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SATHYABAMA UNIVERSITY (Established under section 3 of UGC Act, 1956) Jeppiaar Nagar, Rajiv Gandhi Salai, Chennai - 119. SYLLABUS BACHELOR OF TECHNOLOGY PROGRAMME IN CHEMICAL ENGINEERING (8 SEMESTERS) REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING SATHYABAMA UNIVERSITY REGULATIONS – 2010 Effective from the academic year 2010-2011 and applicable to the students admitted to the Degree of Bachelor of Engineering / Technology. (Eight Semesters) 1. Structure of Programme 1.1 2. Every Programme will have a curriculum with syllabi consisting of theory and practical such as: (i) General core courses comprising Mathematics, Basic Sciences, Engineering Sciences. (ii) Core course of Engineering / Technology. (iii) Elective course for specialization in related fields. (iv) Workshop practice, Computer Practice, Engineering Graphics, Laboratory Work, Industrial Training, Seminar Presentation, Project Work, Educational Tours, Camps etc. 1.2 Each semester curriculum shall normally have a blend of lecture courses not exceeding 7 and practical courses not exceeding 4. 1.3 The medium of instruction, examinations and project report will be in English. Duration of the Programme A student is normally expected to complete the B.E/B.Tech. Programme in 8 semesters but in any case not more than 12 consecutive semesters from the time of commencement of the course (not more than 10 semesters for those who join 3rd semester under Lateral entry system) The Head of the Department shall ensure that every teacher imparts instruction as per the number of hours specified in the syllabus and that the teacher teaches the full content of the specified syllabus for the course being taught. 3. Requirements for Completion of a Semester A candidate who has fulfilled the following conditions shall be deemed to have satisfied the requirement for completion of a semester. 4. 3.1 He/She secures not less than 90% of overall attendance in that semester. 3.2 Candidates who do not have the requisite attendance for the semester will not be permitted to write the University Exams. Examinations The examinations shall normally be conducted between October and December during the odd semesters and between March and May in the even semesters. The maximum marks for each theory and practical course (including the project work and Viva Voce examination in the Eighth Semester) shall be 100 with the following breakup. (i) Theory Courses Internal Assessment : 20 Marks University Exams (ii) : 80 Marks Practical Courses Internal Assessment : - University Exams B.Tech. (CHEMICAL ENGINEERING) : 100 Marks i REGULATIONS 2010 SATHYABAMA UNIVERSITY 5. 6. FACULTY OF CHEMICAL ENGINEERING Passing requirements (i) A candidate who secures not less than 50% of total marks prescribed for the course (For all courses including Theory, Practicals and Project work) with a minimum of 35 marks out of 80 in the University Theory Examinations, shall be declared to have passed in the Examination. (ii) If a candidate fails to secure a Pass in a particular course, it is mandatory that he/she shall reappear for the examination in that course during the next semester when examination is conducted in that course. However the Internal Assessment marks obtained by the candidate in the first attempt shall be retained and considered valid for all subsequent attempts. Eligibility for the Award of Degree A student shall be declared to be eligible for the award of the B.E/B.Tech. degree provided the student has successfully completed the course requirements and has passed all the prescribed examinations in all the 8 semesters within the maximum period specified in clause 2. 7. Award of Credits and Grades All assessments of a course will be done on absolute marks basis. However, for the purpose of reporting the performance of a candidate, Letter Grades will be awarded as per the range of total marks (out of 100) obtained by the candidate as given below: RANGE OF MARKS FOR GRADES Range of Marks Grade Grade Points (GP) 90-100 A++ 10 80-89 A+ 9 70-79 B++ 8 60-69 B+ 7 50-59 C 6 00-49 F 0 ABSENT W 0 CUMULATIVE GRADE POINT AVERAGE CALCULATION The CGPA calculation on a 10 scale basis is used to describe the overall performance of a student in all courses from first semester to the last semester. F and W grades will be excluded for calculating GPA and CGPA. CGPA = Σi C i GPi Σi C i where Ci - Credits for the subject GP i - Grade Point for the subject Σi - Sum of all subjects successfully cleared during all the semesters 8. Classification of the Degree Awarded 1. A candidate who qualifies for the award of the Degree having passed the examination in all the courses of all the semesters in his/her first appearance within a maximum period of 8 consecutive semesters after commencement of study (maximum of 6 semesters for Lateral entry system who join the course in the third semester) securing a CGPA not less than 9.0 shall be declared to have passed the examination in First Class – Exemplary. B.Tech. (CHEMICAL ENGINEERING) ii REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING 2. A candidate who qualifies for the award of the Degree having passed the examination in all the courses of all the semesters in his/her first appearance within a maximum period of 8 consecutive semesters after commencement of study (maximum of 6 semesters for Lateral entry system who join the course in the third semester) securing a CGPA not less than 7.5 shall be declared to have passed the examination in First Class with Distinction. 3. A candidate who qualifies for the award of the Degree having passed the examination in all the courses of all the semesters within a maximum period of 8 consecutive semesters after commencement of study (maximum of 6 semesters for Lateral entry system who join the course in the third semester) securing a CGPA not less than 6.0 shall be declared to have passed the examination in First Class. 4. All other candidates who qualify for the award of the Degree having passed the examination in all the courses of all the 8 semesters within a maximum period of 12 consecutive semesters (10 consecutive semesters for Lateral Entry system who join the course in the third semester) after his/her commencement of study securing a CGPA not less than 5.0 shall be declared to have passed the examination in Second Class. 5. A candidate who is absent in semester examination in a course/project work after having registered for the same, shall be considered to have appeared in that examination for the purpose of classification of degree. For all the above mentioned classification of Degree, the break of study during the programme, will be counted for the purpose of classification of degree. 6. A candidate can apply for revaluation of his/her semester examination answer paper in a theory course, within 1 week from the declaration of results, on payment of a prescribed fee along with prescribed application to the Controller of Examinations through the Head of Department. The Controller of Examination will arrange for the revaluation and the result will be intimated to the candidate concerned through the Head of the Department. Revaluation is not permitted for practical courses and for project work. Final Degree is awarded based on the following: CGPA ≥ 9.0 - First Class - Exemplary CGPA ≥ 7.50 < 9.0 - First Class with Distinction CGPA ≥ 6.00 < 7.50 - First Class CGPA ≥ 5.00 < 6.00 - Second Class Minimum CGPA requirements for award of Degree is 5.0 CGPA. 9. Discipline Every student is required to observe disciplined and decorous behaviour both inside and outside the University and not to indulge in any activity which will tend to bring down the prestige of the University. If a student indulges in malpractice in any of the University theory / practical examination, he/she shall be liable for punitive action as prescribed by the University from time to time. 10. Revision of Regulations and Curriculum The University may revise, amend or change the regulations, scheme of examinations and syllabi from time to time, if found necessary. B.Tech. (CHEMICAL ENGINEERING) iii REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING B.Tech - CHEMICAL ENGINEERING REGULATIONS 2010 – CURRICULUM SEMESTER I Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SCHX1001 Environmental Science and Engineering 3 0 0 3 1 2. SMTX1001 Engineering Mathematics – I 3 1 0 4 2 3. SPHX1001 Physics of Materials 3 0 0 3 3 4. SCYX1001 Engineering Chemistry 3 0 0 3 4 5. SBTX1005 Biology for Engineers 3 0 0 3 5 6. SMEX1002 Engineering Graphics 3 0 0 3 6 7. SCSX1002 Programming in C 3 0 0 3 7 8. SPHX4001 Physics Lab – I 0 0 2 1 8 9. SCYX4001 Chemistry Lab-I 0 0 2 1 8 10. SCSX4002 Programming in C Lab 0 0 4 2 8 PRACTICAL TOTAL CREDITS 26 SEMESTER II Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SHSX1001 English For Science and Technology 3 0 0 3 9 2. SMTX1002 Engineering Mathematics – II 3 1 0 4 10 3. SPHX1002 Applied Physics 3 0 0 3 11 4. SCYX1003 Chemistry of Industrial Materials 3 0 0 3 12 5. SPRX1001 Basic Mechanical and Civil Engineering 3 0 0 3 13 6. SEEX1002 Basic Electrical and Electronics Engineering 3 0 0 3 14 7. SMEX1006 Material Technology 3 0 0 3 15 8. SPHX4002 Physics lab – II 0 0 2 1 16 9. SCYX4002 Chemistry lab-II 0 0 2 1 16 10. SPRX4001 Mechanical workshop Lab 0 0 4 2 16 PRACTICAL TOTAL CREDITS 26 L - Lecture hours; T - Tutorial hours; P - Practical hours; C - Credits B.Tech. (CHEMICAL ENGINEERING) iv REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING SEMESTER III Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SMTX1009 Engineering Mathematics – III 3 1 0 4 17 2. SCSX1014 Object Oriented programming 3 0 0 3 18 3. SCHX1002 Chemical Engineering Thermodynamics-I 3 0 0 3 19 4. SCHX1003 Fluid Mechanics 3 0 0 3 20 5. SCHX1004 Chemical Process Calculations 3 1 0 4 21 6. SMEX1010 Strength of Materials 3 0 0 3 22 7. SCHX1005 Inorganic Chemical Technology 3 0 0 3 23 8. SMEX4007 Mechanical Engineering Lab 0 0 4 2 24 9. SCSX4009 Object Oriented programming Lab 0 0 4 2 24 PRACTICAL TOTAL CREDITS 27 SEMESTER IV Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SMTX1010 Engineering Mathematics – IV 3 1 0 4 25 2. SCHX1006 Physical Chemistry 3 0 0 3 26 3. SCHX1007 Chemical Engineering Thermodynamics-II 3 1 0 4 27 4. SCHX1008 Organic Chemical Technology 3 0 0 3 28 5. SCHX1009 Mechanical Operations 3 0 0 3 29 6. SCHX1010 Instrumental Methods of Analysis 3 0 0 3 30 7. SCHX4001 Physical Chemistry & Chemical Technology Lab 0 0 4 2 31 8. SCHX4002 Fluid Mechanics Lab 0 0 4 2 31 PRACTICAL TOTAL CREDITS B.Tech. (CHEMICAL ENGINEERING) v 24 REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING SEMESTER V Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SMTX1011 Applied Numerical Methods 3 1 0 4 32 2. SCHX1025 Mass Transfer - I 3 0 0 3 33 3. SCHX1026 Chemical Reaction Engineering - I 3 0 0 3 34 4. SCHX1027 Chemical Plant Utilities 3 0 0 3 35 5. SCHX1028 Heat Transfer 3 0 0 3 36 6. SCHX1029 Process Equipment Design & Drawing – I 3 0 0 3 37 7. SCHX1030 Instrumentation & Process Control 3 0 0 3 38 8. SCHX4004 Mechanical Operations Lab 0 0 4 2 39 9. SCHX4005 Process Dynamics & Control Lab 0 0 4 2 39 PRACTICAL TOTAL CREDITS 26 SEMESTER VI Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SMEX1017 Resource Management Techniques 3 0 0 3 40 2. SCHX1031 Mass Transfer - II 3 1 0 4 41 3. SCHX1032 Chemical Reaction Engineering – II 3 1 0 4 42 4. SCHX1033 Process Equipment Design & Drawing – II 3 0 0 3 43 5. Elective – I 3 0 0 3 6. Elective – II 3 0 0 3 PRACTICAL 7. SCHX4006 Heat Transfer Lab 0 0 4 2 44 8. SCHX4007 Mass Transfer Lab 0 0 4 2 44 TOTAL CREDITS B.Tech. (CHEMICAL ENGINEERING) vi 24 REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING SEMESTER VII Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SBAX1001 Principles of Management & Professional Ethics 3 0 0 3 45 2. SCHX1034 BioChemical Engineering 3 0 0 3 46 3. SCHX1035 Transport Phenomena 3 1 0 4 47 4. SCHX1036 Energy Engineering 3 0 0 3 48 5. Elective – III 3 0 0 3 6. Elective – IV 3 0 0 3 Chemical Reaction Engineering Lab 0 0 4 2 PRACTICAL 7. SCHX4008 TOTAL CREDITS 52 21 SEMESTER VIII Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. THEORY 1. SBAX1002 Engineering Economics & Marketing Management 3 0 0 3 49 2. SCHX1037 Process Modeling Simulation & Optimization 3 0 0 3 50 3. SCHX1038 Industrial Safety & Hazard Analysis 3 0 0 3 51 4. SCHX4009 Process Simulation Lab 0 0 4 2 52 5. S19PROJ Project Work & Viva Voce 0 0 30 15 52 PRACTICAL B.Tech. (CHEMICAL ENGINEERING) TOTAL CREDITS 26 TOTAL CREDITS FOR THE COURSE 200 vii REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING ELECTIVES Note: ONE SUBJECT IS TO BE CHOSEN FROM EACH GROUP COMPULSORILY Sl. No. SUBJECT CODE SUBJECT TITLE L T P C Page No. Group 1: COMPUTER APPLICATIONS IN CHEMICAL ENGINEERING 1. SCHX1040 Optimization of chemical processes 3 0 0 3 53 2. SCHX1054 Computer applications in chemical engineering 3 0 0 3 54 3. SMEX1038 Computational fluid dynamics 3 0 0 3 55 Group 2: CHEMICAL ENGINEERING BASED TECHNOLOGIES 4. SCHX1041 Food technology 3 0 0 3 56 5. SCHX1042 Fertilizer technology 3 0 0 3 57 6. SCHX1043 Polymer technology 3 0 0 3 58 7. SCHX1044 Oils and fats technology 3 0 0 3 59 8. SCHX1049 Drugs and pharmaceutical technology 3 0 0 3 60 9. SCHX1052 Petroleum technology 3 0 0 3 61 10. SCHX1055 Nano technology 3 0 0 3 62 Group 3: CHEMICAL ENGINEERING ALLIED 11. SBAX1003 Entrepreneurship development 3 0 0 3 63 12. SCHX1046 Environmental pollution and control 3 0 0 3 64 13. SCHX1047 Novel separation processes 3 0 0 3 65 14. SCHX1051 Industrial catalysis 3 0 0 3 66 15. SCHX1053 Multicomponent separation system 3 0 0 3 67 Group 4: ENGINEERING APPLICATIONS 16. SCHX1039 Corrosion engineering 3 0 0 3 68 17. SCHX1045 Fluidization engineering 3 0 0 3 69 18. SCHX1048 Electrochemical engineering 3 0 0 3 70 19. SCHX1050 Nuclear engineering 3 0 0 3 71 B.Tech. (CHEMICAL ENGINEERING) viii REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING DUAL DEGREE IN COMPUTER SCIENCE Provision for candidates from Non-IT Branches of B.E/B.Tech to undergo Dual Degree Programme leading to B.E in Computer Science. A. Duration and Curriculum Candidates selected for a Dual degree programme shall undergo additional courses pertaining to Computer Science. These courses constitute with additional Curriculum as per annexure and consist of both core course and electives. The additional courses are to be undergone concurrently from the 3rd semester of the B.E/B.Tech. (Non-IT) degree programme and extends for one more year beyond the fourth year of the regular B.E/B.Tech. (Non-IT) degree programme to which he/she was first admitted. The additional courses are to be offered from 3rd to 8th Semester after normal working hours so that the regular B.E/B.Tech. (NonIT) remains unaffected. B. A candidate undergoing dual degree programme should satisfy minimum attendance requirements for the course of additional Curriculum for each semester, as stipulated for the regular B.E/B.Tech. Degree Programme. C. For the courses of additional Curriculum, a candidate has to write the same examination that is held for the regular B.E. Computer Science. D. The passing rules for the dual degree programme shall be same as that of the regular B.E/B.Tech. Degree programme. E. A candidate shall be declared to be eligible for the additional degree of B.E. Computer Science provided that (i) (ii) (iii) The candidate has qualified for the regular B.E. or B.Tech. Degree in the non-IT branch in which he/she was originally admitted. The candidate has successfully completed all the courses prescribed in the additional Curriculum within a maximum period of 12 semesters from the date of first admission. There is no disciplinary action pending against the student. B.Tech. (CHEMICAL ENGINEERING) ix REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING CURRICULUM SUBJECTS FOR DUAL DEGREE PROGRAMME IN COMPUTER SCIENCE THIRD SEMESTER Sl.No. SUBJECT CODE NAME OF THE SUBJECT L T P C THEORY 1 SCSX1004 Software Engineering 3 0 0 3 2 SCSX1005 Data Structures & Algorithms 3 1 0 4 SCSX4004 Data Structures Lab 0 0 4 2 PRACTICALS 3 TOTAL CREDITS 9 FOURTH SEMESTER THEORY 1 SCSX1007 Java Programming 3 0 0 3 2 SCSX1009 Computer Architecture & Organization 3 0 0 3 SCSX4005 Java Programming Lab 0 0 4 2 PRACTICALS 3 TOTAL CREDITS 8 FIFTH SEMESTER THEORY 1 SCSX1017 Data Communication and Computer Networks 3 1 0 4 2 SCSX1018 Database Systems 3 1 0 4 SCSX4011 RDBMS Lab 0 0 4 2 PRACTICALS 3 TOTAL CREDITS 10 SIXTH SEMESTER THEORY 1 SCSX1019 System Programming 3 0 0 3 2 SCSX1022 J2EE 3 0 0 3 SCSX4010 System Programming Lab 0 0 4 2 PRACTICALS 3 TOTAL CREDITS B.Tech. (CHEMICAL ENGINEERING) x 8 REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING SEVENTH SEMESTER THEORY 1 SCSX1008 C# and .Net 0 0 0 3 2 SCSX1011 Operating System 3 1 0 4 SCSX4006 C# and .Net Lab 0 0 4 2 PRACTICALS 3 TOTAL CREDITS 9 EIGHTH SEMESTER THEORY 1 SCSX1024 Network Programming & Management 3 0 0 3 2 Elective I 3 0 0 3 3 Elective II 3 0 0 3 Network Programming Lab 0 0 4 2 PRACTICALS 4 SCSX4012 TOTAL CREDITS 11 NINETH SEMESTER THEORY 1 SCSX1023 Computer Systems 2 SCSX1030 3 4 Graphics & Multimedia 3 0 0 3 Datamining & Warehousing 3 0 0 3 SCSX1025 Wireless & Mobile Networks 3 0 0 3 SCSX1027 Hardware Peripherals and Interfacing 3 0 0 3 5 Elective III 3 0 0 3 6 Elective IV 3 0 0 3 PRACTICALS 7 SCSX4014 Hardware Peripherals Lab 0 0 4 2 8 SCSX4015 Case Tools & Testing Lab 0 0 4 2 TOTAL CREDITS 22 TENTH SEMESTER 1 S11XPROJ Project Work and Viva-Voce 0 0 30 TOTAL CREDITS 15 15 TOTAL COURSE CREDITS : 92 B.Tech. (CHEMICAL ENGINEERING) xi REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING ELECTIVES FOR DUAL DEGREE PROGRAMME IN COMPUTER SCIENCE Sl.No. SUBJECT CODE 1. SCSX1020 2. L T P C Component Based Technology 3 0 0 3 SCSX1026 Cryptography & Network Security 3 0 0 3 3. SCSX1028 Distributed Computing 3 0 0 3 4. SCSX1032 Management Information System 3 0 0 3 5. SCSX1036 FOSS 3 0 0 3 6. SCSX1038 Software Quality Assurance and Testing 3 0 0 3 7. SCSX1039 Unified Modeling Language 3 0 0 3 8. SCSX1042 Robotics 3 0 0 3 9. SCSX1043 Unix Internals 3 0 0 3 10. SCSX1044 Multicore Programming 3 0 0 3 11. SCSX1047 High Performance Network 3 0 0 3 12. SCSX1048 Grid Computing 3 0 0 3 13. SCSX1049 Client Server Architecture 3 0 0 3 14. SCSX1050 TCP/IP and Socket Programming 3 0 0 3 15. SCSX1057 Cloud Computing 3 0 0 3 B.Tech. (CHEMICAL ENGINEERING) NAME OF THE SUBJECT xii REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1001 FACULTY OF CHEMICAL ENGINEERING ENVIRONMENTAL SCIENCE AND ENGINEERING L T P Credits Total Marks (Common to all Branches) 3 0 0 3 100 UNIT I INTRODUCTION TO ENVIRONMENTAL STUDIES AND NATURAL RESOURCES 12 hrs. Definition, scope and importance, need for public awareness, forest resources: use and over-exploitation, deforestation, case studies. Timber extraction, mining, dams, floods, drought, conflicts over water, dams-benefits and problems, mineral resources: use effects on forests and tribal people. water resources: use and over-utilization of surface and ground water, exploitation, environmental effects of extracting and using mineral resources, case studies - food resources: world food problems, changes caused by agriculture and overgrazing, effects of modern agriculture, fertilizer-pesticide problems, water logging, salinity, case studies. Energy resources: growing energy needs, renewable and non renewable energy sources, use of alternate energy sources. Case studies. land resources: land as a resource, land degradation, man induced landslides, soil erosion and desertification, role of an individual in conservation of natural resources, equitable use of resources for sustainable lifestyles. UNIT II ECOSYSTEMS AND BIODIVERSITY 12 hrs. Concept of an ecosystem, structure and function of an ecosystem - producers, consumers and decomposers energy flow in the ecosystem, ecological succession, food chains, food webs and ecological pyramids. Introduction, types, characteristic features, structure and function of the (a) forest ecosystem (b) grassland ecosystem (c) desert ecosystem (d) aquatic ecosystems (ponds, streams, lakes, rivers, oceans, estuaries). Introduction to biodiversity, definition: genetic, species and ecosystem diversity - biogeographical classification of India - value of biodiversity: consumptive use, productive use, social, ethical, aesthetic and option values, biodiversity at global, national and local levels. India as a mega-diversity nation, hot-spots of biodiversity, threats to biodiversity: habitat loss, poaching of wildlife, man-wildlife conflicts, endangered and endemic species of India, conservation of biodiversity, in-situ and ex-situ conservation of biodiversity. UNIT III ENVIRONMENTAL POLLUTION 10 hrs. Definition - causes, effects and control measures of: (a) air pollution (b) water pollution (c) soil pollution (d) marine pollution (e) noise pollution (f) thermal pollution (g) nuclear hazards. solid waste management: causes, effects and control measures of urban and industrial wastes, role of an individual in prevention of pollution, pollution case studies, disaster management: floods, earthquake, cyclone and landslides. UNIT IV SOCIAL ISSUES AND THE ENVIRONMENT 8 hrs. From unsustainable to sustainable development, urban problems related to energy, water conservation, rain water harvesting, watershed management, resettlement and rehabilitation of people; its problems and concerns, case studies, environmental ethics: issues and possible solutions, climate change, global warming, acid rain, ozone layer depletion, nuclear accidents and holocaust, case studies. wasteland reclamation, consumerism and waste products - environment protection act: air (prevention and control of pollution) act - water (prevention and control of pollution) act, wildlife protection act; forest conservation act. Issues involved in enforcement of environmental legislation - public awareness. UNIT V HUMAN POPULATION AND THE ENVIRONMENT 8 hrs. Population growth, variation among nations, population explosion, family welfare programme, environment and human health, human rights, value education, HIV / AIDS, women and child welfare, role of information technology in environment and human health, case studies. Visit to a local area to document environmental assets-river/forest/grassland/hill/mountain. Visit to a local polluted site-urban/rural/ industrial/agricultural-study of common plants, insects, birds-study of simple ecosystems, pond, river, hill slopes etc. TEXT / REFERENCE BOOKS: 1. Meenakshi.P, Elements of Environmental Science and Engineering, 1st Edition, Prentice Hall of India, New Delhi, 2009. 2. Ravikrishnan. A, Environmental Science & Engineering, 3rd Edition, Sri Krishna Publications, Chennai, 2008. 3. Wrigh.R.T & Nebel B.J, Environmental science-towards a sustainable future by Richard 8th edition, Prentice Hall of India, NewDelhi, 2006 4. Erach Bharucha, Text Book of Environmental Studies, University Press, Chennai, 2006. UNIVERSITY EXAM QUESTION PAPER PATTERN: Max. Marks: 80 Exam Duration: 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 1 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMTX1001 FACULTY OF CHEMICAL ENGINEERING ENGINEERING MATHEMATICS – I L T P Credits Total Marks (Common to all branches except Bio Groups) 3 1 0 4 100 UNIT I TRIGONOMETRY 10 hrs. Review of Complex numbers and De Moivre’s Theorem. Expansions of Sinnθ and Cosnθ; Sinθ and Cosθ in powers of θ, Sinnθ and Cosnθ in terms of multiples of θ. Hyperbolic functions – Inverse hyperbolic functions. Separation into real and imaginary parts of complex functions UNIT II MATRICES 10 hrs. Characteristic equation of a square matrix - Eigen values and Eigen vectors of a real matrix- properties of Eigen values and Eigen vectors, Cayley-Hamilton theorem (without proof) verification – Finding inverse and power of a matrix. Diagonalisation of a matrix using similarity transformation (concept only) , Orthogonal transformation – Reduction of quadratic form to canonical form by orthogonal transformation. UNIT III GEOMETRICAL APPLICATIONS OF DIFFERENTIAL CALCULUS 10 hrs. Curvature –centre, radius and circle of curvature in Cartesian co-ordinates only – Involutes and evolutes – envelope of family of curves with one and two parameters – properties of envelopes and evolutes – evolutes as envelope of normal. UNIT IV FUNCTIONS OF SEVERAL VARIABLES 10 hrs. Functions of two variables – partial derivatives – Euler’s theorem and problems - Total differential – Taylor’s expansion – Maxima and minima – Constrained maxima and minima – Lagrange’s multiplier method – Jacobian – Differentiation under integral sign. UNIT V ORDINARY DIFFERENTIAL EQUATION 10 hrs. ax Second order linear differential equation with constant coefficients – Particular Integrals for e , sin ax, cos ax, xn, xneax, eax sinbx, eax cos bx. Equations reducible to Linear equations with constant co-efficient using x=et. Simultaneous first order linear equations with constant coefficients - Method of Variations of Parameters. