP OF EMPLOYER
……………………………..
DATE
34
RECOMMENDATION BY UNIVERSITY RE ISSUING OF DIPLOMA
Candidate …………………………………………………………………………………………
successfully completed his/her Chemical Industry: Practical P1. It is recommended that the
National Diploma: Analytical Chemistry
is issued to him/her with effect from ………………………………………… 20……
……………………………………………..
HEAD OF DEPARTMENT: CHEMISTRY
……………………………..
DATE
35