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. Veerarajan. T , “Engineering Mathematics for First Year”, Tata McGraw Hill Publishers ,II Edition, 2008. Kandaswamy.P. & co., “Engineering Mathematics for First Year”, S.Chand & Co Pub., IX revised edition, 2010. Moorthy M.B.K, Senthilvadivu. K ,”Engineering Mathematics-I”, VRB Pub., Revised Edition, 2010. Arumugam. S & co. “Engineering Mathematics Vol-I”, SciTech Pub., Revised Edition, 2010. Venkataraman M.K.,”Engineering Mathematics – First Year” (2nd edition), National Publishing Co., 2000. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 2 REGULATIONS 2010 SATHYABAMA UNIVERSITY SPHX1001 FACULTY OF CHEMICAL ENGINEERING PHYSICS OF MATERIALS L T P Credits Total Marks (Common to all Branches of B.E / B.Tech) 3 0 0 3 100 UNIT I CONDUCTING AND SUPERCONDUCTING MATERIALS 10 hrs. Classical Free electron theory of Metals-Derivation of Electrical and Thermal Conductivity- Deduction of Wiedemann Franz law-Lorentz number. Introduction to Band theory, Difference between Conductors, Semiconductors and Insulators - Superconductivity-Transition temperature - occurrence of superconductivity - BCS Theory(Qualitative), properties of superconductors -Type I &Type II superconductors, High Tc superconductors, AC & DC Josephson effects. Applications of superconductors – basic concepts of SQUID, cryotron, magnetic levitation. UNIT II MAGNETIC AND DIELECTRIC MATERIALS 10 hrs. Types based on spin. Hard and soft magnetic materials, domain theory of Ferromagnetism, magnetic bubbles, formation and propagation of magnetic bubbles, applications of magnetic materials - Magnetic storage devices. Dielectric parameters, polarization, polarisability, types of polarization. Internal or local electric field - derivation of Lorentz Equation and Clausius - Mossotti Equation, dielectric loss and breakdown, types of dielectric breakdown, types of dielectric materials, applications. UNIT III OPTICAL MATERIALS 10 hrs. Optical processes and Excitons - types, Traps - Trapping and recombination, types, Point defects –Frenkel and Schottky defects - Colour centers - types and their mechanisms, Luminescence - Photoluminescence - TypesFluorescence and Phosphorescence- Mechanism and its applications, Cathodoluminescence, Electroluminescence. Non-linear Optical Materials – Basic Principle, Classifications, Properties - Frequency Doubling or Tripling, Optical Mixing - Applications. UNIT IV MODERN ENGINEERING MATERIALS 10 hrs. Metals and alloys – steel and its properties - Iron-carbon phase diagram, Titanium and Aluminium based alloys - Introduction, properties and Applications. Shape Memory Alloys (SMA) - Principle of shape memory effects, Hysteresis curve, Two way shape memory alloys, super-elasticity and thermo-mechanical behavior. Characterization methods to identify the phase transformation of SMA, commercial SMA – Ni-Ti alloys, copper alloys and Cu-Al alloys, Applications. Ceramics – Classification, Properties, fabrication, advanced ceramics and applications. Composites – particle reinforced composites and fiber reinforced composites – processing and applications. UNIT V CHARACTERIZATION OF MATERIALS 10 hrs. Structural characterization – X-ray diffraction, electron diffraction and neutron diffraction – Determination of crystal structure. Difference among these diffraction techniques.Micro structural characterization – optical microscope, scanning electron microscope, transmission electron microscope, atomic force microscopy, micro and nano hardness testing – principle and applications. REFERENCE BOOKS : 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. Ragavan.V, Material science and Engineerimg, 5th Edition, Eastern Eco, 2004. Suresh.R and Jayakumar.V, Materials Science, 1 st Edition, Lakshmi Publication, 2003. Wilson.J and Hawkes.J.F.B, Optoelectronics- An Introduction, 2 nd Edition, Prentice-Hall of India, 2001. Dr.Arumugam M., Semiconductor Physics and Opto electronics, 1st Edition, Anuradha Publishers, 2003. Gaur.R.K and Gupta.S.L, Engineering Physics, 8 th Edition, Dhanbat Rai Publications,2007. Palanisamy.P.K, Engineering Physics, 1 st Edition, SCITECH Publications, 2007. Sankar.B.N and Pillai.S.O, A text book of Engineering Physics, 1 st Edition, New Age international Publishers, 2007. Rajendran.V, Engineering Physics, 2nd Edition, Tata McGraw-Hill, 2008. Avadhanulu.M.N and P.G. Kshirsagar.P.G, Engineering Physics, 2 nd Edition, S. Chand & Company, 2007. Dr. Arumugam M., Engineering Physics, 2nd Edition, Anuradha Publications, 2002. William D.Callister,Jr, Materials Science and Engineering An introduction, 6 th Edition, John-Wiley and Sons, 2004. Cullity.B.D, Principles of X-ray diffraction, 3 rd Edition, Prentice Hall, 2001 ‘Applications’ mentioned in the syllabus refer to the basic applications and not to any specific case. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration: 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks Out of 20 marks, maximum of 10% problems may be asked. 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks Out of 60 marks, maximum of 10% problems may be asked 60 marks B.Tech. (CHEMICAL ENGINEERING) 3 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCYX1001 FACULTY OF CHEMICAL ENGINEERING ENGINEERING CHEMISTRY L T P Credits Total Marks (Common to all branches) 3 0 0 3 100 UNIT I WATER TECHNOLOGY 10 hrs. Introduction: Impurities present in water, Hardness: Types of hardness, Expression, Units. Estimation of hardness by EDTA method, Problems. Boiler Troubles: Sludge & Scales, Boiler Corrosion. Water Softening: Zeolite process, Demineralization process, Merits and Demerits. Reverse osmosis, Merits and Demerits. Domestic water treatment: Flow chart diagram only. UNIT II BATTERIES AND FUEL CELLS 10 hrs. Introduction - Battery terminology: Primary cells, Secondary batteries, Charging and Discharging characteristics, Capacity, Energy density, Cycle life, Internal resistance. Secondary batteries: Lead-acid accumulator, Nickel-cadmium batteries , Lithium primary cells: Lithium-thionyl chloride cell, Lithium-iodine cell. Lithium secondary batteries: Lithium-ion batteries. Fuel cells: Hydrogen-Oxygen fuel cell, Solid oxide fuel cell (SOFC): Principle, construction, anode cathode and electrolyte. Proton Exchange Membrane Fuel Cell. UNIT III CORROSION SCIENCE 10 hrs. Introduction - Electrochemical cell representation. Electrochemical series: Significance. Galvanic series. Corrosion: Definition of corrosion, Dry corrosion: Mechanism of Dry corrosion, Pilling-Bedworth rule, Wet Corrosion: Mechanism. Types of corrosion: Galvanic corrosion, Differential aeration corrosion, Pitting corrosion, Microbial Corrosion. Factors influencing corrosion: Nature of the metal, nature of the environment. Corrosion control: Material selection and Design, Cathodic protection. Corrosion inhibitors: Anodic, cathodic and Vapour phase inhibitors. UNIT IV EXPLOSIVES AND ROCKET PROPELLANTS 10 hrs. Introduction - Explosives: Requirements, Classification of Explosives: Low explosives, primary explosives and high explosives. Assessment of explosives. Rocket engines: Types of rocket engines. Basic principle, Mass fraction, Specific impulse, Thrust, Effective exhaust velocity, Specific propellant consumption. Chemical propellants: Requirements, Classification: Liquid fuels, Liquid oxidizers, Solid fuels, Solid oxidizers. UNIT V SURFACE CHEMISTRY 10 hrs. Introduction. Adsorption: Types, Adsorption of gases on solids, Adsorption of solutes from solution. Adsorption isotherms: Freundlich adsorption isotherm, Langmuir adsorption isotherm. Industrial adsorbent materials: Role of adsorbents in catalysis and water softening. Emulsion: Types: water/oil, oil/water. Applications of adsorption: Cottrell’s precipitator, Coating of rubber on metals, Electrostatic painting. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. Jain P.C. and Monica Jain,Engineering Chemistry, 15th Edition Dhanpat Rai Publishing Co. 2009 Dara S.S., Text Book of Engineering Chemistry, S.Chand & Co, 2008 Sheik Mideen A., Engineering Chemistry (I & II),13 th Edition, Shruthi Publishers, 2010 Parameswara Murthy C, Agarwal C V, Andra Naidu, Textbook of Engineering Chemistry, B S Publications, 2006 Kuriakose J.C. and Rajaram J., Chemistry in Engineering and Technology",. Vol.1 & 2, 5 th reprint, Tata McGraw Hill Publishing Company (P) Ltd., 2010. Sharma B.K., Engineering Chemistry, 2nd Edition, Krishna Prakasam Media (P) Ltd., 2001 Puri Br, Sharma Lr, Madhan S Pathania, Principles of Physical Chemistry, 41st Edition, Vishal Publishing Co., 2004 Mars G Fontana, Corrosion Engineering, 3rd Edition, Tata McGraw Hill, 2008 David Linden, Thomas B Reddy, Handbook of Batteries, 4th Edition, McGraw-Hill, 2010 George Paul Sutton, Oscar Biblarz, Rocket Propulsion Elements, 8 th Edition, John Wiley & Sons, 2010 UNIVERSITY EXAM QUESTION PAPER PATTERN: Max. Marks: 80 Exam Duration: 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks One problem for 5 marks may be asked in Unit 1 - Water Technology B.Tech. (CHEMICAL ENGINEERING) 4 REGULATIONS 2010 SATHYABAMA UNIVERSITY SBTX1005 FACULTY OF CHEMICAL ENGINEERING BIOLOGY FOR ENGINEERS L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION TO CELL BIOLOGY AND BIO-ORGANIC CHEMISTRY 10 hrs. Cell structure and function of cell organelles, Eukaryotic and prokaryotic cells, Cell division, Mitosis, Meiosis, Introduction to peptides, Carbohydrates, fats, proteins-structure, classification. UNIT II INTRODUCTION TO ENZYMES 10 hrs. Enzyme nomenclature, Classification of Enzymes, Michaelis Menten kinetics, Determination of Km, Lineweaver Burk plot, Eadie-Hofstee plot, Hanes -Woolf plot, Types of Enzyme Inhibition, Competitive inhibition, Uncompetitive inhibition, Non-competitive Inhibition, Enzyme immobilization. UNIT III INTRODUCTION TO GROWTH KINETICS 10 hrs. Phases of microbial growth, Microbial growth curve, Cell growth kinetics,-Batch and continuous growth, Kinetics of batch and continuous culture, Sterilization kinetics. UNIT IV INTRODUCTION TO FERMENTATION TECHNOLOGY 10 hrs. Fermentation- basic definition, Types of media and media components, Fermentors and their accessories, Types of Fermentors, Airlift fermentor, Tower fermentor, Continuous stirred tank fermentor. UNIT V INTRODUCTION TO DOWNSTREAM PROCESSING 10 hrs. Stages in downstream operations, Flotation, Flocculation, Filtration, Centrifugation, Release of intracellular products-Cell disruption, Concentration-Liquid Liquid extraction, Evaporation, Membrane filtration, Lyophilization, Drying, Purification by Chromatography. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. Satyanarayana, Biotechnology, 4th Edition, Books and Allied (p) Ltd. 2005-01-01, ISBN . Lehninger A.L, Nelson D.L, Cox .M.M, Principles of Biochemistry. CBS Publications 1993 Shuler.M.L. and Kargi.F, Bioprocess Engineering 1st Edition. Pearson Education India, 2003. Stanbury P.F., A.Whitaker, and Hall S.J. , Principles of Fermentation Technology, 2nd Edition, Butterworth-Heinemann 1997. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration: 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 5 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMEX1001 FACULTY OF CHEMICAL ENGINEERING ENGINEERING GRAPHICS L T P Credits Total Marks (Common to all branches of B.E / B.Tech) 1 2 0 3 100 UNIT I CONSTRUCTION OF PLANE CURVES 10 hrs. Introduction - Importance of graphics in engineering applications – Use of drafting instruments – BIS specifications and conventions – Size, layout and folding of drawing sheets – Lettering and dimensioning- Polygons used in engineering practice– methods of construction of pentagon and hexagon– Construction of ellipse, parabola and hyperbola. UNIT II PROJECTION OF POINTS AND LINES 10 hrs. General principles of orthographic projection – first angle projection – layout of views – projections of points, straight lines located in the first quadrant – Determination of true lengths of lines and their inclinations to the planes of projection – Traces UNIT III PROJECTION OF SOLIDS AND SECTION OF SOLIDS 10 hrs. Projection of solids like prism, pyramid, cylinder and cone when the axis is inclined to only one plane of projection – Change of position method only - Sectioning of above mentioned solids in simple vertical positions by cutting plane inclined to one reference plane and perpendicular to the other – True shapes of sections UNIT IV DEVELOPMENT OF SURFACES AND FREE HAND SKETCHING 10 hrs. Need for development of surfaces – Development of lateral surfaces of simple and truncated solids – Prisms, pyramids, cylinders and cones.- Pictorial representation of engineering objects – Representation of three dimensional objects in two dimensional media – Need for multiple views – Developing visualization skills through free hand sketching of three dimensional objects. UNIT V ISOMETRIC PROJECTIONS & PERSPECTIVE PROJECTIONS 10 hrs. Principles of isometric projection – Isometric scale – Isometric projections of simple solids and combination of solids - Prisms, pyramids, cylinders, cones and spheres (excluding isometric projections of truncated solids) - Perspective projections - Simple objects like – cube, prisms, pyramids by Vanishing point method & Visual Ray method (excluding perspective projections of truncated solids) TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. 7. 8. Natarajan, K.V, “ A Textbook of Engineering Graphics”, Dhanalakshmi Publishers, Chennai, 2006 . Venugopal, K. and Prabhu Raja, V., “Engineering Graphics”, New Age International(P) Ltd.,2008. Ramachandran. S, Pandian. K, Ramanamurthy. E.V.V. and Devaraj. R “Engineering Graphics”, AirWalk Publications, Chennai, 2009 IS 10711-2001: Technical Products Documentation – Size and Layout of Drawing Sheets IS 9609 (Parts 0 & 1 )-2001: Technical Products Documentation – Lettering IS 10714(Part 20)-2001 & SP 46 -2003: Lines for Technical Drawings IS 11669-1986 & SP 46-2003: Dimensioning of Technical Drawings IS 15021(Parts 1 to 4)-2001: Technical Drawings-Projection Methods UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part A: equal distribution of questions from each unit. Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks Part B - Split up: Unit 1: 1 question from construction of hexagon / pentagon / ellipse & 1 question from construction of parabola / hyperbola Unit 2: 1 question from projection of points & 1 question from projection of lines inclined to both the planes. Unit 3: 1 question from projection of solids & 1 question from section of solids. Unit 4: 1 question from development of surfaces & 1 question from orthographic projection. Unit 5: 1 question from isometric projection & 1 question from perspective projection. B.Tech. (CHEMICAL ENGINEERING) 6 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCSX1002 FACULTY OF CHEMICAL ENGINEERING PROGRAMMING IN C L T P Credits Total Marks (Common to all branches of B.E / B.Tech.) 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Algorithms & flowcharts-Overview of C-Features of C-IDE of C Structure of C program-Compilation & execution of C program-Identifiers, variables, expression, keywords, data types, constants, scope and life of variables, local and global variables. Operators: arithmetic, logical, relational, conditional and bitwise operators- Special operators: size of () & comma (,) operator-Precedence and associativity of operators & Type conversion in expressions. Basic input/output and library functions: Single character input/output i.e. getch(), getchar(), getche() & putchar()-Formatted input/output: printf() and scanf()-Library Functions: concepts, mathematical and character functions. UNIT II CONTROL STRUCTURES, FUNCTIONS 10 hrs. Conditional control-Loop control and Unconditional control structures. The Need of a function-User defined and library function- Prototype of a function-Calling of a function-Function argument-Passing arguments to function- Return values-Nesting of function- main()-Command line arguments and recursion. Storage class specifier – auto, extern, static, & register. UNIT III ARRAYS, STRINGS, STRUCTURE AND UNION 10 hrs. Single and multidimensional arrays-Array declaration and initialization of arrays-Array as function arguments. Declaration-Initialization and string handling functions. Defining structure-Declaration of structure variable-Accessing structure members-Nested structures-Array of structures-Structure assignment-Structure as function argument-Function that returns structure- Union. UNIT IV POINTERS AND DMA FUNCTIONS 10 hrs. The ‘&’ and ‘* ’ operators-Pointers expressions-Pointers vs arrays-Pointer to functions-Function returning pointers-Static and dynamic memory allocation in C. malloc(), calloc(), sizeof(), free() and realloc()-Preprocessor directives. UNIT V FILE MANAGEMENT AND GRAPHICS 10 hrs. Defining, opening & closing a file, text file and binary file- Functions for file handling: fopen, fclose, gets, puts,fprint, fscanf, getw, putw, fputs, fgets, fread, fwrite-Random access to files: fseek, ftell, rewind-File name as Command Line Argument. Graphics in PC-Initialize Graphics Mode-Functions used In Graphics - Drawing a Point on the Screen-Drawing lines, rectangles, ovals, circles, arcs, polygon, filling colors-Using Text in Graphics Display. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. Balaguruswami.E, ‘Programming in C’, TMH Publications,1997 Behrouz A. Forouzan & Richard F. Gilberg, “Computer Science A Structured Programming using C”, Cengage Learning, 3rd Edition, 2007 Gottfried , ‘Programming with C’, schaums outline series, TMH publications,1997 Mahapatra , ‘Thinking in C’, Prentice Hall of India, 2nd Edition, 2006. Stevens , ‘Graphics programming in C’, BPB publication, 2006 Subbura.R , ‘Programming in C’, Vikas publishing, 1st Edition, 2000 UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 7 REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING PHYSICS LAB - I SPHX4001 L T P Credits Total Marks 0 0 2 1 50 1. Torsional pendulum- Determination of MI of the disc and rigidity modulus of the wire. 2. Quincke’s method - Determination of magnetic susceptibility of a liquid 3. Semiconductor diode - Determination of width of the forbidden energy gap 4. Ultrasonic interferometer – Determination of Compressibility of liquid 5. Lees disc - Determination of thermal conductivity of a bad conductor. 6. Optical Fiber – Determination of Numerical aperture and attenuation loss. SCYX4001 CHEMISTRY LAB - I L T P Credits Total Marks 0 0 2 1 50 1. Determination of total, permanent and temporary hardness of a water sample. 2. Estimation of copper in an ore by iodometric titration. 3. Determination of strength of HCl by conductometric titration. 4. Estimation of the amount of ferrous ion by titrating with chromate ion using potentiometer. 5. Verification of the Freundlich isotherm by using acetic acid adsorption on charcoal. 6. Determination of the rate of corrosion of iron metal by hydrogen evolution method. SCSX4002 PROGRAMMING IN C LAB L T P Credits Total Marks 0 0 4 2 100 1. To write a simple menu driven calculator program using switch statement. 2. To write a program to calculate the nCr using functions. 3. To write a program to find the largest and smallest number using arrays. 4. To write a program to generate Fibonacci series. 5. To write a program to find the factorial of a number using recursion. 6. To write a program to print the sum of elements of an array using pointers. 7. To write a program to implement file handling 8. To write a program to perform matrix addition and multiplication. 9. To write a program to check for perfect number. 10. To write a program to implement string manipulation functions without using library functions. 11. To write a program to perform ASCII equivalent keystrokes. 12. To write a program to solve a polynomial equation. B.Tech. (CHEMICAL ENGINEERING) 8 REGULATIONS 2010 SATHYABAMA UNIVERSITY SHSX1001 FACULTY OF CHEMICAL ENGINEERING ENGLISH FOR SCIENCE AND TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I 10 hrs. Reading comprehension- Skimming and Scanning - Transcoding -Bar diagram, Tables and Pie chart –Discussing topics of general interest or on current topics and making a presentation in the class - Conjunctions and discourse markers- cloze reading- affixes – definitions- tense- voice – jumbled sentences. UNIT II 10 hrs. Subject verb agreement - Idioms and phrases, reading passages to answer evaluative, inferential and hypothetical type of questions- Listening - Creative thinking and speaking- Formal letters - application for job- resume preparationinviting dignitaries to department workshops, symposium and university functions - Letter to the editor. UNIT III 10 hrs. Reading and summarising reports - Writing a project proposal - Editing - Checking punctuation and grammatical errors- Types of Sentences – preparation of Check List- formulating questions and answers - communicating politely. UNIT IV 10 hrs. Reported speech- Parts of speech- confusable words - Report on industrial visit - project report - Making effective Power Point presentations - speaking about the future plans-expressing opinions-reading and guessing meanings of unknown words from the context – using appropriate verb forms UNIT V 10 hrs. Modal auxiliaries – Presentation of problems and solutions – wh- questions- question tags- punctuation- hyponymylistening and taking notes – study skills – preparing notes TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. 7. 8. Aeda Abidi & Ritu Chowdary, “English For Engineers Made Easy”, Cengage India Learning Limited, New Delhi. 2010 Geetha Nagaraj, “A Course In Grammar and Composition”, Foundation Books Pvt. Ltd., New Delhi, 2006. Hewings. M, “Advanced English Grammar”, Cambridge University Press, Chennai. 2000. Nagini, P S et al, “Excellence Through communication”, Shri Jai Publications, Chennai, 2005. Raman M & Sangeetha Sharma, “Technical Communication”, Oxford University Press, USA 2005. Reddy Devika and Chowdhary S, “Technical English”, Mac Millan, Chennai. 2009 Rizvi, M.A., “Effective Technical Communication”, Tata McGRaw Hill Publishing Company Limited, New Delhi, 2006. Verma. Shivendra K, “Interactive Grammar of Modern English”, Frank Brothers & Company, India, 2000. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 10 questions of 2 marks each – no choice 20 marks Part B: 6 questions from the five units with internal choice, each carrying 10 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 9 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMTX1002 FACULTY OF CHEMICAL ENGINEERING ENGINEERING MATHEMATICS II L T P Credits Total Marks (Common to all branches except BIO Groups) 3 1 0 4 100 UNIT I THEORY OF EQUATIONS 10 hrs. Relation between roots and Co-efficient of equations – Symmetry function of roots – Formation of equations – To increase or decrease the roots of a given equation by a given quantity – Reciprocal equations – Descartes rule of signs – Cardon’s method of solving cubic equations. UNIT II THREE DIMENSIONAL ANALYTICAL GEOMETRY 10 hrs. Direction cosines and ratios – The equation of a plane – Equation to a straight line – Shortest distance between two skew lines –Coplanar lines – Sphere – Tangent line – Plane section of a sphere – Orthogonal spheres. UNIT III INTEGRAL CALCULUS 10 hrs. Double integrals – Change of order of integration – Change of Variables from Cartesian to Polar coordinates – Area - using double integral - Triple integrals - Volume using Triple integrals. UNIT IV BETA AND GAMMA FUNCTIONS 10 hrs. ax n Properties of definite Integrals – Related definite Integrals – Reduction formulae for e , x sinax, xn cos ax, sin x, cosnx and sinm x cosn x. Definitions of Beta and Gamma integrals – Relation between them – Properties – Evaluation of definite integrals in terms of Beta and Gamma function – Simple applications. n UNIT V VECTOR CALCULUS 10 hrs. Differentiation of a vector function – Gradient, divergence and curl – Directional derivative – Identities (without proof) - Irrotational and Solenoidal fields, Vector Integration – Line, Surface and Volume Integrals, Integral theorems (without proof), Green’s theorem (in the plane), Gauss divergence theorem and Stoke’s theorem – Simple applications involving rectangles and cuboids. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. Veerarajan.T, “Engineering Mathematics for First Year”, 2nd Edition , Tata McGrawHill Publications ,2008 Kandaswamy. P & co., “Engineering Mathematics for First Year”, 9th revised Edition, S.Chand & Co Pub., 2010 Arumugam.S & co, “Engineering Mathematics Vol-II”, Revised Edition, SciTech Pub., 2010 Grewal. B.S, “Higher Engineering Mathematics”, 40th Edition, Khanna Publications, 2007 Chandrika Prasad, “Text book on Algebra and theory of equations”, Pothishala Private Ltd., Allahabad, 2009 UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 10 REGULATIONS 2010 SATHYABAMA UNIVERSITY SPHX1002 FACULTY OF CHEMICAL ENGINEERING APPLIED PHYSICS L T P Credits Total Marks (Common for all branches) 3 0 0 3 100 UNIT I FIBER OPTICS 10 hrs. Introduction - Principle and structure of optical fibers-Acceptance angle-Numerical aperture-Types of optical fibers-Preparation of fiber – Double crucible technique-Types of rays-Theory of propagation of light-Energy loss in optical fiber- Attenuation and distortion-Fiber splicing – Fusion and mechanical splicing-Fiber connectors -Butt joint and expanded beam connectors-Optical fiber communication system (block diagram) - Advantages and its applications. UNIT II ACOUSTICS OF BUILDINGS 10 hrs. Introduction – Musical sound & noise-Characteristics of musical sound : pitch, loudness, quality – Weber-Fechner law-Relation between pitch & frequency-Factors on which intensity & loudness depend-Decibel scale-Sound intensity level and sound pressure level-Sound absorption-OWU-Sound absorption coefficient and its measurements – Reverberation - Reverberation time – Standard Reverberation time – Sabine’s formula to determine the Reverberation time (Jaegar method)- Factors affecting the acoustics of a building and the remedies-Principles to be followed in the acoustical design of a good auditorium. UNIT III FUNDAMENTALS OF DIGITAL ELECTRONICS 10 hrs. Number systems - Binary, decimal, Hexadecimal and Octadecimal-Conversion from one number system to another-Binary addition-Subtraction - Subtraction by 1’s & 2’s complement- BCD-ASCII-Excess 3 code and gray code. UNIT IV NANO DEVICES 10 hrs. Definition-Fabrication-Top down approach and bottom up approach-Nanomagnets – Particulate Nanomagnets, Geometrical Nanomagnets-Magneto Resistance – Ordinary Magneto Resistance, Giant Magneto Resistance, Tunneling Magneto Resistance- Probing Nanomagnetic Materials-Nanomagnetism in Technology-Nano Devices – Injection Laser – Quantum Cascade Laser – Optical Memories and Coulomb Blockade Devices UNIT V MEDICAL PHYSICS 10 hrs. Ultrasonics –Introduction- Production of ultrasonic waves - Piezo-electric method-properties-Doppler effect - Blood flow meter – Determination of upward and downward transit time- A- scan, B-scan and M-scan-X-rays – Introduction-Units of X-rays- Diagnostic technologies of X-rays – Radiography-Fluoroscopy-Image intensifier-Nuclear medicine – Introduction-units of radioactivity, 99 m Tc generator, nuclear medicine imaging devices - Gamma camera. TEXT / REFERENCE BOOKS : 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. Mathur.D.S, Heat and Thermodynamics, 5th Edition, Sultan Chand & Sons, 2004. Gerd Keiser, Optical fiber communication, 3 rd Edition, Tata Mc Graw Hill, 2000. John M. Senior, Optical fiber communications - Principle and Practice, 2nd Edition, Pearson Education, 2006. Franz J.H, Jain V.K, Optical communication – Components and Systems,1st Edition, Narosa Publications, 2001. Malvino,Leach & Gautam Saha, Digital Principles and applications, 6th Edition, McGraw Hill, 2006. William H. Gothman, Digital electronics – An int. to theory and practice,2nd Edition, PHL of India, 2007. Roy, Medical Bio Physics, 1st Edition, Saras Publications, 2001. Vasantha Pattabhi, Bio Physics, 1 st Edition, Narosa, 2004. Gaur. R.K. and Gupta. S.L., Engineering Physics, 8 th Edition, Dhanbat Rai Publications,2007. Avadhanulu. M.N. and. Kshirsagar. P.G, Engineering Physics, 2 nd edition, S. Chand & Company, 2007. Dr. Arumugam M., Engineering Physics, 2nd Edition, Anuradha Publications, 2002. William D.Callister, Jr, Materials Science and Engineering An introduction, 6th Edition, John-Wiley and Sons, 2004. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration: 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Out of 20 marks, maximum of 10% problems may be asked Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks Out of 60 marks, maximum of 10% problems may be asked ‘Applications’ mentioned in the syllabus refer to the basic applications and not to any specific case B.Tech. (CHEMICAL ENGINEERING) 11 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCYX1003 FACULTY OF CHEMICAL ENGINEERING CHEMISTRY OF INDUSTRIAL MATERIALS L T P Credits Total Marks (Common to Mech, Mech & Prod, Chem, Civil, Auto and Aero) 3 0 0 3 100 UNIT I FUELS 10 hrs. Introduction - Classification. Calorific values: GCV, NCV. Determination of calorific value by Bomb Calorimeter. Liquid Fuels: Petroleum, Refining of petroleum. Cracking: Fluidized bed catalytic cracking. Knocking in Internal Combustion engines , Cetane number, Octane number, Antiknocking agents: MTBE, ETBE. Gaseous Fuels: Natural gas, CNG. Flue gas analysis using Orsat’s apparatus. Calculation of minimum quantity of air for combustion of fuels (simple problems) UNIT II LUBRICANTS AND ADHESIVES 10 hrs. Lubricants: Introduction. Lubrication mechanism: Hydrodynamic lubrication, Boundary lubrication, Extreme pressure lubrication. Properties of lubricants: Viscosity index (VI), Flash and Fire point, Cloud and Pour point, Aniline point, Oiliness, Sligh oxidation test. Classification of lubricants: Liquid lubricants, Compounding of oil. Semi solid lubricants: Greases, Types of greases. Solid lubricants: Graphite and Molybdenum disulphide (MoS 2). Adhesives: Classification: Natural and synthetic adhesives. Adhesive action. Development of bond strength. Physical and chemical factors influencing adhesive action. UNIT III PHASE RULE 10 hrs. Introduction - Statement, Definition of terms involved with examples. Applications of phase rule to one component system: Water system. Reduced Phase rule: Construction of simple eutectic phase diagram using Thermal analysis, Lead silver system, Iron carbon system: Allotropes of Iron, Micro constituents of Fe-C phase diagram. UNIT IV ALLOYS AND COMPOSITES 10 hrs. Alloys: Definition, Purpose of making alloys, Effect of alloying elements, Ferrous alloys: Stainless Steel. Non Ferrous alloys: Aluminium and Copper alloys. Composites: Definition , Constituents: Matrix Phase and Dispersed phase. Types of Composites: Metal matrix composites (MMC), Ceramic matrix composites (CMC), Polymer matrix composites (PMC), Fiber reinforced plastics (FRP), Cermets. UNIT V INTRODUCTION TO NANOMATERIALS 10 hrs. Introduction - Nanomaterials: definition, Nanoparticles: Synthesis by Chemical reduction method. Nanoporous materials: Synthesis by Sol-gel method. Nanowires: Synthesis by VLS mechanism. Carbon Nanotubes: Singlewalled and multiwalled nanotubes, Mechanical and electrical properties, Applications. Synthesis of Carbon Nanotubes: Electric arc discharge method, Physical Vapour Deposition (PVD), Chemical Vapour Deposition (CVD), Laser Ablation method. TEXT / REFERENCE BOOKS: Jain.P.C and Monica Jain,"Engineering Chemistry", 15th Edition, Dhanpat Rai Publishing Co. (2009) Charles P.Poole Jr, and Frank J Owens, "Introduction to Nanotechnology", John Wiley and Sons (2006). Sheik Mideen.A, "Engineering Chemistry (I & II)", 13th Edition, Shruthi Publishers, (2010) Dara.S.S, "Text Book of Engineering Chemistry", Reprint, S.Chand & Co, (2009) Kuriakose.J.C and Rajaram.J, "Chemistry in Engineering and Technology",. Vol.1 & 2, 5th Rreprint, Tata McGraw Hill Publishing Company (P) Ltd., 2009 6. Puri Br, Sharma Lr, Madhan S Pathania, "Principles of Physical Chemistry", 41 st Edition, Vishal Publishing Co., (2004) 7. Uppal.M.M, "Engineering Chemistry", 6th Ed, Khanna Publ. (2006) 8. Aggrawal.O.P, "Engineering Chemistry", 3 rd Ed, Khanna Publ. (2003) 1. 2. 3. 4. 5. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Part A: 2 Questions from each unit, each carrying 2 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks B.Tech. (CHEMICAL ENGINEERING) 12 Exam Duration : 3 hrs. 20 marks 60 marks REGULATIONS 2010 SATHYABAMA UNIVERSITY SPRX1001 FACULTY OF CHEMICAL ENGINEERING BASIC MECHANICAL AND CIVIL ENGINEERING L T P Credits Total Marks (Common to Mech, Mech & Prod, Auto, Chem, ECE, EEE, E&I, E&C and ETCE) 3 0 0 3 100 BASIC MECHANICAL ENGINEERING UNIT I ENERGY SOURCES AND ENERGY CONVERSION 8 hrs. Alternate sources of energy - solar, wind, wave, tidal and geo-thermal. Boilers: Classification and principles of modern high pressure steam generators -Layout and working principles of hydraulic (hydel), steam, gas turbine, diesel and nuclear power plants. UNIT II INTERNAL COMBUSTION ENGINES 8 hrs. Working principle of petrol and diesel engines - Two stroke and four stroke engines - Ignition systems -single jet carburetor-spark plug-cooling systems- lubrication systems - fuel pump and fuel injector. UNIT III MANUFACTURING PROCESSES 9 hrs. Foundry process and technology: Foundry tools, pattern, moulding process. Metal forming processes: Principles of forging, rolling, drawing and extrusion. Metal joining process: Principles of welding - fundamentals of arc welding, gas welding and gas cutting - brazing and soldering. Metal machining process: Lathe -Specifications - Main components and their functions-Lathe operations. Machining Concept - Drilling, Milling, Turning, Grinding and surface Finishing. BASIC CIVIL ENGINEERING UNIT I BUILDING MATERIALS AND STRUCTURES 8 hrs. Construction materials - Physical and Mechanical properties - stone, brick, cement, concrete, bitumen, insulation materials & steel. Buildings - various components and their functions. Foundation - functions - classification and suitability. Flooring - function - types - cement concrete, tile, marble and granite flooring. Masonry - Stone and Brick masonry and construction details. Roof - Types - Flat & sloped RCC roof. Introduction to seismic resistant structures. UNIT II GENERAL PROPERTIES OF MATERIALS AND BUILDING VALUATION 8 hrs. Stress, strain & modulus of elasticity. Simple maintenance methodologies, Valuation - plinth area method depreciation rate method. Land development process - Set backs, Authorities involved. Basics of interior design and landscaping. Introduction to Orientation of the building & Energy efficient buildings. UNIT III TRANSPORTATION AND SURVEYING 9 hrs. Importance of Transport - Roads - Classification of roads - Traffic signs & signals - Surveying - Classification and principles - Applications of Theodolite and Total Station - Measurements of distances - angle - Computation of areas - Trapezoidal and Simpson’s rule. TEXT / REFERENCE BOOKS 1. 2. 3. 4. 5. 6. 7. 8. 9. Ramamrutham S, "Basic Civil Engineering", Dhanpat Rai Publishing Co. (P) Ltd. 1999 Shanmugam G and Palanichamy M S,"Basic Civil and Mechanical Engineering", Tata Mc Graw Hill Publishing Co., New Delhi, 2009. Ramesh Babu.V, Text book on Basic Civil & Mechanical Engineering ,VRP publication,2009. Helen Shanthi., Ramachandran. S and Premkumar, Basic Civil and Mechanical Engineering, Air Walk Publications, Chennai, 2009. Natarajan K.V., Basic Civil Engineering Palanichamy M S,"Basic Civil and Mechanical Engineering", Tata Mc Graw Hill Publishing Co., New Delhi, 3rd Edition Reprint 2009. Venugopal.K, Basic Mechanical engineering , Anuradha Publications, Kumbakonam Palani Kumar. K,Basic Mechanical engineering , AirWalk Publications, Chennai-4 VenuGopal K. and Prabhu Raja V.,"Basic Civil and Mechanical Engineering", 3rd Edition, Anuradha Publications, 2010. UNIVERSITY EXAM QUESTION PAPER PATTERN Max.Marks: 80 Exam Duration : 3 hrs. Basic Mechanical Part A: 5 questions of 2 marks each - no Choice Part B: 3 questions from each of the three units of internal choice, each carrying 10 marks 10 marks 30 marks Basic Civil Part A: 5 questions of 2 marks each - no Choice Part B: 3 questions from each of the three units of internal choice, each carrying 10 marks. B.Tech. (CHEMICAL ENGINEERING) 13 10 marks 30 marks REGULATIONS 2010 SATHYABAMA UNIVERSITY SEEX1002 FACULTY OF CHEMICAL ENGINEERING BASIC ELECTRICAL AND ELECTRONICS ENGINEERING L (Common to Mech, Mech & Prod, Auto, Aero & Chem) 2 T P 1 0 Credits Total Marks 3 100 BASIC ELECTRICAL ENGINEERING UNIT I D.C.CIRCUITS 11 hrs. Electrical quantities, Ohm’s Law, Resistors - Series and parallel combinations, Kirchoff’s laws, Node and Mesh Analysis - Star delta Transformation UNIT II MAGNETIC CIRCUITS 8 hrs. Definition of MMF, Flux and reluctance - Leakage factor - Reluctances in series and parallel (series and parallel magnetic circuits) - Electromagnetic induction - Fleming’s rule - Lenz’s law - Faraday’s laws - statically and dynamically induced EMF - Self and mutual inductance - Energy stored and energy density - Analogy of electric and magnetic circuits UNIT III A.C.CIRCUITS 11 hrs. Sinusoidal functions - RMS(effective) and Average values- Phasor representation - J operator - sinusoidal excitation applied to purely resistive , inductive and capacitive circuits - RL , RC and RLC series and parallel circuits - power and power factor - Three phase circuits - Star / Mesh connections - with balanced loads - measurement of power by two wattmeter method. TEXT BOOKS: 1. Mittle.B.N, Aravind Mittle, "Basic Electrical Engineering", Tata McGraw Hill", 2nd Edition. Sep 2005 2. Theraja.B.L, "Fundamentals of Electrical Engineering and Electronics", S.Chand & Co., 1st Multicolor Edition, 2006 (Reprint 2009) REFERENCE BOOKS: 1. 2. 3. 4. Smarajit Ghosh, "Fundamentals of Electrical and Electronics Engineering", PHI Learning Private Ltd, 2nd Edition, 2010. Wadhwa.C.L, "Basic Electrical Engineering", New Age International, 4th Edition, 2007. (Reprint June 2010) Abhijit Chakrabarti, Sudipta nath & Chandan Kumar Chanda, "Basic Electrical Engineering", Tata McGraw Hill, 1st Edition, 2009. T. Thyagarajan, “Fundamentals of Electrical Engineering”, SciTech Publications, 5th Edition, Reprint Jan 2010 BASIC ELECTRONICS ENGINEERING UNIT I SEMICONDUCTOR DEVICES AND LOGIC GATES 10 hrs. Discrete devices - PN junction diodes - Zener diodes - Tunnel diodes- Thermistors - Bipolar junction transistors - Field effect transistors (FET and MOSFET) - Uni junction transistors - Silicon controlled rectifiers and Triacs. Universal Gates - Half Adder - Full Adder. UNIT II RECTIFIERS, AMPLIFIERS AND OSCILLATORS 10 hrs. Half and full wave rectifiers- Capacitive and inductive filters- ripple factor- PIV-rectification efficiency. CB, CE and CC Configuration - RC coupled amplifier- positive and negative feedback - Barkhausen criterion for oscillations RC and LC oscillators. TEXT BOOK/REFERENCE BOOKS: 1. Sedha.R.S, A Text book of Applied electronics, 2nd Edition, S.Chand & company, 2005. 2. Dr.Bhattacharya.S.K and Dr.Renu vig, Principles of electronics, 3rd Edition, S.K.Kararia & Sons, 2002. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration: 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks (Distribution may be 70% Theory and 30% Numerical) B.Tech. (CHEMICAL ENGINEERING) 14 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMEX1006 FACULTY OF CHEMICAL ENGINEERING MATERIAL TECHNOLOGY L T P Credits Total Marks (Common to Mech, Mech & Prod, Auto, Aero & Chem) 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Basic Principles: Crystal structures - BCC -FCC -HCP -Methods to determine crystal structure - Atomic radius -APF - Allotropy -Solid solution - Intermetallic compunds Phase diagrams: Solidification of metals, phase rules, construction of phase diagram, Isomorphous, eutectic diagram showing partial solid solubility, peritectic system. Non-equilibrium cooling of above types of alloys Equilibrium solid state reactions. UNIT II FERROUS AND NON-FERROUS ALLOYS 10 hrs. Fe − Fe 3 C diagram, Cooling Curves of pure Fe, Critical points in Fe − Fe 3 C equilibrium diagrams, Phase changes. Simple calculation of amount of phases. Plain carbon steels, Effect of alloying elements on steel, Alloy steel, IS designation of steels - classification of cast iron, Properties and Uses Composition and uses of important aluminium based alloys, copper based alloys and Nickel based alloys. UNIT III HEAT TREATMENT OF STEEL 10 hrs. Non-equilibrium transformation of austenite - Annealing, Normalizing, spheroidizing, TTT diagram. Continuous cooling transformation diagram - Hardening and tempering, martempering, austempering - Hardenability and its determination - Surface hardening processes. Heat treatment of non-ferrous alloys - Age hardening, precipitation hardening UNIT IV POWDER METALLURGY 10 hrs. Introduction, Methods of production of metal powder - mixing - blending - compacting - sintering -hot pressing - secondary and finishing operations - Advantages and applications. UNIT V MECHANICAL PROPERTIES AND TESTING 10 hrs. Elastic and plastic deformation of metals - elastic effects - Deformation by slip Tensile test - Stress - strain curve for mild steel & brittle material, determination of yield, ultimate stresses, and percentage elongation- Impact tests. Ductile -Brittle transition -fatigue and creep Stress cycle for fatigue testing, endurance limit. Fatigue limit, S-N Curve, Creep Curve Fracture: Ideal fracture, brittle fracture, Griffith’s theory -fracture toughness, ductile failure cup and cone. Type of fracture. Fatigue failure, crack propagation. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. Avener, S.H., Introduction to Physical Metallurgy, 2nd Edition, McGraw Hill, NY, 1990 Raghavan, V., Material Science and Engineering. 5th Edition, Prentice Hall. 2005 Khurmi R.S., Sedha, R.S., Material Science, 4th Edition, S. Chand & Co. 2009 Dieter, G.E., Mechanical Metallurgy, 3rd Edition, McGraw Hill, 1986 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration: 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 15 REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING PHYSICS LAB II SPHX4002 L T P Credits Total Marks 0 0 2 1 50 1. Air wedge - Determination of thickness of a thin wire 2. B.H. Curve - Determination of energy loss. 3. Spectrometer- Hollow prism - Determination of refractive index of the given liquid 4. Non uniform bending - Determination of Young’s modulus of the material of the beam by Microscopic method. 5. Copper Voltameter - Determination of electrochemical equivalent of copper. 6. Hall effect -Determination of Hall coefficient. CHEMISTRY LAB II SCYX4002 L T P Credits Total Marks 0 0 2 1 50 1. Estimation of Glycine by Sorenson’s Formal titration method. 2. Determination of Ferric ion by thiocyanate method using Calorimeter. 3. Determination of Chemical oxygen demand in wastewater by dichromate titration method. 4. Estimation of the strength of acid by pH titration. 5. Determination of molecular weight of a polymer by viscosity measurement method. 6. Determination of calorific value of a substance using Bomb calorimeter SPRX4001 MECHANICAL WORKSHOP LAB L T P Credits Total Marks 0 0 4 2 100 CARPENTRY Handling of carpentry tools, A practice in marking, sawing planning and chiseling to size. Making simple joints such as half-lap, dove-tail and mortise and tenon joints. Use of modern materials such as plywood, chip board, novapan, laminated sheet (demonstration only). FITTING Use of fitting tools-practice in marketing, fitting to size and drilling-making of simple mating and profiles such as V, Square, Dove-tail, Half-round joints. WELDING i. Electric Arc Welding a) Study on Edge preparation techniques for Arc welding b) List of Welding Exercises 1. Lap Joint 2. Butt Joint 3. Fillet Joint 4. Tee Joint 5. V Joint 6. Corner Joint ii. Study on gas welding and gas cutting iii. Study on TIG & MIG welding FOUNDRY i. Sand testing - Grain fineness - Permeability test. ii. Study on Pattern Allowances iii. Preparation of green sand moulding 1. Flanges 2. Glands 3. Bush 4. Dumbbell iv. Metal casting technique (Demonstration only) B.Tech. (CHEMICAL ENGINEERING) 16 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMTX1009 FACULTY OF CHEMICAL ENGINEERING ENGINEERING MATHEMATICS III L T P Credits Total Marks (Common to all branches except Bioinformatics) 3 1 0 4 100 UNIT I LAPLACE TRANSFORM 10 hrs. Transforms of simple functions – properties of transforms – Transforms of derivatives and Integrals – Periodic functions – Inverse transforms – Convolution theorems – Initial and final value theorems UNIT II APPLICATIONS OF LAPLACE TRANSFORM 10 hrs. Application of Laplace Transforms for solving : linear ordinary differential equations – simultaneous differential equations – integral equations. UNIT III COMPLEX VARIABLES 10 hrs. Analytic functions – Cauchy – Riemann equations in Cartesian and Polar form – properties of analytic functions – construction of analytic functions – conformal mapping – standard types – bilinear transformations. UNIT IV COMPLEX INTEGRATION 10 hrs. Cauchy’s integral theorem – integral formula – Taylor’s and Laurent’s series (without proof) – Residues – Cauchy’s residue theorem – Contour integration and the circle and semi circular contours. UNIT V THEORY OF SAMPLING AND TEST OF HYPOTHESIS 10 hrs. Test of Hypothesis – Large sample – test of significance – single proportion - difference of proportions – Single mean - difference of means. Small sample – students ‘t’ test – single mean – difference of means – Fisher’s test – difference of variance, Exact sample – Chi square test – goodness of fit – independence of attributes. TEXT / REFERENCE BOOKS: 1. Kandasamy, P., Thilagavathy, K., and Gunavathy, K., “Engineering Mathematics”, Volumes II & III, 4th Revised Edition, S. Chand & Co., New Delhi, 2001. 2. Venkataraman, M.K. “Engineering Mathematics” Volumes III - A & B, 13th Edition National Publishing Company, Chennai, 1998. 3. Veerarajan, T., “Engineering Mathematics”, Tata McGraw Hill Publishing Co., NewDelhi, 1999. 4. Grewal, B.S., “Higher Engineering Mathematics”, 35th Edition, Khanna Publishers, Delhi, 2000. 5. Kreyszig, E., “Advanced Engineering Mathematics”, 8th Edition, John Wiley and Sons (Asia) Pvt. Ltd., Singapore, 2001. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 17 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCSX1014 FACULTY OF CHEMICAL ENGINEERING OBJECT ORIENTED PROGRAMMING L T P Credits Total Marks (Common to EEE, ETCE, ECE, Chem, E&I and E&C) 3 0 0 3 100 UNIT I INTRODUCTION TO FUNDAMENTAL CONCEPTS 10 hrs. Object oriented fundamentals, Structured verses Object oriented development, elements of object oriented programming, fundamentals of OOP – class, object, and abstraction and its importance, encapsulation, polymorphism, benefits of OOP, structure of C++ program. UNIT II CLASSES AND OBJECTS 10 hrs. Working with classes – classes and objects – class specification, class objects, accessing class members, defining member functions, inline functions, accessing member functions within class, data hiding, class member accessibility, empty classes, constructors, parameterized constructors, constructor overloading, copy constructors, new, delete operators, “this” pointer, friend classes and friend functions. UNIT III OVERLOADING 10 hrs. Function overloading, operator overloading, overload able operators, unary operator overloading, operator keyword, limitations of increment/ decrement operators, binary operator overloading, arithmetic operators, function templates, class templates. UNIT IV INHERITANCE 10 hrs. Base class and derived class relationship, derived class declaration, forms of inheritance, inheritance and member accessibility, constructors in derived class, destructors in derived class, multiple inheritance, multi level inheritance, hybrid inheritance, virtual base classes, virtual functions. UNIT V EXCEPTION HANDLING AND FILES 10 hrs. Files and streams, opening and closing of files, file modes, file pointers and manipulation, sequential access to a file, binary file, random access to a file, error handling during file manipulation, exception handling, exception handling model, exception handling constructs, list of exceptions, catching exceptions, handling exceptions. REFERENCE BOOKS: 1. Venu Gopal.K.R, Ravishankar.T, and Raj kumar, “Mastering C++”, Tata McGraw Hill, 1997. 2. Balaguruswamy.E, “Object Oriented Programming with C++”, 2nd Edition, Tata McGraw Hill, 2004. 3. Bjarne Stroustrup, “The C++ programming language”, 3rd Edition, Addison Wesley, 1998. 4. John R Hubbard, “Programming with C++”, Shaums Outline Series, 2nd Edition, McGraw Hill. 5. James Martin & James J.Odell, “Object Oriented methods, A foundation” Prentice Hall, 1997 6. Grady Booch, “Object Oriented Analysis and Design with application”, 2nd Edition, Addision Wesley, 1994 UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 18 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1002 FACULTY OF CHEMICAL ENGINEERING CHEMICAL ENGINEERING THERMODYNAMICS - I L T P Credits Total Marks 3 0 0 3 100 (AII Tables/ Data books/ Graph Sheets must be allowed during the Examination) UNIT I BASIC CONCEPTS 10 hrs. The terminologies of thermodynamics, the variables and quantities of thermodynamics, categorization of systems and processes. Energy classifications, point and path properties, energy in transition, heat and work, reversible and irreversible processes, phase rule. UNIT II LAWS OF THERMODYNAMICS 10 hrs. First law and internal energy, statements of first law for the non flow and flow systems, enthalpy and heat capacity limitations of the first law.Zeorth law of thermodynamics, Statements of the second law of thermodynamics, available and unavailable energies, The entropy function, applications of the second law. Third law of thermodynamics. UNIT III THERMODYNAMIC EQUATIONS OF STATE 10 hrs. The PVT behaviour of fluids, laws of corresponding states and equation of states approaches to the PVT relationships of non ideal gas, problems; compressibility factors, generalized equations of state, property estimation via generalized equation of state. UNIT IV THERMODYNAMIC FORMULATIONS 10 hrs. Measurable quantities, basic energy relations, Maxwell relations, thermodynamic formulations to calculate enthalpy, internal energy and entropy as function of pressure and temperature, other formulations involving Cp and Cv, complex thermodynamic formulations, thermodynamic properties of an ideal gas, entropy change in reversible and irreversible process. UNIT V COMPRESSION OF FLUIDS 10 hrs. Thermodynamic aspects of compression process, classification of compression processes, basic equation for change of state of gases, the work expression for different situations, the effect of clearance volume, multistage compression, convergent divergent flow, Ejectors. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. Smith, J.M., and Van Ness, H.C., “Introduction to Chemical Engineering Thermodynamics”, 6th Edition Mc-Graw-Hill, 2004. Narayanan K.V “A Text Book of Chemical Engineering Thermodynamics” 3rd Edition Prentice Hall of India Pvt. Ltd. 2001. Hougen, O.A., Watson, K.M., and Ragatz, R.A., “Chemical Process Principles Part II, Thermodynamics”, John Wiley 1970. Gopinath Halder, “Introduction to Chemical Engineering Thermodynamics”, 2nd Edition PHI Learning Private Limited, 2009. Rao Y.V.C, Chemical Engineering Thermodynamics, University Press (I) Ltd., Hyderabad, 1997. Kyle, B.G., “Chemical and Process Thermodynamics 2nd Edition.”, Prentice Hall of India Pvt. Ltd., 1990. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 19 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1003 FACULTY OF CHEMICAL ENGINEERING FLUID MECHANICS L T P Credits Total Marks 3 0 0 3 100 (All Tables/Data Books / Graph Sheets must be allowed in the Exam). UNIT I FLUID FLOW PHENOMENA 10 hrs. Nature of fluids: incompressible and compressible, hydrostatic equilibrium, manometers, potential flow, boundary layer, the velocity field, laminar flow, Newtonian and non-Newtonian fluids, Newton’s-law of viscosity, turbulence, Reynolds number and transition from laminar to turbulent flow, Eddy viscosity, flow in boundary layers, laminar and turbulent flow in boundary layers, boundary-layer formation in straight tubes. UNIT II KINEMATICS OF FLUID FLOW 10 hrs. Streamlines and stream tubes, equation of continuity, Bernoulli equation, pump work in Bernoulli equation. Flow of incompressible fluids in conduits and thin layers: friction factor, relationships between skin-friction parameters, average velocity for laminar flow of Newtonian fluids, Hagen-Poiseuille equation, hydraulically smooth pipe, von Karman equation, roughness parameter, friction-factor chart, equivalent diameter, form friction losses in Bernoulli equation, couette flow. UNIT III FLOW PAST IMMERSED BODIES 10 hrs. Drag, drag coefficients, drag coefficients of typical shapes, Ergun equation, terminal settling velocity, free and hindered settlings, Stokes’ law, Newton’s law, criterion for settling regime, fluidization, conditions for fluidization, minimum fluidization velocity. UNIT IV TRANSPORTATION OF FLUIDS AND DIMENSIONAL ANALYSIS 10 hrs. Introduction to: pipe and tubing, joint and fittings, stuffing boxes, mechanical seals, gate valves and globe valves, plug cocks and ball valves, check valves.-Classification and selection of pumps, blowers and compressors. -Pumps: developed head, power requirement, suction lift and cavitation, NPSH, constructional features and working principle of single suction volute centrifugal pump, characteristic curves of a centrifugal pump, Dimensional analysis. UNIT V METERING OF FLUIDS 10 hrs. Constructional features and working principles of: Venturi meter, orifice meter, Rotameter, Pitot tube, Target meter, Vortex-shedding meter, Turbine meter, Magnetic meter.-Application of Bernoulli equation to venturi meter and orifice meter, flow rate calculations from the readings of venture meter, orifice meter and pitot tube. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. McCabe, W.L, Smith J.C and Harriot. P., “Unit Operations in Chemical Engineering”, 7th Edition, Mc-Graw-Hill, 2009. Noel de Nevers, “Fluid Mechanics for Chemical Engineers”, 2nd Edition, McGraw-Hill, 1991. Coulson J.M. and Richardson J.E.., Chemical Engineering, Volume 1, 3rd Edition, Pergamon Press, 2000. Shames, I.H., “Mechanics of Fluids”, 3rd Edition, McGraw-Hill Inc., 1992. White, F.M., “Fluid Mechanics”, 4th Edition, McGraw-Hill Inc., 1999. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 20 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1004 FACULTY OF CHEMICAL ENGINEERING CHEMICAL PROCESS CALCULATIONS L T P Credits Total Marks 3 0 0 3 100 (AII Tables/ Data books/ Graph Sheets must be allowed during the Examination). UNIT I INTRODUCTION 10 hrs. Units and Dimensions, Basic and derived units, use of model units in calculations, Methods of expressing, compositions of mixture and solutions. Gas Calculations: Ideal and real gas laws - Gas constant - calculations of pressure, volume and temperature using ideal gas law. Use of partial pressure and pure component volume in gas calculations, applications of real gas relationship in gas calculation. UNIT II MATERIAL BALANCE 10 hrs. Stoichiometric principles, Application of material balance to unit operations like distillation, evaporation, crystallization, drying etc., - Material balance with chemical reaction - Limiting and excess reactants - recycle - bypass and purging - Unsteady state material balance. UNIT III HUMIDITY AND SATURATION 10 hrs. Calculation of absolute humidity, molal humidity, relative humidity and percentage humidity - Use of humidity in condensation and drying - Humidity chart, dew point. UNIT IV FUELS AND COMBUSTION 10 hrs. Determination of Composition by Orsat analysis of products of combustion of solid, liquid and gaseous fuels Calculation of excess air from orsat technique, problems on sulphur and sulphur containing compounds. UNIT V ENERGY BALANCE 10 hrs. Heat capacity of solids, liquids and gases, mean heat capacity, sensible heat and latent heat, evaluation of enthalpy, Standard heat of reaction, heat of formation, combustion, solution, mixing etc.,calculation of standard heat of reaction - Effect of pressure and temperature on heat of reaction - Energy balance for systems with and without chemical reaction. – Unsteady state energy balances. TEXT / REFERENCE BOOKS: 1. Himmelblau, D.M., “Basic Principles and Calculations in Chemical Engineering”, 6th Edition, Prentice Hall Inc., 2003 (with CD containing programmes and problems). 2. Houghen. O.A., Watson. K.M and Ragatz. R.A, Chemical Process Principles, Part I, John Wiley and Asia Publishing, 1970. 3. Richard M. Felder, Ronald W. Rousseau, “Elementary Principles of Chemical Processes”, 3rd Edition by John Wiley & Sons, Inc. Singapore, 2000 4. Bhatt, B.L., Vora, S.M., “Stoichiometry”, 4th Edition, Tata McGraw-Hill, 2004. 5. Venkataramani, V and Anantharaman, N, Process Calculations, 2 nd Edition, Prentice Hall of India Pvt. Ltd., 2003. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 100% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 21 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMEX1010 FACULTY OF CHEMICAL ENGINEERING STRENGTH OF MATERIALS L T P Credits Total Marks 2 1 0 3 100 UNIT I INTRODUCTION 10 hrs. Stress and strain – Application to uniform and varying, Composite sections – Elastic constants, Stress – Strain diagram for brittle and ductile materials, Definition of creep, fatigue, Thermal stresses UNIT II BENDING MOMENT AND SHEAR FORCE 10 hrs. Types of Beams, Supports and Loads – Concept and significance of shear force and bending moment – Shear force and Bending moment diagram for cantilever, simply supported and overhanging beams. UNIT III BENDING AND SHEAR STRESS DISTRIBUTION, TORSION 10 hrs. Stresses in Beams – Simple bending theory – Composite Beams – Combined bending and Direct stress – Shear stress distribution for Rectangular and I section – Simple Torsion theory – Stresses and deformations in Solid and Hollow circular shafts UNIT IV SLOPE AND DEFLECTION OF BEAMS 10 hrs. Double integration method – Macaulay’s method – Moment area method – Conjugate method for simply supported and cantilever beams, (only point loads & Uniformly distributed loads.) UNIT V THIN CYLINDERS AND SPHERES, THICK CYLINDERS 10 hrs. Stresses and deformation in thin cylinders and spherical shells subjected to internal pressure, Thick cylinders – Hoop and radial stress variation, Lame’s equation, Compound cylinders – Shrink fit TEXT BOOKS: 1. Ramamrutham.R., “Strength of Materials” ,16th Edition, Dhanpat Rai Publishing company, 2007. 2. Bansal.R.K., “Strength of Materials”, 4th Edition, Laxmi Publications, 2007. 3. Vazirani. V.N. & Ratwani, N.M., “Strength of Materials”, 2nd Edition, Vol-I, Khanna Publishers, 1996. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. Punmia.B.C, “Strength of Materials”, 2nd Edition, Laxmi Publications, 1992. Rajput.R.K. “Strength of Materials”, 4th Edition, S.Chand & co, New Delhi, 2002. Khurmi, R.S, “Strength of Materials“, 23rd Edition,S.Chand & Co, 2008 Timoshenko.S.P. and Gere.J.M, “Mechanics of Materials”, 5th Edition,Tata McGraw Hill, 2003. Egor P. Popov, “Introduction of Mechanics of Solids”, 2 nd Edition, Prentice Hall of India, New Delhi, 1996. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 100% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 22 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1005 FACULTY OF CHEMICAL ENGINEERING INORGANIC CHEMICAL TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION - CHLORO ALKALI INDUSTRIES 10 hrs. Introduction - Basic principles of unit operations and unit process to common devices used in manufacturing processes like Reactors, Steam jet ejectors, Pumps, Thickeners, Dryers, Electrostatic precipitators, Condenser, Vacuum evaporator in block diagram - Standard symbols used for such devices, Process flow sheet. manufacturing of soda ash, caustic soda and chlorine - manufacture of bleaching powder, calcium hypochlorite, sodium hypochlorite and sodium chlorite. UNIT II HEAVY CHEMICALS 10 hrs. Manufacture of Sulphur, Hydrochloric Acid and Miscellaneous Inorganic Chemical - Mining and production of Sulphur - Manufacture of Sulphur Trioxide and Sulphuric Acid - Manufacture of Hydrochloric acid - Manufacture of alum, Copper Sulphate, Sodium Dichromate, Hydrogen Peroxide, Aluminium Chloride. UNIT III CEMENT AND GLASS 10 hrs. Manufacture of Cement, Glass & Products Used in Photography: Types and Manufacture of Portland Cement - Manufacture of Glasses and Special glasses. UNIT IV INDUSTRIALS GASES AND PAINTS 10 hrs. Manufacture of Carbon dioxide - Hydrogen - Oxygen - Nitrogen - Acetylene - Water Gas - Producer Gas Production of Natural Gas. Introduction of Paints, Pigments, Emulsions and Varnishes -Manufacture of Paints -Manufacture of White and Coloured Pigments. UNIT V FERTILIZER INDUSTRIES 10 hrs. Nitrogen Industries: Synthesis of Ammonia - Manufacture of Nitric Acid and Urea. Phosphorous Industries: Production and Manufacture of Phosphorous, phosphoric Acid, Super Phosphate and Triple super phosphate. Potassium Industries: Potassium Chloride and Potassium Sulphate TEXT / REFERENCE BOOKS: 1. Dryden’s Outlines of Chemical Technology, 3rd Edition, Affiliated East West Press, New Delhi. 2006 2. Shreve. N, Chemical Process Industries, 8th Edition, McGraw Hill, 2004. 3. Chemical vol. I, II, III & IV, Chemical Engineering Education Development Centre, IIT Madras, 1975-78 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 23 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMEX4007 FACULTY OF CHEMICAL ENGINEERING MECHANICAL ENGINEERING LAB L T P Credits Total Marks 0 0 4 2 100 L T P Credits Total Marks 0 0 4 2 100 1. Valve timing diagram in Diesel engine 2. Port timing diagram in Diesel engine 3. Viscosity Index, Flash and Fire point of Lubricant 4. Volumetric efficiency on two stage reciprocating compressor 5. Test on air conditioning system 6. Performance test on Diesel engine 7. Load test on diesel alternator set 8. Heat balance on diesel engine 9. Mechanical load test on petrol engine 10. Morse test on multi cylinder petrol engine 11. COP in compression refrigeration cycle 12. Study Of Steam Power Plant SCSX4009 OBJECT ORIENTED PROGRAMMING LAB 1. Write C++ program to calculate final velocity using the formula: v = u + a ∗ t, with initial velocity, acceleration and time as input. 2. Write C++ program to find the area of square, rectangle, circle using function overloading concept. 3. Write C++ program to change the sign of an operands using unary operator overloading concept. 4. Write C++ program to add two complex numbers using binary operator overloading concept. 5. Write C++ program to find mean value of two integers using friend function concept. 6. Write C++ program to multiple and divide two different data type using inline function concept. 7. Implement parametrized constructor, default conctructor, copy constructor and destructor 8. Write C++ program to enter the sale value and print the agent’s commission using single inheritance. 9. Write C++ program to enter salary and output income tax and net salary using multiple inheritance concept. 10. Write C++ program to enter the unit reading and output the customer’s telephone bill using hierarchical inheritance. 11. Write C++ program to find the grade of the students based on academic marks and sports using multilevel inheritance. 12. Write a program having student as an abstract class and create many derived classes such as Engineering, Medical etc from student’s class. Create their objects and process them. 13. Write C++ program to count the words and characters in given text using virtual function. 14. Write C++ program to calculate net pay of employee using virtual base class concept. 15. Write C++ program to calculate division of two number with a try block to detect and throw an exception if the condition” divide by-zero” occurs. 16. Write C++ program to merge two files into one single file 17. Write C++ program to swap two values using funtion templates 18. Write C++ program to sort the numbers using class templates B.Tech. (CHEMICAL ENGINEERING) 24 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMTX 1010 FACULTY OF CHEMICAL ENGINEERING ENGINEERING MATHEMATICS IV L T P Credits Total Marks (Common to all branches except Bio Informatics) 3 1 0 4 100 UNIT I PARTIAL DIFFERENTIAL EQUATION 10 hrs. Formulation of equations by elimination of arbitrary constants and arbitrary functions-solutions by equations-general, particular and complete integrals-Lagrange’s linear equation-standard type of first order equation-second and higher order equations with constant coefficients-homogenous equations. UNIT II FOURIER SERIES 10 hrs. Euler’s formula-Dirichlets conditions-convergence statement only-change of interval-odd and even functions-half range series-RMS value-Parseval’s formula-complex form of Fourier series-harmonic analysis. UNIT III WAVE AND HEAT EQUATION 10 hrs. One dimensional wave equation-Transverse vibration of finite elastic string with fixed ends-boundary and initial value problems-Fourier series solution-Derivation of one dimensional heat equation-steady and unsteady state-boundary and initial value problems-Fourier series solutions. Two dimensional heat equation-steady state heat flow in two dimensions-Laplace equation in Cartesian coordinates - Fourier series solution. UNIT IV FOURIER TRANSFORM 10 hrs. The infinite Fourier transform-sine and cosine transform-Properties-Inversion theorem-Finite Fourier transform-sine and cosine transform-Convolution theorem-Parseval’s identity. UNIT V Z – TRANSFORM AND DIFFERENCE EQUATIONS 10 hrs. Z – Transforms – Elementary Properties – Inverse Z – transforms – Convolution theorem – Formation of difference equations – Solution of difference equations using Z – transforms. TEXT / REFERENCE BOOKS: 1. Kandasamy, P., Thilagavathy, K., and Gunavathy, K., “Engineering Mathematics”, Volumes II & III, 4th Revised Edition, S. Chand & Co., New Delhi, 2001. 2. Venkataraman, M.K. “Engineering Mathematics” Volumes III - A & B, 13th Edition National Publishing Company, Chennai. 3. Veerarajan, T., “Engineering Mathematics”, Tata McGraw Hill Publishing Co., New Delhi, 1999. 4. Grewal, B.S., “Higher Engineering Mathematics” 35th Edition, Khanna Publishers, Delhi, 2000. 5. Kreyszig, E., “Advanced Engineering Mathematics” 8th Edition, John Wiley and Sons (Asia) Pvt Ltd., Singapore, 2001. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 25 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1006 FACULTY OF CHEMICAL ENGINEERING PHYSICAL CHEMISTRY L T P Credits Total Marks 3 0 0 3 100 (All Tables / Handbooks / Graph Sheets must be allowed in the Exam) UNIT I PHASE RULE AND SOLUTIONS 10 hrs. Phase rule - Definition of terms - Derivation of phase rule - One component system -Water and Sulphur - Two component systems - Eutectic and compound formation - Simple three component systems Solutions - Solubility and factors affecting solubility of gases in liquids - Henry’s law - Binary solutions - Completely miscible liquids – Raoult’s law- Ideal and Non ideal solutions -Vapour Pressure and Boiling Point diagrams - Partially miscible liquids - Critical Solution Temperature (CST) - Criteria of purity test - Completely immiscible liquids - Steam distillation and its application. Dilute solution and their Colligative properties. Lowering of Vapour pressure of solvent - Elevation of Boiling point - Depression of freezing point - Osmotic pressure - Molecular weight determination using Colligative properties. UNIT II REACTION KINETICS AND CATALYSIS 10 hrs. Introduction to Chemical Reaction Kinetics, Temperature dependence of rate constants - Determination of rate constants for First and Second order reactions. Characteristics and mechanisms of catalyzed reactions - Homogeneous catalysis- Acid base catalysis - Heterogeneous catalysis - Chemisorption-Langmuir and ideal mechanisms.- Promoters and Poisons -Temperature coefficient of catalyzed reactions- Enzyme catalysis - Oxidation - Hydrogenation - Cracking and Acid catalysis in industries. UNIT III ADSORPTION AND COLLOIDS 10 hrs. Physical and Chemical adsorption - Types of Adsorption isotherms(qualitative treatment only) - Surface area of solids, BET method,. Introduction to Colloids (Preparation details not required) Electro Kinetic Phenomena - Donnan membrane equilibrium -Thixotropy and Colloidal Electrolytes. UNIT IV ELECTRICAL CONDUCTANCE 10 hrs. Electrolytes -Types - strong electrolytes and weak electrolytes - Arrhenius theory. Debye - Huckell Onsager theory; Ostwald’s dilution law - solubility of electrolytes and solubility product - common ion effect - acids, bases – definitions- dissociation constant, amphoteric electrolyte - pH - Buffer solutions UNIT V ELECTRODE POTENTIAL 10 hrs. Electrode potential - hydrogen electrode, reference electrodes, electrochemical series, faraday’s laws of electrolysis. Decomposition potential, over voltage, definitions of current density, current concentration, current efficiency, energy consumption, electrical conductance, specific conductance and its determination -equivalent conductance, oxidation -reduction redox couple; e.m.f and energy relations. Conductometry, Potentiometry. TEXT / REFERENCE BOOKS: 1. Puri B.R., Sharma L.R. and Madan S. Pathania, Principles of Physical Chemistry, 38th Edition., Shobhanlal Nagin Chand & Co, Jalandhar, 2000. 2. Gurdeep R. Chatwal and Sham K. Anand, Instrumental Methods of Chemical Analysis, 5th Edition., Himalaya Publishing House, Mumbai, 2002. 3. Samuel H. Maron and Carl F. Prutton, Principles of Physical Chemistry, 4th Edition., Amerind Publishing Co., 1972 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 30% Problems 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 26 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1007 FACULTY OF CHEMICAL ENGINEERING CHEMICAL ENGINEERIING THERMODYNAMICS-II L T P Credits Total Marks 3 1 0 4 100 (All Tables/Data book/Graph Sheets must be allowed in the Exam). UNIT I PROPERTIES OF SOLUTIONS 10 hrs. Partial molar properties, ideal and non-ideal solutions, standard states definition and choice, Gibbs-Duhem equation, excess properties of mixtures. fugacity and fugacity coefficient. UNIT II PHASE EQUILIBRIA 10 hrs. Criteria for equilibrium between phases in multi component non-reacting systems in terms of chemical potential and fugacity, application of phase rule, vapour-liquid equilibrium, phase diagrams for homogeneous systems and for systems with a miscibility gap, effect of temperature and pressure on azeotrope composition, liquid-liquid equilibrium, ternary liquid-liquid equilibrium. UNIT III CORRELATION AND PREDICTION OF PHASE EQUILIBRIA 10 hrs. Activity and Activity coefficient, Excess Gibbs free energy model, thermodynamic consistency of phase equilibria, application of the correlation and prediction of phase equilibria in distillation process, Bubble point and Dew point calculation. UNIT IV CHEMICAL REACTION EQUILIBRIA 10 hrs. Definition of standard state, standard free energy change and reaction equilibrium constant, evaluation of reaction equilibrium constant, prediction of free energy data, equilibria in chemical reactions, calculation of equilibrium compositions for homogeneous chemical reactions, thermodynamic analysis of simultaneous reactions. UNIT V REFRIGERATION 10 hrs. Principles of refrigeration, methods of producing refrigeration, liquefaction process, co-efficient of performance, evaluation of the performance of vapour compression and gas refrigeration cycles. TEXT / REFERENCE BOOKS: 1. Smith, J.M., Van Ness, H.C., and Abbott, M.M., Introduction to Chemical Engineering Thermodynamics, 6th Edition., McGraw Hill International Edition, Singapore 2001 2. Hougen, O.A., Watson, K.M., and Ragatz, R.A., “Chemical Process Principles Part II”, Thermodynamics, John Wiley, 1970. 3. Gopinath Halder, “Introduction to Chemical Engineering Thermodynamics”, 1st Edition, PHI Learning Private Limited, 2009. 4. Sandler, S.I., “Chemical and Engineering Thermodynamics”, 2nd Edition, Wiley, 1989. 5. Kyle, B.G., Chemical and Process Thermodynamics., 2nd Edition., Prentice Hall of India Pvt. Ltd., 1990. 6. Rao Y.V.C, Chemical Engineering Thermodynamics, University Press (I) Ltd., Hyderabad, 1997 7. Narayanan K.V., Chemical Engineering Thermodynamics, 1st Edition, PHI Learning, 2009 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 27 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1008 FACULTY OF CHEMICAL ENGINEERING ORGANIC CHEMICAL TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I PULP, PAPER AND SUGAR 10 hrs. Introduction to Organic Chemical Processes. Manufacture of Chemical, Semi-chemical and NSSC pulp. Manufacture of Newsprint paper and Writing paper. Manufacture of Sugar, Starch and Starch derivatives. UNIT II FERMENTATION, OILS AND FATS 10 hrs. Fermentation processes for the manufacture of ethyl alcohol, citric acid and antibiotics. Refining of Edible oils and Fats. Manufacture of Soaps and Detergents. UNIT III PETROLEUM AND PETRO CHEMICALS 10 hrs. Introduction to petrochemicals - Petroleum refining processes - Cracking, Reforming processes - Processes for the manufacture of petro-products - Ethylene, propylene, xylene, benzene, toluene, butadiene, Synthesis gas Gasification of coal and coal chemicals. UNIT IV PLASTICS, RUBBER AND LEATHER 10 hrs. Raw materials, Classification of polymers, synthetic polymers – Polyethylene, polypropylene, PVC, Polystyrene, ABS, Teflon, formaldehyde and epoxy resins. Rubber - Natural rubber, synthetic rubber, SBR, polybutadiene, Poly isoprene, poly chloroprene, acrylic and silicone rubber, compounding of rubber. Leather tanning and finishing. UNIT V SYNTHETIC FIBRE, DYES AND INTERMEDIATES 10 Hrs. Viscose rayon, cuprammonium and cellulose acetate, nylons, polyesters, acrylics, mono acrylic polypropylene, Dyes and intermediates. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. George T. Austin, Shreve’s Chemical Process Industries, 5th Edition., McGraw-Hill International Editions, Singapore, 1984. Gopala Rao M. and Marshall Sittig, Dryden’s Outlines of Chemical Technology, 3rd Edition., East-West Press, New Delhi, 1997. Kent, J.A. (ed), Riggel’s Hand book of Industrial Chemistry, Van Nostrant Reinhold, 1974. Chemical Vol. I, II, III & IV, Chemical Engineering Education Development Centre, IIT Madras, 1975-78. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 28 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1009 FACULTY OF CHEMICAL ENGINEERING MECHANICAL OPERATIONS L T P Credits Total Marks 3 0 0 3 100 (All Tables / Handbooks / Data Books / Graph Sheets must be allowed in the Exam). UNIT I PARTICLE CHARACTERISTICS AND SIZE ANALYSIS 10 hrs. Particulate solids particle shape, size, mixed particle sizes and size analysis -cumulative and differential analysis - various mean diameters - screen analysis, standard screens - types of screen, BSS, Tyler, ISS - calculations of efficiency of screen -various industrial screen - particle separation not involving fluid mechanics- electrostatic precipitation and magnetic separation, jig -rimed tables, storage of solids - flow of solids - conveying of solids. UNIT II SIZE REDUCTION 10 hrs. Size reduction Principles of Comminution - Energy and Power Requirements in Comminution - Crushing Efficiency - Mechanical Efficiency - Laws of Crushing -Size Reduction Equipments -Crushers -Grinders - Cutting Machines Open and Closed Circuit Operation - Feed Control - Mill Discharge - Energy Consumption -Removal or supply of Heat. UNIT III MECHANICAL SEPARATIONS 10 hrs. Particulate solids flow and hydro mechanical separations: motion of a particle through a fluid - terminal velocity under laminar flow and turbulent flow - free and hindered settling. Classification- separation ratio - Classification equipment - GST - elutriator - cone classifier - cyclone separator - wet scrubber sedimentation; gravity sedimentation -mechanism- continuous sedimentation -thickener -classifier- Kynch theory- settling area -centrifugal sedimentation -centrifuges. Floatation: equipment -modifiers -collectors -frothing agents. Electro floatation UNIT IV FILTRATION 10 hrs. Filtration Equipment - Sand Filters - Filter presses - Leaf Filter - Rotary continuous Filters - Filter Media - Filter Aids - Principles of Cake Filtration -pressure drop through Filter Cake - Compressible and Incompressible Filter Cakes - Specific Cake resistance - Filter Medium Resistance Constant pressure Filtration - Continuous Filtration - Constant Rate Filtration - Clarifying filters - Liquid clarification - Gas cleaning - Principles of clarification - cross flow filtration. UNIT V AGITATION AND MIXING 10 hrs. Agitation and Mixing of Liquids - Principles of Agitation - Agitation Equipment - Impellers - Flow Pattern in Agitated Vessel - Power Consumption in Agitated Vessel, Flow number - Power Correlation - Calculation of Power Consumption in Newtonian and Non Newtonian Liquids, Blending and Mixing - Jet Mixers -Motionless Mixers. Mixing of Solids: Mixtures of Cohesive Solids - Power requirements Criteria for mixer effectiveness. Mixers for free flowing granular solids - Rate of Mixing. TEXT / REFERENCE BOOKS: 1. Warren L. Mccabe, Julian C. Smith and peter Harriott, Unit Operations of Chemical Engineering, 7 th Edition., McGraw Hill International Edition, New York 2009 2. Badger and Banchero, Introduction to Chemical Engineering, 2nd Edition McGraw Hill, 2001. 3. Coulson J.M., Richardson J.F., Backhurst J.R. and Harker J.M., Coulson & Richardson’s Chemical Engineering, Vol. II, 5 th Edition., Butter worth Heinemann, Oxford, 2002 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 29 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1010 FACULTY OF CHEMICAL ENGINEERING INSTRUMENTAL METHODS OF ANALYSIS L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION TO SPECTROSCOPICAL METHODS OF ANALYSIS 10 hrs. Electromagnetic Radiation: Various ranges, Dual Properties, Various energy levels, Interaction of photons with matter, absorbance, & transmittance and their relationship, Permitted energy levels for the electrons of an atom and simple molecules, Classification of instrumental methods based on physical properties. Quantitative Spectroscopy: Beer-Lambert’s law, Limitations, Deviations (Real, Chemical Instrumental). Nephelometry, Duboscq colorimetry, Estimation of inorganic ions such as Fe, Ni using Beer-Lambert’s Law. UNIT II MOLECULAR SPECTROSCOPY 10 hrs. Various electronic transitions in organic and inorganic compounds effected by UV, Visible and infra red radiations, Various energy level diagrams of saturated, unsaturated and carbonyl compounds, excitation by UV and Visible radiations, Woodward-Fischer rules for the calculation of absorption maxima (dienes and carbonyl compounds) Effects of auxochromes and effects of conjugation on the absorption maxima, Instrumentation for UV, Visible and IR spectroscopies (source, Optical parts and Detectors), Multi component analysis, Photometric titration (Experimental set-up and various types of titrations), Applications of UV, Visible and IR spectroscopy. UNIT III ATOMIC SPECTROSCOPY 10 hrs. Atomic Absorption Spectrophotometry: Principle, Instrumentation and Applications, Various interferences observed in AAS. polarimetry and refractrometry, Principle, instrumentation and Applications. UNIT IV ELECTROMETRIC METHODS OF ANALYSIS 10 hrs. Introduction of electrometric methods, difference between redox and acid- base reactions, types of cells, schematic representation of cell, single electrode potential, laboratory reference electrodes (Standard hydrogen, saturated calomel, Ag -AgCl and inert electrodes), ion-selective electrodes. Potentiometry: Nernst equation, experimental set-up and measurement of pH; Conductometry- Measurement of conductance, experimental set-up and various conductometric titrations. UNIT V CHROMATOGRAPHIC METHODS 10 hrs. Basic principles of chromatography, Classification of chromatographic methods, Column, Thin layer, Paper, Gas, High Performance Liquid Chromatography (Principle, mode of separation and Technique).Separation of organic compounds by column and Thin layer, mixture of Cu, Co and Ni by Paper, separation of amino acids by paper, estimation of organic compounds by GC and, HPLC. TEXT / REFERENCE BOOKS: 1. Willard H.H., Merritt I.I., Dean J.A., and Settle, F.A., Instrumental Methods of Analysis, 6th Edition, CBS Publishers, 1986. 2. Skoog D.A and Weswt D.M.M., Fundamentals of Analytical Chemistry, 8th Edition Saunders-College Publishing, 2004. 3. Gurdeep R. Chatwal and Sham K. Anand, Instrumental Methods of Chemical Analysis, 5th Edition., Himalaya Publishing House, Mumbai, 2002. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 30 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX4001 FACULTY OF CHEMICAL ENGINEERING PHYSICAL CHEMISTRY & CHEMICAL TECHNOLOGY LAB L T P Credits Total Marks 0 0 4 2 100 1. Determination of Eutectic temperature and composition of a simple Eutectic system. 2. Determination of critical solution temperature of phenol-water system. 3. Determination of molecular weight by Rast’s method. 4. Determination of partition coefficient of Iodine between two immiscible solvents. 5. Determination of cell constant & to verify Ostwald’s dilution law. 6. Determination of Hardness of water for the given sample. 7. Determination of available chlorine in bleaching powder. 8. Determination of Saponification value of oil. 9. Determination of TFM & Alkalinity of given soap. 10. Determination of MnO 2 in the given ore. SCHX4002 FLUID MECHANICS LAB 1. Flow through Venturimeter 2. Flow through Orifice meter 3. Flow through Pitot tube 4. Characteristics of a Reciprocating pump 5. Characteristics of a Centrifugal pump 6. Characteristics of a Jet pump 7. Characteristics of a Gear pump 8. Pipe friction calculation 9. Flow through packed bed 10. Flow through Fluidization 11. Flow through helical coil 12. Flow through annular pipe/ non circular conduits 13. Flow through Weirs and Notches B.Tech. (CHEMICAL ENGINEERING) 31 L T P Credits Total Marks 0 0 4 2 100 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMTX1011 FACULTY OF CHEMICAL ENGINEERING APPLIED NUMERICAL METHODS L T P Credits Total Marks (Common to Mech, M & P, Aero, Auto, Civil, Chem, E&I, ECE, EEE, E&C and ETCE) 3 1 0 4 100 UNIT I CURVE FITTING AND RELATION BETWEEN OPERATORS 10 hrs. Curve Fitting-Method of group averages-Principle of least squares-Method of moments-Finite Differences-Operators E & D-Relationship between operators. UNIT II INTERPOLATION 10 hrs. Interpolation-Newton’s method-Lagrange’s method-Numerical Differentiation and Integration-Trapezoidal and Simpson’s Rule-Finite Difference Equations. UNIT III ALGEBRAIC AND TRANSCENDENTAL EQUATIONS 10 hrs. Numerical solution of Algebraic and Transcendental Equations-Regula Falsi method-Newton Raphson method-Graffe’s Root Squaring method-Simultaneous linear algebraic equations- Gauss Jordan method-Crout’s method-Gauss Seidel method-Relaxation method. UNIT IV ORDINARY DIFFERENTIAL EQUATIONS 10 hrs. Numerical solution of Ordinary Differential Equations-Taylor’s series-Modified Euler’s method-Runge Kutta method of fourth order-Predictor-Corrector methods-Milne’s method-Adam’s Bashforth method. UNIT V PARTIAL DIFFERENTIAL EQUATIONS 10 hrs. Numerical solution to Partial Differential Equations-Classification-Elliptic equations-Poisson’s equations-Leibmann’s iteration procedure-Parabolic equation-Bender Schmidt Scheme-Crank Nicholson’s Scheme-Hyperbolic equations. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. 5. Kandasamy P & Co., Numerical Methods, S.Chand & Co., New Delhi, 2003. Venkataraman M.K., Engineering Mathematics – First Year, 2nd Edition, National Publishing Co., 2000. Grewal, B.S., “Higher Engineering Mathematics”, 35th Edition, Khanna Publishers, Delhi, 2000. Balgurusamy .E, Numerical Methods, Tata McGraw Hill, New Delhi, 2006. Steven C.Chapra, Raymond P. Canale, Numerical Methods for Engineers, Tata McGraw Hill, New Delhi, 2003. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 32 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1025 FACULTY OF CHEMICAL ENGINEERING MASS TRANSFER – I L T P Credits Total Marks 3 0 0 3 100 UNIT I DIFFUSION 10 hrs. Molecular and Eddy diffusion in gases and liquids – Measurement and calculation of diffusivity – Diffusion in Multicomponent gaseous mixtures – Diffusion in solids and its applications – Steady state diffusion under stagnant and laminar flow conditions. UNIT II MASS TRANSFER CO-EFFICIENT AND OPERATIONS 10 hrs. Concept of mass transfer co-efficient – Mass transfer under laminar and turbulent flow past the solids – Boundary layers- Correlation of mass transfer co-efficient – Analogies between momentum, heat and mass transfer – Theories of mass transfer and their application – Interphase and overall mass transfer co-efficient in binary systems. - jd factor. Material balances on batch, co-current and counter-current staged operations, Equipments for gas liquid operations. UNIT III HUMIDIFICATION 10 hrs. Basic concepts – construction of psychometric charts – Methods of humidification and dehumidification operations: Design calculation – Cooling towers principle and operation, equipments. UNIT IV DRYING 10 hrs. Theory and mechanism of drying - Drying characteristics – Design and performance of Batch and Continuous Dryers - Estimation of Drying rates – Drying equipments. UNIT V CRYSTALLIZATION 10 hrs. Theory of Crystallization - Factors governing nucleation and crystal growth - Growth coefficient, Classification of Crystallization and Applications – Batch and Continuous Industrial Crystallizer- equipments. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Treybal, R.E, Mass Transfer Operations, 3rd Edition, McGraw Hill, 2004. McCabe and Smith, Unit Operations of Chemical Engineering, 7th Edition, McGraw Hill, 2009 Coulson J.M. and Richardson J.F., Chemical Engineering, Vol – II, 6th Edition, Pergamon Press, 2002. Sherwood T.K., Pigford R.L. and Wilke C.R., Mass Transfer, 2nd Edition, McGraw Hill, 1960. UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 33 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1026 FACULTY OF CHEMICAL ENGINEERING CHEMICAL REACTION ENGINEERING-I L T P Credits Total Marks 3 0 0 3 100 UNIT I BASICS OF REACTOR DESIGN 10 hrs. Definition of reaction rate, different ways of expressing reaction rate, Molecularity and order of reaction, elementary and non elementary reactions, single and multiple reactions. Temperature dependency of reaction rate, Arrhenius theory, Collision theory, Transition state theory. Mechanism of chemical reactions. Concentration dependent term of rate equation. Interpretation of batch reactor data. Constant and variable volume reactions. Conversion from total pressure data. Methods of determining the order of a reaction, Integral and Differential methods, methods of isolation, initial rates, excess. Autocatalytic reactions, Runaway reactions. UNIT II REACTOR DESIGN FOR SINGLE REACTIONS 10 hrs. Design equation for batch reactor. Flow reactors – Concept of Space time, Space velocity. Material balance and design equation for PFR and CSTR. Semi-batch reactors. Size comparison of reactors for single reactions. Recycle reactors. UNIT III DESIGN OF MULTIPLE REACTORS FOR SINGLE REACTIONS 10 hrs. Charts comparing the sizes of single PFR and CSTR’s for various orders of reaction - calculating conversion from these charts. Multiple reactor systems for single reaction – PFR’s in series and parallel; CSTR’s in series and parallel. Material balance and design equations for multiple reactions. Graphical method for finding number of CSTR’s. Charts for comparison of sizes of multiple CSTR’s and PFR and calculating conversions. UNIT IV DESIGN OF SINGLE AND MULTIPLE REACTORS FOR MULTIPLE REACTIONS 10 hrs. Multiple reactions – Series, Parallel and Series-Parallel. Qualitative and Quantitative treatment of series and parallel reactions. Definitions of Instantaneous and Overall fractional yields and selectivity. Design of single multiple reactors for multiple reactions. UNIT V NON-ISOTHERMAL REACTOR DESIGN 10 hrs. Isothermal and Non isothermal reactor systems. Single reactions – Irreversible and reversible reaction, Temperature and Pressure effects – Information from thermodynamics. Equilibrium flow reactor design, adiabatic temperature and equilibrium conversion, optimum temperature progression. TEXT/REFERENCE BOOKS: 1. Octave Levenspiel, Chemical Reaction Engineering, 3rd Edition, McGraw Hill, 1998 2. Scott Fogler, Chemical Reaction Engineering, 4 th Edition, McGraw Hill, 2005 3. Smith J.M., Chemical Kinetics and Reactor Design, 2nd Edition, McGraw Hill, 2004 UNIVERISTY EXAM QUESTION PAPER PATTERN Max.Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 34 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1027 FACULTY OF CHEMICAL ENGINEERING CHEMICAL PLANT UTILITIES L T P Credits Total Marks 3 0 0 3 100 UNIT I WATER 10 hrs. Water Resources, Treatment and Cooling, Environmental protection, water quality, water supply and regulations. Storage and Distribution of Water. Reuse and Conservation of Water. UNIT II COMPRESSORS AND VACUUM PUMPS 10 hrs. Performance Characteristics of Compressors and Vacuum Pumps. Boosters, Air Receivers. Piping Systems -Air Leaks -Lubrication -Oil Removal UNIT III REFRIGERATION 10 hrs. Refrigeration Systems and their Characteristics, Evaporative refrigeration, Vapour refrigeration system, steam jet refrigeration, thermoelectric cooling, simple vapour compression refrigeration system- production of cryogenic temperatures UNIT IV AIR CONDITIONING AND VENTILATION 10 hrs. Classification factors affecting air conditioning systems, comfort air – conditioning system, characteristics of Air water systems- Transport air conditioning, evaporative condensers, cooling towers, heat pumps, Humidification and Dehumidification Equipments – Air Blowing – Exhaust Ventilation UNIT V STEAM 10 hrs. Steam generation in Chemical Process Plants -Properties of Steam -Boilers and Power Generation Equipments -Steam Engines and Turbines -Steam Handling and Distribution –Steam traps and Steam Economy. Electric Power Distribution in Process Plants -Heat Transfer media. TEXT/REFERENCE BOOKS: 1. Cramer and Watkins (EDS), Chemical Engineering Practice, Vol. 10, Butterworths, London, 1960. 2. Bhasin, S.D. Project Engineering of Process Plants, Chemical Engineering, Ecu Dev. Centre IIT, Madras, 1979. UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 35 REGULATIONS 2010 SATHYABAMA UNIVERSITY FACULTY OF CHEMICAL ENGINEERING HEAT TRANSFER SCHX1028 L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION TO BASIC HEAT TRANSFER 10 hrs. Basic Considerations: Importance of heat transfer in Chemical Engineering operations. Modes of heat transfer. Mean temperature difference. Conduction: Concept of heat conduction. Fourier’s law of heat conduction. One-dimensional steady state heat conduction equation for flat plate, hollow cylinder and hollow sphere. Heat conduction through a series of resistances. Analogy between flow of heat and flow of electricity. Thermal conductivity. Conduction through liquids. UNIT II CONDUCTION AND CONVECTION 10 hrs. Film Coefficients and their applications: Individual and overall heat transfer coefficients and relationship between them. Conduction through extended surfaces. Two dimensional steady state conduction. Analytical and graphical methods. Transient heat conduction. Convection: Concept of heat transfer by convection. Natural and forced convection. Applications of dimensional analysis for convection. Derivation of equations for forced convection under laminar, transition and turbulent conditions. Equations for natural convections. Heat transfer from condensing vapors. Heat transfer to boiling liquids. Influence of boundary layer on heat transfer. Heat transfer to molten metals. Heat transfer in packed and fluidized beds. UNIT III HEAT EXCHANGERS 10 hrs. Parallel and counter flow heat exchangers. Log mean temperature difference. Single pass and multi pass heat exchangers. Plate heat exchangers. Use of correction factor charts. Heat exchanger effectiveness and its use. Number of transfer units charts for different configurations. Fouling factor and Wilson’s plot. Various types of heat exchangers. Heat exchanger design. Design of condensers. Effect of non-condensable. UNIT IV RADIATION 10 hrs. Concept of thermal radiation. Concept of black and gray bodies. Stefan-Boltzmann law. Kirchoff’s law. Radiation between surfaces. Radiation from gases. Clouds of particles and luminous flames. Radiation error in temperature measurement. UNIT V EVAPORATION 10 hrs. Introduction. Types of evaporators. Single and multiple effect evaporation. Capacity and economy of multi effect evaporators. Thermo compression evaporators. Effect of liquid head and boiling point elevation. Duhring’s rule. Liquid characteristics. Material and energy balance in evaporators. Illustrated examples. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. 5. M.L. McCabe and J.C. Smith, Unit Operations in Chemical Engineering, 7th Edition, McGraw Hill, 2009 Donald Q. Kern, Processes Heat Transfer, 4th Edition, Tata McGraw Hill, 1997. McAdams W.H., Heat Transmission, 2nd Edition, McGraw Hill, 1954. Holman J.P., Heat Transfer, 6th Edition, McGraw Hill and Kogakusha, 1997. Necati Ozisik M., Basic Heat Transfer, 2th Edition, McGraw Hill and Kogakusha, 1977. UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 36 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1029 FACULTY OF CHEMICAL ENGINEERING PROCESS EQUIPMENT DESIGN AND DRAWING-I L T P Credits Total Marks 3 0 0 3 100 All Tables/Chemical Engineers’ Handbook/Data Books/Graph Sheets are permitted during the Examination. UNIT I FASTENERS 10 hrs. Design and drawing considerations of bolt, nut and screws, welded and riveted joints, flanged joints, nozzles and reinforcements. Pipe fittings. UNIT II FLOW METERS AND SUPPORTS 10 hrs. Fundamental principles, equations, general design and drawing considerations of flow meters, and vessel supports such as bracket, saddle, skirt, etc. UNIT III PRESSURE VESSELS 10 hrs. Fundamental principles, equations, general design and drawing considerations of vessels subjected to internal pressure, vessel subjected to external pressure. High pressure vessels. Storage tanks. UNIT IV UNIT OPERATION EQUIPMENTS 10 hrs. Fundamental principles, equations, general design and drawing considerations of cyclones, centrifuges, thickeners and filtration equipments. UNIT V MIXING EQUIPMENTS 10 hrs. Fundamental principles, equations, general design and drawing considerations of agitated vessel, jacketed and coil-heated vessels. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. 7. Perry R.H. , “Chemical Engineers’ Handbook”, 8th Edition, McGraw Hill, 2008. McCabe W.L., Smith J.C. and Harriet, “Unit Operation of Chemical Engineering”, 7th Edition, McGraw Hill. 2009 Robert Treybal, “Mass Transfer Operations”, 3rd Edition, McGraw Hill, 2004. Coulson J.M. and Richardson J., “Chemical Engineering”, Vol. 6, Asian Books Printers Ltd. R.S. Khurmi, “Machine design”. 2002 Joshi M.V. and Mahajan V.V., “Process Equipment Design”, 5 th Edition, MacMillan India Ltd, 2005. Dawande S.D., “Process Design of Equipments”, 2nd Edition, Central Techno Publications, Nagpur, 2000. Indian Standard Specifications IS-803, 1962; IS-4072, 1967; IS-2825, 1969. Indian Standards Institution, New Delhi. UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 37 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1030 FACULTY OF CHEMICAL ENGINEERING INSTRUMENTATION AND PROCESS CONTROL L T P Credits Total Marks 3 0 0 3 100 UNIT I INSTRUMENTATION 10 hrs. Temperature measurement: Thermocouples, resistance thermometers, optical and radiation pyrometers. Pressure measurement: Use of manometers, Bourdon gauge, bellows type gauge. Flow measurement: Variable area meters. Positive displacement type meters. Liquid level easurement: direct and differential method, measurement in open and pressure vessels. Measurement of viscosity, conductivity, humidity and pH. UNIT II BASIC CONCEPTS OF PROCESS CONTROL 10 hrs. Response of first order systems Examples of first order systems Process Dynamics of linear open systems Second order and first order systems in series Higher order systems Transfer Function Step, Ramp, Pulse and Sinusoidal inputs, Linearization UNIT III LINEAR CLOSED LOOP SYSTEMS 10 hrs. Development of a block diagram, Controllers and Final control element Closed loop control systems. Block Diagram for feed back control systems, Servo and Regulator problems. Principles of Pneumatic and Electronic controllers Transportation Lag Transient response of closed loop control systems Control valve PI, P, PID control. UNIT IV STABILITY ANALYSIS 10 hrs. Stability, Stability criterion Routh test for stability. Theorems of Routh test root locus Root locus diagram Frequency response Substitution rule Bode diagrams Bode stability criterion Gain and Phase margins Ziegler Nichols control settings Transient response Nyquist diagram. UNIT V CONTROL VALVES, DYNAMICS AND MICROPROCESSOR 10 hrs. Control valves, Valve sizing Characteristics Control valve construction Valve positioning Power unit Transducers Electric to Pneumatic and pneumatic to electric types Transfer function matrix Dead time compensation Step testing Frequency testing Pulse testing. Dynamics and control of chemical reactors Heat exchangers and Distillation columns Analog and digital computer applications Microprocessors and computer control of chemical processes. Introduction to advanced control systems TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Coughanowr D.R. and Koppel L.M., Process Systems Analysis and Control, 2nd Edition, McGraw Hill, New York, 1991. Harriot P., Process Control, 3rd Edition, Tata McGraw Hill, New Delhi, 2008. Eckman D.P., Industrial Instrumentation, 2 nd Edition, Wiley Eastern Ltd, 1996. George Stephanopolus, Chemical Process Control, 2nd Edition, Prentice Hall of India Pvt. Ltd., 1990 UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 50% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 38 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX4004 1. 2. 3. 4. 5. 6. 7. 8. FACULTY OF CHEMICAL ENGINEERING MECHANICAL OPERATIONS LAB L T P Credits Total Marks 0 0 4 2 100 Particle size distribution - differential and cumulative analysis by manual method using standard screens Determination of Screen Effectiveness by Mechanical Method using Standard screens Energy requirement and crushing constants determination using: Jaw Crusher Ball mill Drop weight crusher Determination of filtration constants at constant pressure conditions using: Plate and Frame Press Vacuum Leaf Filter Minimum thickener area calculations performing Batch Sedimentation test Calculation of Angle of nip – Roll Crusher Calculation of Critical Speed of impeller – Agitated Vessels Minimum particle size determination for treating dust laden air – Cyclone Separator SCHX4005 PROCESS DYNAMICS AND CONTROL LAB 1. ON-OFF control of thermal process 2. Simulation of Proportional Controller 3. Flow control loop and Flow Transmitter 4. Level Control loop and Level Transmitter 5. Pressure control loop and Pressure Transmitter 6. Control valve characteristics 7. Verifying the inherent characteristics of control valve 8. Flow co-efficient of control valve 9. Range ability of control valve L T P Credits Total Marks 0 0 4 2 100 10. Verifying the response of Non-Interacting level system 11. Verifying the response of Interacting level system 12. Effect of PI controller on flow control system 13. The effect of a P controller on level process for set point and load changes 14. Effect of P, PI, PID Controller on Pressure Control Loop 15. Optimum Controller Setting using Ziegler Nichols Method 16. Optimum Controller Tuning on Level Process Station B.Tech. (CHEMICAL ENGINEERING) 39 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMEX1017 FACULTY OF CHEMICAL ENGINEERING RESOURCE MANAGEMENT TECHNIQUES L T P Credits Total Marks (Common to all branches) 3 0 0 3 100 UNIT I INTRODUCTION AND LINEAR PROGRAMMING 10 hrs. Operations Research(OR)-Nature-Characteristics-Phases.-Role of OR in Decision making- Outline of OR Models Linear Programming – Formulation of L.P.problems –Solution by graphical method, simplex method, and big M methods – Applications of O.R. in production management UNIT II TRANSPORTATION AND ASSIGNMENT MODEL 10 hrs. Transportation problem – Initial feasible solution- Northwest corner method, Least Cost method, Vogel’s approximation method – Test for optimality-MODI method Assignment problems- Hungarian assignment models- Travelling salesman problems UNIT III RESOURCE SCHEDULING AND NETWORK ANALYSIS 10 hrs. Problem of Sequencing – Problem with N jobs and 2 machines, 3 jobs and M machines. Project Management – Basic concepts – Case studies – Network construction and scheduling, Program evaluation and resource leveling by network techniques, time – Cost trade off. UNIT IV INVENTORY CONTROL AND SIMULATION 10 hrs. Inventory Control – Various Types of inventory models – deterministic inventory models – Production model, Purchase model– with and without shortage- EOQ – Buffer stock – Shortage quantity, Probabilistic inventory models – Quantity Discount and Price Breaks Simulation – Use, advantages & limitations, Monte –Carlo simulation, application to queuing, inventory & other problems UNIT V QUEUEING THEORY, GAME THEORY AND REPLACEMENT MODELS 10 hrs. Queuing theory – Poisson arrivals and exponential service times, Single channel models only. Game theory-Pay off matrix, competitive games with pure strategy, minimax criterion, principles of dominance &mixed strategies Replacement policy for items whose maintenance cost increases with time- Consideration of money value- Replacement policy- Individual, Group replacement of items that fail completely TEXT/REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. 7. Kanti Swarup, P.K.Gupta, & Manmohan., Operations Research – S. Chand & Sons. Mital K.V. and Mohan C.,” Optimization Methods in O.R and System Analysis”, New Age International Publishers. Sharma S.D., ”Operations Research”, Kedarnath Ramnath& Co, 2002. Hamdy A. Taha,” Operations Research”, 5th Edition., PHI, 1995 Hiller & Liberman, ”Introduction to Operation Research”, 5th Edition., McGraw Hill, 2001. Ravindran,Phillips & Solberg, “Operations Research: Principles and Practice”, 2nd Edition., Wiley India Lts, 200 Kanti Swarup Gopta. P. Kand manoharan, "Operations Research 11th Edition S.chand Sans, New Delhi" UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 40 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1031 FACULTY OF CHEMICAL ENGINEERING MASS TRANSFER – II L T P Credits Total Marks 3 1 0 4 100 UNIT I DISTILLATION 10 hrs. Vapor liquid equilibria, Raoult’s law and deviations from ideality, Methods of distillation Batch, Continuous, Flash, steam, vacuum. McCabe Thiele method Ponchon Savarit method, Azeotropic, Extractive and Molecular distillation. UNIT II ABSORPTION 10 hrs. Equilibrium and operating line concept in absorption calculations, Calculation of NTU, HTU, Number of stages, Packed and plate type absorbers. Absorption with chemical reaction, HETP Operating characteristics of stage wise and differential contactors. UNIT III LIQUID – LIQUID EXTRACTION AND LEACHING 10 hrs. Equilibrium in ternary systems, Stage wise contact equipments, Calculations for batch and continuous extractors Calculation of number of stages, Equipments. Solid Liquid equilibrium Equipments - Batch and Continuous types, Calculation of number of stages. UNIT IV ADSORPTION 10 hrs. Types of adsorption Nature of adsorption, Theories of adsorption, Adsorption isotherms, Operation of adsorption columns, Batch and continuous operations, Equipments. UNIT V MISCELLANEOUS SEPARATION PROCESSES 10 hrs. Solid and liquid membranes, Concept of Osmosis, reverse osmosis, Dialysis, Foam Separation, Thermal and Sweep diffusion process, Ion Exchange, Zone Refining. TEXT/REFERENCE BOOKS: 1. Treybal, R.E, Mass Transfer Operations, 3rd Edition, McGraw Hill, 2004 2. McCabe and Smith, Unit Operations of Chemical Engineering, 7th Edition, McGraw Hill, 2009 3. Coulson J.M. and Richardson J.F., Chemical Engineering, Vol. II, Pergamon Press. 2002 UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 70% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 41 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1032 FACULTY OF CHEMICAL ENGINEERING CHEMICAL REACTION ENGINEERING – II L T P Credits Total Marks 3 1 0 4 100 UNIT I NON - IDEAL REACTOR DESIGN 10 hrs. Non ideal reactors, residence time distribution studies, stimulus response techniques, Pulse and step input, other types of inputs, definition of C, E and F curves and relationship between the curves. Developing RTD equation for CSTR, PFR, CSTR. Macromixing and Micromixing data. Zero parameter model – complete segregation model. One parameter model. Tanks in series and dispersion modes. Equations for no. of tanks in series and conversion using these two models (for first order reactions). Definition of vessel dispersion number and Peclet number. UNIT II NON-CATALYTIC REACTIONS 10 hrs. Heterogeneous non-catalytic fluid particle reactions. External diffusion effects on heterogeneous reactions, definitions of reactions rates for heterogeneous reactions. Incorporating the mass transfer term – steps in series. Overall resistance – combining resistances for steps in series and linear reaction. Steady state assumption for steps in series. Models for heterogeneous non catalytic fluid (GAS) – solid reactions – Progressive conversion model, unreacted or shrinking core model. Steps in the unreacted core model. Diffusion and reaction steps. Diffusion through gas film and ash layer: Chemical reaction as the controlling steps – Development of equations for rate controlling steps. UNIT III CATALYSIS AND CATALYTIC REACTIONS 10 hrs. Introduction to catalysis, general properties of homogeneous, steps in a catalytic reaction, adsorption, surface reaction and description as rate limiting steps, physisorption and chemisorption, adsorption isotherm, unimolecular and bimolecular surface reactions, applications of adsorption, B.E.T. theory of multilayer adsorption, synthesizing a rate law mechanism and rate limiting step, preparation and evaluation of industrial catalysts. UNIT IV DESIGN OF HETEROGENEOUS CATALYTIC REACTORS 10 hrs. Rate equation for heterogeneous catalytic system, film resistance, surface reaction and pore diffusion as the controlling steps, internal effectiveness factor of a porous catalyst pellet, overall effectiveness factor, mass transfer and reaction in a packed bed, experimental methods for finding rates – design and comparison of experimental heterogeneous reactors. UNIT V CATALYST DEACTIVATION 10 hrs. Catalytic poisoning, mechanism of catalyst deactivation, the rate equation, regeneration of catalyst. Multiphase reactors – slurry, fluidized and packed bed and some important examples of industrial reactors. TEXT/REFERENCE BOOKS: 1. Octave Levenspiel, Chemical Reaction Engineering, 3rd Edition, McGraw Hill, 1998 2. Fogler, Chemical Reaction Engineering, 4th Edition, McGraw Hill, 2005 3. Smith J.M., Chemical Kinetics and Reactor Design, 2nd Edition, McGraw Hill,2004 UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 42 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1033 FACULTY OF CHEMICAL ENGINEERING PROCESS EQUIPMENT DESIGN AND DRAWING – II L T P Credits Total Marks 3 0 0 3 100 (All Tables/Handbook/Data Books/Graph Sheets are permitted during the Examination) UNIT I REACTORS 10 hrs. Fundamental principles, equations, general design and drawing considerations of Reactors. UNIT II DRIERS AND CRYSTALLIZERS 10 hrs. Fundamental principles, equations, general design and drawing considerations of cooling towers, driers and crystallizers. UNIT III HEAT EXANGERS AND EVAPORATORS 10 hrs. Fundamental principles, equations, general design and drawing considerations of heat exchangers, condensers, ,reboilers and evaporators. UNIT IV DISTILLATION COLUMNS 10 hrs. Fundamental principles, equations, general design and drawing considerations of distillation columns - plate and packed. UNIT V ABSORPTION AND ADSORPTION 10 hrs. Fundamental principles, equations, general design and drawing considerations of equipments for adsorption and absorption. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. 7. Perry R.H., “Chemical Engineers’ Handbook”, 8th Edition, McGraw Hill, 2008 McCabe W.L., Smith J.C. and Harriet, “Unit Operation of Chemical Engineering”, 7th Edition, McGraw Hill,2009 Robert Treybal, “Mass Transfer Operations”, 3rd Edition, McGraw Hill, 2004 Coulson J.M. and Richardson J., “Chemical Engineering”, Vol. 6, Asian Books Printers Ltd. Joshi M.V. and Mahajan V.V., “Process Equipment Design”, 5 th Edition, MacMillan India Ltd, 2005. Dawande S.D., “Process Design of Equipments”, 2nd Edition, Central Techno Publications, Nagpur, 2000. Indian Standard Specifications IS-803, 1962; IS-4072, 1967; IS-2825, 1969. Indian Standards Institution, New Delhi, 1969. UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 80% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 43 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX4006 FACULTY OF CHEMICAL ENGINEERING HEAT TRANSFER LAB L T P Credits Total Marks 0 0 4 2 100 1. To measure the emissivity of the test plate and plot a graph between emissivity and temperature. 2. To determine the thermal conductivity of metal rod. (Brass rod) 3. To determine the thermal conductivity of hylem, wood, and asbestos. 4. To find the thermal conductivity of the given insulated material by using lagged pipe. 5. To determine the temperature distribution for a cylinder due to heat transfer by natural convection. 6. To study and compare temperature distribution heat transfer rate, overall heat transfer co-efficient in parallel flow heat exchanger. 7. To study and compare temperature distribution, heat transfer rate, overall heat transfer co-efficient in counter flow heat exchanger SCHX4007 MASS TRANSFER LAB L T P Credits Total Marks 0 0 4 2 100 1. Study the drying characteristics of calcium carbonate and find the critical moisture content and equilibrium moisture content of the sample. 2. Determine the diffusivity coefficient for the acetone - air system. 3. Verify Rayleigh’s equation for the given acetone - water system by simple distillation. 4. Conduct a batch leaching test to leach out sodium carbonate from the mixture given and hence find out the percentage of sodium carbonate leached out. 5. Verify Frendlich equation for the adsorption of oxalic acid onto activated carbon. 6. Determine the liquid - liquid equilibrium of the system (Benzene - acetic acid - Water) and hence draw the ternary graph for the system. 7. Determine the HETP of the packed column by Fenske’s method. B.Tech. (CHEMICAL ENGINEERING) 44 REGULATIONS 2010 SATHYABAMA UNIVERSITY SBAX1001 FACULTY OF CHEMICAL ENGINEERING PRINCIPLES OF MANAGEMENT AND PROFESSIONAL ETHICS L T P Credits Total Marks 3 0 0 3 100 UNIT I MANAGEMENT FUNCTIONS & STRUCTURE 10 hrs. Management – Definition – Basic Function – Contribution of Taylor & Fayol. Types of structure – Line, staff, Functional, Committee, Project & Matrix – Structures. Departmentalization – Centralization – Decentralization – span of control. Management By Objectives – Management By Exception. UNIT II MANAGEMENT OF ORGINASATION 10 hrs. Forms of Business / Industrial Ownership – Sole Trader, Partnership, Company, Performance Appraisal – Basic Principles – Pitfalls – Methods to Overcome. Industrial Safety – Causes of Accidents – Cost of Accident – How to minimize Accidents. Plant Layout & Maintenance – Need, Types & Managerial Aspects. UNIT III ORGANISATIONAL BEHAVIOUR 10 hrs. OB – Definition – Nature & Scope – Contributing Disciplines – Importance of OB to Managers. Personality – Definition – Theories – Factors Influencing Personality. Motivation – Definition – Theories. Theory X & Y – Transactional Analysis. Morale & Job Satisfaction – Factors Influencing Job Satisfaction. UNIT IV GROUP DYNAMICS 10 hrs. Group – Definition – Types – Determinants of Group Cohesiveness – Communication – Process – Barriers – Effective Communication. Leadership Theories – Factors Contributing to Effective Leadership – Role of Trade Union in Organizations – Functions of Trade Union – Why Trade Union is required? – Types of Trade Union. UNIT V PROFESSIONAL ETHICS 10 hrs. Ethics in Workplace – Formulation of Ethics – Managerial Ethics – Managing Ethical Behaviour – Codes of Ethics – Encouraging Ethical Behaviour – Social Responsibility – Spirituality. TEXT / REFERENCE BOOKS 1. 2. 3. 4. 5. Gupta C.B., Management Theory and Practice, 14th Edition, Sultan Chand & Sons, 2009. Dr. Prasad L.M., Principle & Practice of Management, 7th Edition, Sultan Chand & Sons, 2008. Aswathappa, Organisational Behaviour, 8th Edition, Himalaya Publishing House, 2010. Dr. Prasad L.M., Organisational Behaviour, 4 th Edition, Sultan Chand & Sons, 2008. Harold Koontz, Principles of Management, 1st Edition, Tata McGraw Hill, 2004. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 45 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1034 FACULTY OF CHEMICAL ENGINEERING BIOCHEMICAL ENGINEERING L T P Credits Total Marks 3 0 0 3 100 UNIT I MICROBIOLOGY 10 hrs. Types of Microorganism: Structure and function of microbial cells. Fundamentals of microbial growth, batch and continuous culture. UNIT II ENZYME AND ENZYME KINETICS 10 hrs. Introduction to Biochemistry, Function and applications. Nature and function of enzyme. Coenzyme / Cofactor. Classification of enzymes. Isolation and purification of enzymes from cells. Assay methods and units. Examples of applications of enzymes in Pharmaceutical industry. UNIT III FERMENTATION AND KINETICS 10 hrs. Fermentation – Types of mechanisms, Continuous fermentation aeration and agitation, kinetics of fermentation Processes Immobilization: Cell and enzyme immobilization UNIT IV DESIGN OF BIOREACTOR 10 hrs. Introduction of Bioreactor design: Continuously stirred aerated tank bioreactors. Mixing power correlation. Determination of volumetric mass transfer rate of oxygen from air bubbles and effect of mechanical mixing and aeration on oxygen transfer rate, heat transfer and power UNIT V INDUSTRIAL BIOREACTORS 10 hrs. Industrial Bioreactors Utilizing Isolated enzymes and biosensors development and applications. Design of reactor, Batch and continuous type; analysis for immobilized enzyme reactors. Sterile and non sterile operations; reactors in series with and without recycle. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Bailey J.E. and Ollis D.F., “Bio Chemical Engg. Fundamentals”, 2nd Edition., Mc Graw Hill Publishing Company New York, 1986. Wiseman A., “Hand Book of Enzyme Biotechnology”, Ellis Horwood, 1983. Pye E.K. and Wingard L.B., “Enzyme Engg II”, 2 nd Edition, Plenum Press, Newyork, 1974. Aaiba S; Humphrey A E; Millis N.F., Bio Chemical Engg., 2 nd Edition., Academic Press, 1973. UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 30% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 46 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1035 FACULTY OF CHEMICAL ENGINEERING TRANSPORT PHENOMENA L T P Credits Total Marks 3 0 0 3 100 UNIT I FUNDAMENTALS OF TRANSPORT PHENOMENA 10 hrs. Newton’s law, Non-Newtonian fluids, pressure and temperature dependence of viscosity theory of viscosity of liquids, Shell Momentum balances, flow of falling film, flow through a circular tube, flow through an annulus, adjacent flow of two immiscible fluids The equation of Continuity, The equation of Motion , use of the Equations of Change to set up steady flow problems UNIT II TEMPERATURE DISTRIBUTION 10 hrs. Fourier’s Law of Heat Conduction, Temperature Distribution in Solids and in Laminar Flow, Shell Energy Balances, Heat Conduction with an electrical heat source, heat conduction with a viscous heat source, heat conduction with a chemical heat source, heat conduction through composite walls, heat conduction in a cooling fin, forced and free convection. UNIT III CONCENTRATION DISTRIBUTION 10 hrs. Definitions of concentrations, velocities and mass fluxes, relations among the molar fluxes, Fick’s law of Diffusion, Temperature and Pressure Dependence of Mass Diffusivity, Theory of ordinary diffusion in gases at a low density, theories of ordinary diffusion in liquids, Shell mass balances, Diffusion through a stagnant gas film, Diffusion with heterogeneous chemical reaction, Diffusion with homogeneous chemical reaction, Diffusion and Chemical reaction inside a porous catalyst and the “Effectiveness Factor”. UNIT IV FRICTION FACTORS AND MACROSCOPIC MOMENTUM BALANCE 10 hrs. Definition of Friction factors, friction factors for flow in tubes and for flow around spheres, Determination of diameter of a falling sphere, Friction factors for packed columns, the macroscopic mass, Momentum and Mechanical energy balances, use of Macroscopic balances to set up steady flow problems, Pressure rise and friction loss in a sudden expansion, performance of a liquid- liquid ejector, thrust on a pipe bend, Isothermal flow of a liquid through an orifice UNIT V TRANSPORT IN TURBULENT AND ANALOGIES BETWEEN TRANSPORT PROCESSES 10 hrs. Turbulence, Reynolds equation for incompressible turbulent flow, Reynolds stresses Prandtl’s mixing length theory, Eddy viscosity, the statistical theory of turbulence, Correlation coefficients, intensity and scale of turbulence. Turbulence measurement, Hot – wire anemometer. Turbulence flow in a closed conduit, Prandtl’s Power law of Velocity distribution in smooth and rough pipes. Analogy between Momentum, Heat and Mass transfer. The Reynolds’Analogy for turbulent flow over a flat plate, The Prandtl’s Analogy, The Von karmon Analogy, Coulburn analogy TEXT/REFERENCE BOOKS: 1. Bird R.B., Stewart W.E. and Lightfoot E.N., Transport Phenomena, 2nd Edition, Wiley, New York, 2006, 2. Knudson J.G. and Katz D.L., Fluid Dynamics and Heat Transfer, 2nd Edition, McGraw Hill, New York, 2000. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 60% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 47 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1036 FACULTY OF CHEMICAL ENGINEERING ENERGY ENGINEERING L T P Credits Total Marks 3 0 0 3 100 UNIT I CONVENTIONAL ENERGY SOURCES 10 hrs. Energy sources, Coal, Oil, Natural gas, Nuclear fuels, Hydro power, The Formation of Natural, Resources, energy situation, exploration. UNIT II NEW AND RENEWABLE ENERGY SOURCES 10 hrs. Study and design aspect of power plants using new and renewable energy sources. Viz., solar, wind, geothermal, ocean thermal, tidal wave. Design of bio gas plant. Bio mass energy, alternate fuels from biomass for automotive engines. UNIT III DIRECT ENERGY CONVERSION 10 hrs. Solar cells, photovoltaic cells, theory of junction type cells and construction details. Fuel cells, types, practical considerations. Magneto hydrodynamic generator, electrical conductivity and formation of MHD, performance. Prospects of large, medium and small-scale generations. UNIT IV NEW ENERGY CONVERSION SYSTEMS 10 hrs. Other energy transformations, coal gasification and liquefaction, role of coal in energy crisis, fluidized bed combustion. Synfuels. Hydrogen- methods of application, co- generation. UNIT V ENERGY CONVERSION AND MANAGEMENT 10 hrs. Waste heat recovery, heat pump. Demand forecasting, global developments, principles of energy accounting and auditing, economics. Principles of energy management. Technology assessment. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. 5. 6. Rai G.D., Solar Energy Utilisation, 3rd Edition, Khanna Publishers, New Delhi, 2000. Rai G.D., Non Conventional Energy Sources, 3rd Edition, Khanna Publishers, New Delhi, 2000 Rao S.S., Energy Technology, 3rd Edition, Khanna Publishers, New Delhi, 2006 Rused C.K., Elements of Energy Conservation, 4th Edition, McGraw Hill, 1985 Christopher H. and Armsteed H., Geothermal Energy, 2nd Edition, John Wiley, New York, 1978. Pandyan S.B., Conventional Energy Technology, Fuels and Chemical Engineering, 2nd Edition, Tata McGraw Hill, New Delhi, 1988. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 48 REGULATIONS 2010 SATHYABAMA UNIVERSITY SBAX1002 FACULTY OF CHEMICAL ENGINEERING ENGINEERING ECONOMICS & MARKETING MANAGEMENT L T P Credits Total Marks 3 – – 3 100 UNIT I ENGINEERING ECONOMICS FOR PROCESS ENGINEERS, INTEREST & INVESTMENT COSTS 10 hrs. Value of Money - Equivalence, Equations for Economic Studies and Equivalence, Amortization, Capital Recovery, Depreciation, Depletion. UNIT II COST ESTIMATION, ANNUAL REPORTS AND ANALYSIS OF PERFORMANCE 10 hrs. Capital Requirements for Process Plants, Cost Indices. Equipment Costs, Service Facilities, Capital requirements For Complete Plant, Balance Sheet, Cost Earnings, Profits and Returns, Variable Costs, Fixed Costs, Income Statement, Economic Production Charts, Capacity Factors. UNIT III INVESTMENT ALTERNATIVE AND ECONOMIC BALANCE 10 hrs. Economics of Selecting alternates, annual Cost methods, Present worth method, Equivalent Alternate, Rate of Return and payback Time. Cash flow analysis Economic balance - batch Operations, cyclic Operations and Multiple Equipment Units. UNIT IV MICRO AND MACRO ECONOMICS 10 hrs. Micro Economics - Elasticity of Demand and Supply, Demand Forecasting Methods. Economic Analysis, Cost Analysis. Time Element, BEP Macro Economics – Multiplier and Accelerator, National Income Accounting, Business Cycle. UNIT V MARKETING MANAGEMENT 10 hrs. Marketing Management - Concepts of Consumer and Producer, Industrial Marketing, Tools for Market forecasting - Advertisements and Promotions. Distribution Channels -Middlemen -Franchising - (SRP/RM/ VEC) TEXT / REFERENCE BOOKS 1. 2. 3. 4. Schweyer H.E., “Process Engineering Economics”, 2nd Edition, McGraw Hill, Newyork, 1959. Peter N.Y. and Timmerhaus, “Plant Design and Economics for Chemical Engineers”. 3 rd Edition, McGraw Hill, 2000 Philip Kotler, Principles of Marketing Management, 12 th Edition, Pearson Publications, 2009. Sherlekar S.A, Marketing Management, 14 th Edition, Himalaya Publications House, 2008. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 40% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 49 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1037 FACULTY OF CHEMICAL ENGINEERING PROCESS MODELING SIMULATION AND OPTIMIZATION L T P Credits Total Marks 3 0 0 3 100 UNIT I BASICS OF MODELING 10 hrs. Introduction to Modeling, Mathematical model, Types of Mathematical model, Classification of models. Application and scope of coverage, Principles of formulation. Fundamental laws-Continuity equation, Energy equation, Equations of motion. Regression and Correlation analysis UNIT II NUMERICAL METHODS 10 hrs. Review of generation and solution of linear equations, algebraic equations, ordinary and partial differential equations. Solution of linear simultaneous equations, Gauss elimination, Gauss siedel method, successive over relaxation method. Matrix computation, linear transformation, eigenvalue and singular value decomposition. UNIT III MODELING OF REACTORS 10 hrs. Batch reactor, CSTR, series of isothermal, Constant Holdup CSTR, CSTR with variable holdup, non isothermal CSTR, Plug flow Reactor, Packed bed reactor. UNIT IV MODELING OF HEAT AND MASS TRANSFER OPERATIONS 10 hrs. Modeling of heat exchangers, evaporators, absorption columns, ideal binary distillation column, multicomponent non-ideal distillation column, batch distillation with holdup, Single component vaporizer UNIT V SIMULATION AND OPTIMIZATION 12 hrs. Dynamic simulation of batch reactor, CSTR, PFR, Distillation column, Evaporator and Absorption column. Introduction, applications, types of optimization scope and hierarchy of optimization. General procedure for solving optimization problems. TEXT/REFERENCE BOOKS: 1. William L.Luyben, Process Modelling, Simulation and Control For Chemical Engineers, 2nd Edition. McGraw Hill International Editions, New York ,1990. 2. Davis M.E., Numerical methods and Modelling for Chemical Engineers, 1st Edition, Wiley, New York, 1984. 3. Denn M.M., Process Modelling, 2nd Edition, Wiley, New York, 1986. 4. Ramirez W., Computational Methods in Process Simulation, 1 st Edition, Butterworth’s Publishers, New York, 1989. 5. Mickley. H.S.Sherwood.T.S. and Reed C.E., Applied Mathematics for Chemical Engineers, 1st Edition, Tata McGraw Hill Publishing Co. Ltd, New Delhi, 1989. UNIVERSITY EXAM QUESTION PAPER PATTERN Max Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 50 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1038 FACULTY OF CHEMICAL ENGINEERING INDUSTRIAL SAFETY AND HAZARD ANALYSIS L T P Credits Total Marks 3 0 0 3 100 UNIT I INDUSTRIAL SAFETY 10 hrs. Industrial safety principles, accidents, site selection and plant layout, design for ventilation, emergency response systems for hazardous goods, basic rules and requirements which govern the chemical industries. Major Industrial accidents – Case Study UNIT II HAZARDS 10 hrs. Chemical hazards classification, hazards due to fire, explosion and radiation. Potential hazards. Chemical and Physical job-safety analysis, High-pressure and high temperature operations, toxic effects, highly radioactive materials. Safe handling and operation of materials and machineries. UNIT III HAZARD ANALYSIS 10 hrs. Types of hazard analysis -hazard identification –MSDS, Safety Audit- Hazard and Operability studies. Fault tree analysis. Event tree analysis. UNIT IV APPRAISAL 10 hrs. Effective steps to implement safety procedures, periodic training and regular maintenance, personal protective equipments-types, fire fighting equipments. UNIT V HEALTH HAZARDS AND LEGAL ASPECTS 10 hrs. OSHA Health hazards -occupational - Industrial health hazards. Health standards and rules. Safe working environment. Factories act, Labor welfare act, ESI act, Workmen compensation act. TEXT/REFERENCE BOOKS: Fawcett H.H. and Wood W.S., Safety and Accedent Prevention in Chemical Operation, 2nd Edition, Inter Science, 1982 Blake R.P., Industrial Safety, 2 nd Edition, Prentice Hall Inc., New Jersey, 2006. Deshmukh. L.M. Industrial Safety Management, 3 rd Edition, Tata McGraw Hill, New Delhi, 2008 Jain.R.K and Sunil Rao, Industrial Safety, Health and Environmental Management Systems, 1 st Edition, Khanna Publishers Delhi 2006. 5. Shrikant Dawande, Chemical Hazards and Safety, 2nd Edition, Dennet & Co 2007 1. 2. 3. 4. UNIVERISTY EXAM QUESTION PAPER PATTERN Max. Marks :80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 51 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX4008 FACULTY OF CHEMICAL ENGINEERING CHEMICAL REACTION ENGINEERING LAB L T P Credits Total Marks 0 0 4 2 100 1. Determine the rate constant for the saponification of Ethyl acetate with sodium hydroxide in a Plug Flow Reactor 2. Determine the rate constant for the reaction of ethyl acetate with sodium hydroxide of equimolar concentration in a batch reactor 3. Determine the rate constant for the reaction of ethyl acetate with sodium hydroxide of non-equimolar concentration in a batch reactor 4. Study the residence time distribution in a Plug Flow Reactor using Step Input 5. Study the residence time distribution in a Mixed Flow Reactor using Step Input 6. Determine the performance of three Mixed Flow reactors in series 7. Study of residence time distribution in a Mixed Flow Reactor using Pulse Input 8. Determine the rate and enhancement factor using non-catalytic solid liquid reactor 9. Determine the enhancement factor for the dissociation factor of Cinnamic acid in a Photochemical reactor 10. Determine the rate constant for the saponification of Ethyl acetate with sodium hydroxide in a Mixed Flow Reactor 11. Determine the heat of reaction using adiabatic reactor PROCESS SIMULATION LAB SCHX4007 L T P Credits Total Marks 0 0 4 2 100 1. Introduction to software (flow sheeting) 2. Simulation of flash drum 3. Simulation of distillation columns 4. Simulation of absorption columns 5. Simulation of Reactors 6. Simulation of Heat Exchangers. 7. Simulation of pumps and compressors. 8. Simulation of mixing 9. Process simulation study involving mixing, reactor, distillation, heat exchanger for any of the following: (a) Ethylene Glycol from Ethylene oxide (b) Atmospheric distillation of crude oil (c) Propylene Glycol from Propylene oxide (d) Styrene from Ethyl Benzene S19PROJ PROJECT WORK AND VIVA VOCE L T P Credits Total Marks 0 0 30 15 100 The objective of the project work is to make use of the knowledge gained by the student at various stages of the degree course. Students, will also be permitted to undertake industrial/consultancy project Work, outside the department, in industries/Research labs. There shall be three assessments during the semester by a review committee. The student shall make three presentations on the progress made before the committee at various stages of the Project work. The Head of the Department shall constitute the review committee for each branch of study. The total marks obtained in the three reviews, shall be taken in to account. There will be a viva-voce examination at the end of the Project work, conducted by one internal examiner and one external examiner. The total marks secured will be the sum of marks secured in the Project reviews and Viva Voce Examination. Each student is required to submit a Project report on the project assigned to him by the department. The report should be based on the information available in the literature or data obtained by the student by way of experiments conducted in the laboratory/industry. B.Tech. (CHEMICAL ENGINEERING) 52 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1040 FACULTY OF CHEMICAL ENGINEERING OPTIMIZATION OF CHEMICAL PROCESSES L T P Credits Total Marks 3 0 0 3 100 UNIT I OBJECTIVE AND FORMULATION OF OPTIMIZATION 10 hrs. Objective and Introduction, Objective Function and Decision variables, Inequality and Equality Constrains in Models Formulation of the Objective Function, Lower and Upper Bounds, Selecting Functions to Fit Empirical Data, Factorial Experimental Designs, Degrees of Freedom, Economic Objective Functions, Measures of Profitability UNIT II BASIC CONCEPTS OF OPTIMIZATION 10 hrs. Continuity of Function, NLP Problem Statement, Convexity and Its Applications, Interpretation of the Objective Function in Terms of its Quadratic Approximation, Necessary and Sufficient Conditions for an Extremum of an Unconstrained Function Unit III OPTIMIZATION OF UNCONSTRAINED FUNCTIONS 10 hrs. One-Dimensional Search Numerical Methods for Optimizing a Function of One Variable, Scanning and Bracketing Procedures, Newton and Quasi-Newton Methods of Unidimensional Search UNIT IV UNCONSTRAINED MULTIVARIABLE OPTIMIZATION 10 hrs. Linear Programming (LP) and Applications Geometry of Linear Programs, Basic Linear Programming Definitions and Results, Simplex Algorithm, Barrier Methods, Sensitivity Analysis, Linear Mixed Integer Programs, Application of the EXCEL Solver Spreadsheet for Optimization, Formulation. Introduction to Non linear Programming with Constraints and Mixed-Integer Programming Unit V APPLICATION OF OPTIMIZATION IN CHEMICAL ENGINEERING 10 hrs. Examples of Optimization in Chemical Processes like optimizing recovery of waste heat, Optimal Shell and Tube Heat Exchanger Design, Optimal Design and Operation of binary Distillation Column, Optimal pipe diameter etc. Flow sheet Optimization - Case studies. TEXT / REFERENCE BOOK: 1. Edger T.F., Himmelblau D.M. and Lasdon L.S., “Optimization of Chemical Processes”, 2nd Edition, McGraw- Hill, 2001 2. Seider W.D., Seader J.D. and Lewin D.R., “Product and Process Design Principles-Synthesis, Analysis, and Evaluation”, 2nd Edition, John Wiley and Sons Inc., 2008. 3. Kalyan Moy Deb “Optimization for Engineering Design”, 2nd Edition, Prentice Hall of India, 2009 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 80% Problems - 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 53 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1054 FACULTY OF CHEMICAL ENGINEERING COMPUTER APPLICATIONS IN CHEMICAL ENGINEERING L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION TO COMPUTER APPLICATIONS 10 hrs. Understanding of operating systems and networks, Importance of computing in chemical engineering, fundamentals of programming UNIT II DATABASES 10 hrs. Relational databases. SQL. ODBC. Real-time databases; Devise solutions and implement solutions to database queries using interactive SQL DML commands. Devise and implement efficient database design; Data Base Management and Qualitative Interpretation of Process Data UNIT III COMPUTER NETWORKS 10 hrs. Internet, XML, OPC; OPC techniques, capabilities and issues. Build, apply and debug Model-based OPC UNIT IV ARTIFICIAL INTELLIGENCE AND NETWORKS 10 hrs. Artificial Intelligence and Networks in Chemical Engineering, Expert Systems (CONPHYDE, KBS) and Tools (KEE, ART), Artificial Neural Network, Learning and Training, Process Plant Diagnosis, Safety Analysis UNIT V MODELING AND SIMULATION PACKAGES 10 hrs. Process Modelling, Interfacial properties, Fault Diagnosis and Trouble Shooting; Simulation Packages, ASPEN PLUS, Batch Processing Packages (SUPERPRO), FLUENT TEXT / REFERENCE BOOKS: 1. Riggs, J.B., An Intoduction to Numerical Methods for Chemical Engineers, 2nd Edition, Texas Tech University Press, Lubbock, Texas, 1998. 2. Hanna, O.T. and Sandal O.C., Computation Methods in Chemical Engineering, 2nd Edition, Prenti-Hall, Englewood Cliff, New Jersey, 1997. 3. Constantinides, A., Applied Numerical Methods with Personal Computers, 2nd Edition, Mc-Graw Hill, NewYork, 1989 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 54 REGULATIONS 2010 SATHYABAMA UNIVERSITY SMEX1038 FACULTY OF CHEMICAL ENGINEERING COMPUTATIONAL FLUID DYNAMICS L T P Credits Total Marks 3 0 0 3 100 UNIT I GOVERNING DIFFERENTIAL EQUATIONS 10 hrs. Conservation of chemical species -the energy equation – Momentum equation -Time -Averaged equations for Turbulent flow – Turbulence -Kinetic -Energy Equations -The General Differential Equation -Nature of Coordinates-Independent variables-Choice of Co-ordinates-One way and Two-way Co-ordinates. UNIT II DISCRETIZATION METHODS 10 hrs. Nature of numerical methods – Methods of Deriving the Discretization Equations – Taylor Series formulation – variational formulation-Method of weighted residuals -Control volume –Formulation. UNIT III HEAT CONDUCTION, CONVECTION AND DIFFUSION 10 hrs. Steady state one-dimensional conduction – two and three dimensional conduction -Steady state one-dimensional convection and Diffusion – Discretization equations for two dimensional convection and diffusion. UNIT IV CALCULATION OF FLOW FIELD 10 hrs. Representation of the pressure.- Gradient term and continuity equation – Staggered grid – Momentum equations -Pressure and velocity corrections – Pressure. – Correction equation. Introduction to Finite Element method -Solution of Steady state heat conduction by FEM – incompressible flow -Simulation by FEM. UNIT V TURBULENCE MODELS – ALGEBRAIC MODELS 10 hrs. One equation Model – Two equation models – High and Low Reynolds number models – Reynolds stress models – Prediction of fluid flow and heat Transfer using Standard codes. TEXT / REFERENCE BOOKS: 1. 2. 3. 4. Muralidhar K., and Sundarajan T., “Computational Fluid Flow and Heat Transfer”, Narosa Publishing House, New Delhi, 1995. Ghoshdastidar P.S., “Computer Simulation of flow and heat transfer”, Tata McGraw Hill Publishing Company Ltd., 1998. Fletcher C.A.J., “Computational Techniques for Fluid Dynamics “1” Fundamental and General Techniques, Springer-Verlag, 1987. Fletches C.A.J., “Computational Techniques for Fluid Dynamics” 2” Specific Techniques Different Flow Categories, Springer-Verlag, 1987. 5. Bose T.K, “Numerical Fluid Dynamics”, Narosa publishing House, 1997. 6. Muralidhar K., and Biswas “Advanced Engineering Fluid Mechanics”, Narosa Publishing House, New Delhi, 1996. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 hrs. Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 55 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1041 FACULTY OF CHEMICAL ENGINEERING FOOD TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I FOOD PROCESSING ENGINEERING–FUNDAMENTALS 10 hrs. Fundamentals of Food Process Engineering, Application of Quantitative methods of Material & Energy Balances in Food Engineering Practices. Constituents of Food, Quality and Nutritive aspects, Food Adulterations, Deteriorative factors and Control UNIT II UNIT OPERATIONS IN FOOD INDUSTRIES 10 hrs. Fluid Flow, Thermal Process Calculations, Refrigeration, Evaporation and Dehydration operations in Food Processing UNIT III FOOD CANNING TECHNOLOGY 12 hrs. Fundamentals of Food Canning Technology , Heat Sterilization of Canned food , Containers – metal, Glass and Flexible packaging . Canning Procedures for Fruits, Vegetables, Meat, Poultry, marine Products UNIT IV FOOD PRESERVATION METHODS 10 hrs. Preservation by Heat and Cold, Dehydration, Concentration, Drying, Irradiation, Microwave heating, Sterilization and Pasteurization, Fermentation and Pickling, Packaging Methods UNIT V PRODUCTION AND UTILIZATION OF FOOD PRODUCTS 10 hrs. Cereal Grains, Pulses, Vegetables, Fruits, Spices, Fats and Oils, Bakery, Confectionary and Chocolate Products. Soft and Alcoholic Beverages, Dairy Products , Meat , Poultry and Fish Products TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Norman N.Potler Joseph .H. Hotchk’ss, 5th Edition.CBS Publishers & Distributors India, 1987. Owen .R.Fennema.Principles of Food Science Part I & II, Marcel Dekker Inc New York, 1976. Heid, J.L., Joslyn M.A, Fundamentals of Food Processing Operation, 3rd Edition, The AVI Publishing Co., Westport,1967. Heldman, D.R., Food Process Engineering, 2nd Edition, The AVI Publishing Co.,1965. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 56 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1042 FACULTY OF CHEMICAL ENGINEERING FERTILIZER TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION TO CHEMICAL FERTILIZERS 10 hrs. Chemical inorganic Fertilizer and organic manure. Types of fertilizers plant nutrients, location and function of fertilizer components. Manufacture of Ammonia, Nitric acid, Phosphoric acid. UNIT II NITROGENOUS FERTILIZERS 10 hrs. Feed stock for production of Ammonia- Natural gas, Associated gases, Naphtha, Fuel oil, Coke oven gas. Production of nitrogenous fertilizers-Ammonium sulphate, Ammonium nitrate, Urea, Calcium ammonium nitrate, Diammonium phosphate, Ammonium chloride and their methods of production, Specification, storage and handling. UNIT III POTASSIUM FERTILIZERS 10 hrs. Sources of potassium- Location, Methods of production of potassium chloride, Potassium schoenites. Function of potassium in plants. Their methods of production, Characteristic and Specifications UNIT IV PHOSPHATIC FERTILIZERS 10 hrs. Raw materials, Phosphate rock, Sulfur pyrite, etc., Phosphate fertilizer- ground rock phosphate, Bone mealSingle super phosphate, Triple super phosphate, Thermal phosphate, their methods of production, characteristics and specifications. UNIT V COMPLEX FERTILIZER AND MISCELLANEOUS FERTILIZERS 10 hrs. Types of complex fertilizers, composition ,Production of ammonium phosphate fertilizers, Ammonium sulfate, Di ammonium phosphate, Nitro phosphate , Mono Ammonium Phosphate and various grade of NPK fertilizers Produced in industries. Mixed fertilizers and granulated mixtures- Bio fertilizers and nutrients. Secondary nutrients and Micronutrients, Fluid fertilizers. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Handbook of Fertilizer Technology, Fertilizer Association of India, New Delhi, 1998 George T. Austin, Shreve’s Chemical Process Industries, 5th Edition., McGraw-Hill International Editions, Singapore, 1984. Gopala Rao M. and Marshall Sittig, Dryden’s Outlines of Chemical Technology, 3rd Edition., East-West Press, New Delhi, 1997. Slack. A.V., Chemistry and Technology of Fertilizers, 2nd Edition, Interscience, Newyork, 1967 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 57 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1043 FACULTY OF CHEMICAL ENGINEERING POLYMER TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION TO POLYMERS 10 hrs. Classification of polymers, polymerization process, chemistry and Kinetics of step growth and chain growth polymerization, polymerization techniques: Bulk, solution, suspension emulsion, mold, polycondensation, interfacial condensations, solid and gas phase polymerization. UNIT II MOLECULAR WEIGHT & SIZE OF POLYMERS 10 hrs. Number average and weight average molecular weight, significance of molecular weight, determination of molecular weight and group analysis, solution viscosity method, osmotic pressure, light scattering method, gel permeation chromatography method etc. UNIT III POLYMER PROPERTIES & THEIR TESTING 10 hrs. Glass transition temperature and associated properties, thermosetting polymers. Tensile strength & impact strength and their determination, softening point, heat distortion dielectric and power factor etc. Theology of polymeric materials. UNIT IV SYNTHESIS & PROPERTIES OF COMMERCIAL POLYMERS 10 hrs. Plastic, rubber and fibers of commercial importance, polymer auxiliaries; plasticizers, stabilizers, fillers, lubricant etc. Manufacture, processing and properties of resins and fiber forming polymers such as phenol formaldehyde, urea formaldehyde, epoxy resins, urethane foam and silicon polymers; LDPE, HDPE, polypropylene, polyvinyl chloride, polystyrene, polybutadiene, polyacrylonitrile, polyamide, etc. fiber reinforced plastics UNIT V ENGINEERING APPLICATIONS OF POLYMERS 10 hrs. Elastomeric composites in tyre technology, polymers in fiber, man made fibers, acetate fiber, acrylic, nylon, olefin, polyester, rayon, synthetic adhesives, Bio-polymers and their applications, plastics and polymers in agriculture industry, Plastics in consumer goods, polymer powders, coating and medical applications of polymers. Polymer Degradation: Thermal, Mechanical and by ultrasonic waves, photo degradation, heat energy radiation, oxidation and hydrolysis. TEXT/REFERENCE BOOKS: 1. Billmeyer F.W. , “Text Book of Polymer Science” 3rd Edition, Wiley, Singapore, 1984. 2. Anilkumar and Gupta R.K, Fundamental of Polymers, 2nd Edition, McGraw Hill, 1996 3. Ghosh. P, “Polymer Science & Technology of Plastics & Rubber” 2 nd Edition, McGraw Hill, Newyork, 2001 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 58 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1044 FACULTY OF CHEMICAL ENGINEERING OILS AND FATS TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I AN OVERVIEW 10 hrs. General aspects of edible oils, oil seeds and fats technology; World requirement of oils and fats; Indian scenario. UNIT II OILS AND FATS CONSTITUENTS 10 hrs. Constituents and Chemistry of oils and fats; Application of oils and fats; Fat substitutes. UNIT III GENERAL ENGINEERING ASPECTS AND PROCESSING METHODS 10 hrs. Recovery and Pretreatment of oils and fats; Analysis. UNIT IV OIL REFINING 10 hrs. Physical treatment; Chemical Bleaching; Deodorizing; Wintering. UNIT V HYDROGENATION 10 hrs Hydrogenation of oils in general; Equipment; Catalysts; Dry & Wet reduction. The Hardening operation; Hydrogenation products. TEXT/REFERENCE BOOKS: 1. George T. Austin, Shreve’s Chemical Process Industries, 5th Edition., McGraw-Hill International Editions, Singapore, 1984. 2. Gopala Rao M. and Marshall Sittig, Dryden’s Outlines of Chemical Technology, 3rd Edition., East-West Press, New Delhi, 1997. 3. Kent J.A. (ed). Riegel’s “Handbook of Industrial Chemistry", 2nd Edition, Van Nostrand Reinhold, 1974. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 59 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1049 FACULTY OF CHEMICAL ENGINEERING DRUGS AND PHARMACEUTICALS TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Pharmaceutical Industry, Drug discovery and Development of Drugs, Organic Therapeutic agents uses and Economics .Drug Metabolism , Physico Chemical Principles in Drug Metabolism Kinetic Studies and Action of drugs on Human Bodies UNIT II UNIT PROCESSES AND APPLICATIONS 10 hrs. Chemical Conversion Processes - Alkylation ,Carboxylation , Condensation , Cyclisation , Dehydration , Esterification , Halogenation , Oxidation , Sulfonation , Complex Chemical Conversions and Fermentation . UNIT III MANUFACTURING PRINCIPLES 10 hrs. Compressed Tablets, Wet Granulation, Dry Granulation or Slugging, Direct Compression, Tablet Presses, Formulation, Coating Pills, Parental Solutions, Oral Liquid, Injections Ointments, Role of Regulatory Authorities (FDA), Standard of Hygiene and Manufacturing Practice (GMP) UNIT IV PHARMACEUTICAL / MICROBIOLOGICAL AND ANIMAL PRODUCTS 10 hrs. Vitamins, Cold Remedies, Laxatives, Analgesics, Non Steroidal Contraceptives, External Antiseptics, Antacids, Antibiotics, Biologicals, Hormone – Preservation UNIT V ANALYSIS & QUALITY CONTROL 10 hrs. Pharmaceutical Analysis Packaging and Control ,Analytical Methods and Tests for various Drugs & Pharmaceuticals Packaging Techniques & Quality Control of Pharmaceutical Products. TEXT/REFERENCE BOOKS: 1. Rawlnes, E.A., Bentley’s Text Book of Pharmaceuticals, 7th Edition, Bailliere Tindalls, London, 2009. 2. Remingston, Pharmaceutical Sciences, 18th Edition, Mach Publishing Co., 1990. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 60 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1052 FACULTY OF CHEMICAL ENGINEERING PETROLEUM TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Classification of crude oil, Atmospheric distillation, Vacuum distillation of residue – Products and distillation practice UNIT II CRACKING AND REFORMING 10 hrs. Light end products of Distillation, Hydro cracking, Thermal cracking, FCCU, Visbreaking, Catalytic reforming of Naptha and its products. UNIT III PRIMARY FINISHING TREATMENTS 10 hrs. Processes for Kerosene, Diesel and Hydrodesulphurisation. Treatment techniques for removal of objectionable odours, Storage stability. Extraction of aromatics, olefins and recovery operations. UNIT IV SECONDARY FINISHING PROCESSES 10 hrs. Treatment of Gasoline production, Alkylation - Sulphuric acid process and Hydrofluoric acid process, Isomerisation process, Polymer gasoline. UNIT V HEAVY ENDS TREATMENT 10 hrs. Production of Lube Oil stock, Wax and Asphalt TEXT/REFERENCE BOOKS: 1. Nelson W.L., Petroleum Refinery Engineering, 4th Edition, McGraw Hill, 1958. 2. Bhaskara Rao B K, “Modern Petroleum Refining Processes”, 2 nd Edition, Oxford and IBH Publishing Company, New Delhi, 1990. 3. Ramprasad, Petroleum Refining Technology, 1st Edition, Khanna Publishers, New Delhi, 2000. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 61 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1055 FACULTY OF CHEMICAL ENGINEERING NANO TECHNOLOGY L T P Credits Total Marks 3 0 0 3 100 UNIT I SUPRAMOLECULAR CHEMISTRY 10 hrs. Supramolecular Chemistry. Definition and examples of the main intermolecular forces used in supramolecular chemistry. Self-assembly processes in organic systems. Main supramolecular structures. UNIT II NANOMATERIALS 10 hrs. Physical Chemistry of Nanomaterials. Students will be exposed to the very basics of nanomaterials; A series of nanomaterials that exhibit unique properties will be introduced. UNIT III FABRICATION 10 hrs. Methods of Synthesis of Nanometerials. Equipment and processes needed to fabricate nanodevices and structures such as bio-chips, power devices, and opto-electronic structures. Bottom-up (building from molecular level) and top-down (breakdown of microcrystalline materials) approaches. UNIT IV NANO-BIOTECHNOLOGY 10 hrs. Biologically-Inspired Nanotechnology Basic biological concepts and principles that may lead to the development of technologies for nanoengineering systems. molecular nanoscale engineered devices, nanoscale biotechnologies, nano products . UNIT V CHARACTERIZATION OF NANOMATERIALS 10 hrs. Instrumentation for Nanoscale Characterization- Instrumentation SEM, TEM, XRD, FTIR for characterization of properties .Llimits of each technique. TEXT/REFERENCE BOOKS: 1. Jean-Marie Lehn. Supramolecular Chemistry, 1st Edition, Wiley Publications, 1995. 2. Novailhat, Alain, Introduction to Nano technology, 2nd Edition, Wiley Publications, 2007. 3. Hovnyax G., Moore J., Tibbals J., Fundamental of Nanotechnology, 1st Edition, CRC Press, 1997 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 62 REGULATIONS 2010 SATHYABAMA UNIVERSITY SBAX1003 FACULTY OF CHEMICAL ENGINEERING ENTREPRENEURSHIP DEVELOPMENT L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Definition-Need-Scope for Entrepreneurial Development in India-Role Entrepreneurship-Successful cases in Entrepreneurs. Women Entrepreneurs in India. UNIT II ENTREPRENEURIAL GROWTH FACTORS of Government on 10 hrs. Characteristics - Competencies-Qualities of an Entrepreneur-Micro and Macro Factors influencing growth of Entrepreneurship-Identifying potential entrepreneurs-Differences between entrepreneur and intrapreneur & manager. UNIT III CLASSIFICATION AND DEVELOPMENT OF INDUSTRIES 10 hrs. Small Scale Industries-Definition-classification-problems-remedies-Developing Ancillary units-Institutions involved in developing Entrepreneurs: DIC, TIIC, SIDCO, SISI and NSIC. UNIT IV PROJECT PRESENTATION AND FINANCIAL ASSISTANCE 10 hrs. Market research- New Product Development-Product life cycle concept-Feasibility Analysis- Key Elements of developing project report for getting financial assistance-Institutions involved in getting Financial assistance: IFCI, IDBI, SIDBI, SFC’s and commercial banks. UNIT V LEGAL & TECHNICAL ASPECTS FOR ESTABLISHING INDUSTRIES 10 hrs. Brief idea on Factories Act 1948 (Health, Wealth, Safety measures)-Environmental pollution prevention control Acts - Procedures for getting subsidies & licenses from both Centre & State Government. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. 5. Khanka S.S, Entrepreneurial Development,16th Edition, Sultan Chand & Co.,2010. Vasant Desai, Dynamics of Entrepreneurial Development and Management, 13th Edition, Himalaya Publishing House, 2009. Gupta C.B & Srinivasan N.P, Entrepreneurial Development in India, 5 th Edition, Sultan Chand & Sons, 2008. Charantimath, Entrepreneurship Development & Small Business Enterprise, 1st Edition, Pearson Publications, 2009. Rajeev Roy, Entrepreneurship, 1st Edition, Oxford University Publications, 2009. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 63 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1046 FACULTY OF CHEMICAL ENGINEERING ENVIRONMENTAL POLLUTION AND CONTROL L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Environment definition -The biosphere -the hydrologic cycle –the nutrient cycles, pollution of air, water and soil. Air pollution laws and air quality standard. Water pollution quality standards and law. MIMAS. Air pollution effect on human, plant and animal, acid rain. UNIT II WATER POLLUTION AND ANALYSIS 10 hrs. Origin of waste water, types of waste pollutants and their effects, waste water sampling and analysis, determination of organic and inorganic matters, physical characteristics, bacteriological measurements. UNIT III WATER TREATMENT 10 hrs. Characteristics of natural water, water conditioning, softening of water, demineralization of water. Treatment of water for municipal water supplies. Industrial water treatment, the aerobic process, the anaerobic process. Water pollution effect on man, plant and animal. UNIT IV NOISE POLLUTION 10 hrs. Introduction, sources of noise pollution, Characteristics of sound, noise units, types of noise, effects and control of noise pollution.Radioactive pollution (RAP), sources of RAP-classification of its radiation effects on humans, plants and animals. UNIT V POLLUTION CONTROL AND DISPOSAL METHODS 10 hrs. Control of air pollution-UV spectrophotometry -IR spectrometry. Emission spectrometry- chromatography -prevention of water pollution and its control -waste treatment, wastewater reclamation. Various approaches to prevent and control water pollution, effectiveness of prevention and control of water pollution, industrial waste disposal method. Noise prevention and control of the types of noise pollution. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Kapoor B.S., Environmental Engineering, 3rd Edition, Khanna Publishers, 1997 Mahajan S.P., Pollution Control in Process Industries, 1 st Edition, Tata McGraw Hill, New Delhi, 1995. Jain P.C, & Monica Jain, “Engineering Chemistry”. 5th Edition, Dhanpat Rai Publications, New Delhi, 2002 Dara S.S, A Text Book of Engineering Chemistry, 3 rd Edition, S.Chan & Co Ltd, New Delhi, 2006. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 64 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1047 FACULTY OF CHEMICAL ENGINEERING NOVEL SEPARATION PROCESSES L T P Credits Total Marks 3 0 0 3 100 UNIT I THERMAL SEPARATION 10 hrs. Thermal Diffusion: Basic Rate Law, Theory of Thermal Diffusion Phenomena for gas and liquid mixtures, Equipments design and Applications. Zone Melting: Equilibrium diagrams, Controlling factors, Apparatus and Applications. UNIT II SORPTION TECHNIQUES 10 hrs. Types and choice of adsorbents, Normal Adsorption techniques, chromatographic techniques, Equipment and commercial processes, Recent advances and economics, Molecular Sieves. UNIT III MEMBRANE SEPARATION PROCESSES 10 hrs. Types and choice of membranes, their merits, commercial, pilot plant and laboratory membrane permeators, Dialysis, Reverse Osmosis, Ultrafiltration, and Economics of Membrane operations. UNIT IV IONIC SEPARATION 10 hrs. Controlling factors, Applications, Equipments for Electrophoresis, Dielectrophoresis, Electro Dialysis and Ion Exchange, Commercial processes. Other Techniques: Adductive Crystallization: Molecular addition compounds, Clathrate compounds and Adducts, Equipments, Applications, Economics and Commercial processes. UNIT V FOAM SEPARATION 10 hrs. Surface Adsorption, Nature of foams, Apparatus, Applications, and Controlling factors. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Schoen H. M., "New Chemical Engineering Separation Techniques", 2nd Edition, Inter Science Publications, New York, 1972. Loeb .C and Lacey R. E., "Industrial Processing with Membranes", 2 nd Edition, Wiley Inter Science, 1972 Perry R.H. and. Green D.W, “Perry’s Chemical Engineers Hand book”, 6th Edition., McGraw Hill, New York, 1990. Coulson J. M. and Richardson J. F., "Chemical Engineering", Vol. II, 4 th Edition, Butterworth, Heinemann, London, 1991. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 65 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1051 FACULTY OF CHEMICAL ENGINEERING INDUSTRIAL CATALYSIS L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION TO CATALYSIS 10 hrs. General properties of homogenous and heterogeneous catalysis, Life cycle of catalyst, Steps in a catalytic reaction, Physisorption and chemisorption, active site, catalyst characterization, catalyst activity and selectivity. UNIT II GEOMETRIC AND ELECTRONIC FACTORS IN CATALYSIS 10 hrs. Adsorption and reaction kinetics in catalytic (heterogeneous) system, Electron band theory, valence bond theory, Dowdens rule for bond formation, semiconductor theory, charge transfer theory UNIT III CATALYST PREPARATION 12 hrs. Preparation and evaluation of industrial catalysts, catalyst formation, wet methods, precipitation and precipitation deposition, unsupported and supported metal catalyst, sintering, reverse micro emulsion method UNIT IV KINETICS OF HETEROGENEOUS REACTIONS 10 hrs. Reaction engineering applied to catalytic homogeneous and heterogeneous chemical reactions, Kinetics of adsorption and surface reaction, evaluation of kinetic parameters. UNIT V CATALYST POISONING 10 hrs. Catalyst poisoning and deterioration, (sintering) origination of catalyst, types of poison, catalyst deactivation, pour mouth poisioning, poisoning by chemical binding, catalyst cleaning and regeneration, reversible and irreversible poisoning TEXT/REFERENCE BOOKS: 1. 2. 3. 4. Smith J. M, "Chemical Engineering Kinetics", 3rd Edition., McGraw Hill, 1983. Bond G," Heterogeneous Catalysis -Principles and Applications" 2nd Edition., Oxford Univ. Press, 1986. Mukhlyonov I.et al., "Catalyst Technology", 2nd Edition., Mir Publishers, 1976. Thomas C.C., "Catalytic Processes with Proven Catalysts", Academic Press. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 66 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1053 FACULTY OF CHEMICAL ENGINEERING MULTICOMPONENT SEPARATION SYSTEM L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Introduction to multi component separation system –Technological schemes of complex oil, gas condensate processing plant-application of multi component separation system in petrochemical system-Low temperature absorption system-gas, oil and water separation system by using three phase separator UNIT II MULTI COMPONENT DISTILLATION 10 hrs. Introduction to Multi component distillation. Key components, Estimation of minimum theoretical stages (Fenke’s equation), Determination of minimum reflux ratio (Under wood’s method), Approximate calculation for multi component-multistage distillation estimation of actual reflux ratio and theoretical stages (Kirks-Bridge equation) distribution of no, key components at actual refuse UNIT III ABSORPTION 10 hrs. Absorption of multi component–calculation of number of trays by Kremser’s equation, Working of Horizontal multistage plate absorber- vertical plate and packed bed absorber, direct flow multi stage absorption and step direct flow counter flow absorption. UNIT IV EXTRACTION 10 hrs. Extraction of multi component system-Choice of solvent, single stage extraction-‘Multistage extraction-cocurrent and counter current-batch, simulation of continuous counter current cascade extraction, Stage Efficiency, Types of extractors. UNIT V CONSTRUCTION OF SEPARATORS 10 hrs. Construction of Separators, Dividers, and Settlers-vertical and horizontal separators ,gill and grid orifice separators ,centrifugal -one socket and multi socket separators, separators with grid and glass fiber coagulator, gravitation oil gas separator TEXT/REFERENCE: 1. Sinaiski E.G. and Lapiga E.J., Separation of Multiphase, Multicomponent Systems, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2003 2. Treybal R.E., Mass Transfer operation, 3rd Edition, McGraw Hill, 1980 3. Sinnott R.K., Chemical Engineering Design, 3rd Edition, Vol-6, Asian Book Printers Ltd., 2007 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 67 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1039 FACULTY OF CHEMICAL ENGINEERING CORROSION ENGINEERING L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Definition of Corrosion, corrosion damage, effect of material safety and reliability, classification of corrosion, expression of corrosion rate, electrochemical corrosion reation, redox reaction, effect of oxygen, oxidizers. Effect of temperatures and concentration of chemicals on corrosion rate , Corrosion direct & two stage attack, electrochemical attack, environment conditioning. UNIT II TYPES OF CORROSION 10 hrs. Effect of galvanic coupling, metallurgical aspects, metallic properties, ringworm corrosion, Principle of modern corrosion theory, Forms of corrosion – Uniform attack, galvanic corrosion, crevice corrosion, pitting intergranular corrosion and hydrogen damage, higher corrosion resistance through proper selection of material, isolation of corrosion prone materials from destructive environment. UNIT III CORROSION PRODUCTIVE MEASURES 10 hrs. Technologies of anodisation, enameling, rubber lining, glass lining, refractory lining, painting and other surface protective measures. UNIT IV APPLICATION OF CORROSION ENGINEERING 10 hrs. Corrosion engineering in special applications such as material transport, pumping, filtration, condensation, boiling, riveting, welding, and high temperature environments. UNIT V CORROSION TESTING AND MEASUREMENTS 10 hrs. Corrosion testing, monitoring and inspection, laboratory corrosion test, accelerated chemical tests for studying different forms of corrosion, electrochemical methods of corrosion rate measurements by DC and AC methods, corrosion monitoring methods, chemical and electrochemical removal of corrosion products, cost factor in competitive corrosion prevention / inhibition techniques. TEXT/REFERENCE BOOKS: 1. 2. 3. 4. 5. Unling, H.H., Corrosion Control, 2nd Edition, John Wiley & Sons, 1971 Butler, G. & Ison, H.C.K., Corrosion & its Prevention in Waters, 2nd Edition, Leonard Hill, London, 1966. Maslow, P., Chemical Materials for Construction, 1st Edition, Structures Publishing Co., 1974. Fontance, M.G. & Gtretrnee, N.D., Corrosion Engineering, 2nd Edition, McGraw Hill, 1967. Rajagopalan, K.S. Corrosion and its Prevention, Chemical Engineering Education Development Centre, IIT Madras, 1975. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 68 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1045 FACULTY OF CHEMICAL ENGINEERING FLUIDIZATION ENGINEERING L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION AND APPLICATIONS 10 hrs. Introduction to Fluidized bed systems. Fundamentals of fluidization. Industrial applications of fluidized beds Physical operations. Synthesis reactions, cracking and reforming of hydrocarbons, Gasification, Carbonization, Gas-solid reactions, calcining and clinkering. UNIT II GROSS BEHAVIOR OF FLUDIZED BEDS 10 hrs. Gross behavior of fluidized beds. Minimum and terminal velocities in fluidized beds. Types of fluidization. Design of distributors. Voidage in fluidized beds. TDH, variation in size distribution with height, viscosity and fluidity of fluidized beds, Power consumption. UNIT III ANALYSIS OF BUBBLE AND EMULSION PHASE 10 hrs. Davidson’s model, Frequency measurements, bubbles in ordinary bubbling bed model for bubble phase. emulsion phase: Experimental findings. Turn over rate of solids. Bubbling bed model for emulsion phase Interchange coefficients. UNIT IV FLOW PATTERN OF GAS AND HEAT & MASS TRANSFER IN FLUIDIZED BEDS 10 hrs. Flow pattern of gas through fluidized beds. Experimental findings. The bubbling bed model for Gas inter change Interpretation of Gas mixing data. Heat and Mass Transfer between fluid and solid: Experiment findings on Heat and Mass Transfer. Heat and Mass Transfer rates from bubbling bed model. UNIT V HEAT TRANSFER BETWEEN FLUIDIZED BEDS AND SURFACES- ENTRAINMENT & ELUTRIATION 10 hrs. Heat transfer between fluidized beds and surfaces: Experiment finding theories of bed heat transfer comparison of theories. Model for entrainment and application of the entrainment model to elutriation. TEXT/REFERENCE BOOK: 1. Kunii D. and Levenspiel O., “Fluidization Engineering”, 2nd Edition, John Wiley & sons, 1992. 2. Gidaspow D., ”Multiphase flow and fluidization continuum and kinetic theory description” Elsevier Science and Technology Books, 1985. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 69 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1048 FACULTY OF CHEMICAL ENGINEERING ELECTROCHEMICAL ENGINEERING L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Faraday’s law, Nernst Potential, Galvanic Cells, Polarography. The Electrical Double layer-It’s role in Electrochemical processes, Electrocappilary curve, Helmholtz layer fields at the interface. UNIT II BATTERIES 10 hrs. Batteries - Primary Batteries and Secondary Batteries, Lechlanche dry cell, Alkaline Manganese cell, Mercury cell Reverse electrolytic cells like Mg–CuCl2, Mg-PbO, Zn-PbO, Secondary cells like lead acid, Ni-Cd, Ni-Fe, AgO-Zn, AgO-Cd, Sodium-Sulfur, Li-S, Fuel Cells. UNIT III ELECTRODES 10 hrs. Electrodes-Metals Graphite, Lead Oxide, Titanium Substrate insoluble electrodes, Iron Oxide, Semiconductor type electrodes. Metal finishing, Electro Deposition, Electro refining, Electro reforming, Electro polishing, Anodizing, Selective Solar Coatings. UNIT IV ION–ION INTERACTIONS 10 hrs. True and Potential Electrolytes The nature of the Electrolyte and the Relevance of Ion-Ion Interactions. The Debye-Huckel Theory of Ion-Ion Interactions, Activity Coefficients and Ion-Ion Interactions-Ion Solvent Interactions and the Activity Coefficient, Ion Transport in Solutions, Ionic drift under an Electric field. Conduction Electro neutrality Coupling between the drifts of different Ionic Species. UNIT V ELECTROCHEMICAL SYSTEMS 10 hrs. Technological Aspects of Electrochemistry, Thermodynamics and the Stability of Metals, The Corrosion Current and the Corrosion Potential, The Passivation Surface Instability and Internal Decay of Metals; Hydrogen Embrittlement-Charge Transfer and the Stability of metals, Electrochemical Energy Conversion, Electricity Storage The Lead-Acid Storage battery, Dry cell, Two Relatively New Electricity Storers. TEXT/REFERENCE BOOKS: 1. Picket, “Electrochemical Engineering”, 1st Edition, Prentice Hall Inc., 1965. 2. Mantell C., “Electrochemical Engineering”, 2nd Edition, McGraw Hill, 1972. 3. Newman J.S.,” Electrochemical Systems”, 2nd Edition, Prentice Hall Inc., 1973. UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 70 REGULATIONS 2010 SATHYABAMA UNIVERSITY SCHX1050 FACULTY OF CHEMICAL ENGINEERING NUCLEAR ENGINEERING L T P Credits Total Marks 3 0 0 3 100 UNIT I INTRODUCTION 10 hrs. Principles of nuclear reactions – nuclear fission and fusion reactions, chain reaction uncontrolled chain reaction and a nuclear bomb, fundamentals of nuclear power generation, controlled chain reaction, control rods, energy from fission and fusion, raw materials and fuels, Isotopes, fuel burn up UNIT II RADIOACTIVE SUBSTANCES 10 hrs. Radioactivity and radioactive substances. Neutron energies, thermal neutrons, Nuclear cross sections, Fission reactor types, reactor control, fuel arrangements in a thermal reactor. Processing of nuclear fuels, Separation and purification of isotopes, Heavy water UNIT III NUCLEAR REACTORS 10 hrs. Pressurized water reactor, PWR power plant, Boiling water reactor, BWR power plant, Gas cooled reactor, high temperature gas cooled reactor. UNIT IV REACTOR ACCESSORIES 10 hrs. Concept of breeding, Fast breeder reactors, Liquid metal fast breeder reactor and accessories. UNIT V NUCLEAR POLLUTION AND ACCIDENTS 10 hrs. Nuclear radiation and Thermal pollution by nuclear power plants, Radio-active pollution of environment by nuclear power plants, nuclear accidents and radio-active waste disposal. TEXT/REFERENCE BOOKS: 1. Samuvel Glasstone, "Nuclear Reactor Engineering" 2nd Edition, Tata McGraw Hill, 2002. 2. Arora and S. Domkundwar, "Power Plant Engineering", 3rd Edition, Dhanpat Rai & Sons, 2002. 3. Singhai D.K., Fundamentals of Nuclear Power Engineering, 2nd Edition, Khanna Publishers, New Delhi, 2006 UNIVERSITY EXAM QUESTION PAPER PATTERN Max. Marks: 80 Exam Duration : 3 hrs Part A: 2 Questions from each unit, each carrying 2 marks 20 marks Part B: 2 Questions from each unit with internal choice, each carrying 12 marks 60 marks B.Tech. (CHEMICAL ENGINEERING) 71 REGULATIONS 2010