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Name of Examination B.Sc (Hons) Part-I B.Sc (Hons) Part-II B.Sc (Hons) Part-III B.Sc (Hons) Part-IV Examination year Session 2006 2007 2008 2009 20052006 20062007 20072008 20082009 The B. Sc (Hons) Examination in Chemistry shall consist of the i) DEPARTMENT OF CHEMISTRY FACULTY OF SCIENCE THE UNIVERSITY OF RAJSHAHI B.Sc (Hons) Part - I Examination of 750 marks (9.5 units, 38 credits) at the end of the 1st academic year; ii) B.Sc (Hons) Part - II Examination of 750 marks (9.5 units, 38 credits) at the end of the 2nd academic year; ii) B.Sc (Hons) Part-III Examination of 850 marks (10.5 units, 42 credits) at the end of the 3rd academic year; iv) B.Sc (Hons) Part-IV Examination of 850 marks (10.5 units, 42 credits) at the end of the 4th academic year. Syllabus for the degree of Bachelor of Science with Honours [B. Sc (Hons)] in Chemistry Examination - 2009 For obtaining B. Sc (Hons) degree in Chemistry a student shall have to take Chemistry courses of 2600 marks, Mathematics courses of 300 marks and Physics or Applied Physics & Electronics courses of 300 marks, distributed in four academic years. The Chemistry courses are represented by the prefix ‘Chem-’ followed by a 3 (three) digit number of which the central digit has the following significance: 0 (general), 1 (Physical), 2 (Organic) and 3 (Inorganic) Chemistry. The first and the last digits of the course number represent the Honours year and the sectional course number; A, V and L at the end of the course number represent the class assessment, the Viva-voce, and for the laboratory courses, respectively. The letters F or H indicate a full or a half unit course. The courses of Mathematics, Physics and Applied Physics & Electronics are represented by the prefix ‘Math-’, ‘PH-’ and ‘APE’ respectively. DEPARTMENT OF CHEMISTRY B. Sc (Hons) Part – I Examination, 2006 Session: 20052006 The courses and distribution of marks are as follows: Courses Title Units Credits Marks Course Chem-101AH (class assessment) includes tutorial, terminal, home assignment and /or class examinations on theoretical courses by the relevant course teacher(s) and attendance* of the students in the classes during the academic year. Class assessment comprises (a) 80% marks in tutorial, terminal, home assignment and /or class examinations and (b) 20% marks for attendance in the class. The class teacher of each course shall submit the average consolidated marks of class assessments and attendance in sealed envelope to the Chairman of the relevant examination committee within three weeks from the last class held. The relevant examination committee shall prepare the result by taking the average marks of class assessments as submitted by the class teachers of all the courses, and send a copy of the average consolidated marks to the controller of examinations. 0.5 1.0 2 4 50 75 Chem-121F General Chemistry – I States of Matter, Thermodynamics and Phase Equilibria Organic Chemistry – I 1.0 4 75 Chem-131F Chem-101AH Inorganic Chemistry – I Class Assessment-I 1.0 0.5 4 2 75 50 Chem-101VH Chem-101L Viva-voce in Chemistry-I Practical Chemistry –I 0.5 1.0 2 4 50 75 Viva-voce examination (Chem-101VH) includes the assessment of the students through oral examination (of all the courses) by the members of the relevant examination committee. The examination committee shall send a copy of the marks to the controller of examinations. PH-111F or APE-111F Mechanics, Properties of Matter & Sound or Mechanics, Heats & Optics Electricity & Magnetism or Electricity & Magnetism Algebra, Trigonometry & Vector Differential & Integral Calculus 1.0 4 75 * No student having less than 60% class attendance shall be allowed to sit for the examination. Chem-101H Chem-111F PH-112F or APE-112F Math-112F Math-115F Total 11 Courses 1.0 4 75 Course : Chem-101H General Chemistry - I Examination - 3 hours 1.0 1.0 4 4 75 75 (Full Marks : 50 (0.5 unit, 2 credit) 50 lectures, two lectures per week, total 25 weeks 9.5 38 750 1. Chemical calculations (7 Lectures): Units, dimensions and standards; SI units, conversion of units, uncertainties in measurements, significant figures and rounding off numbers with some calculations, scientific notation, plotting of data, slope and intercept of a linear plot. Gram atomic and gram molecular weights, gram equivalent weight of an acid, base and salt. Concentration units: normal, molar, and formal solutions, molality and mole fraction, percentage and ppm, practice exercises of molar unit. 2. The gaseous state and the kinetic molecular theory (5 Lectures): Characteristics of gases, the gas laws, the ideal gas equation, evaluation of R. Partial pressure, pressure of gases collected over water, the kinetic theory of gases, different kind of velocity mean free path. Diffusion and effusion of gases, gas density and molecular weight, heat capacity of gases and the principle of equipartition of energy. 3. Chemical equilibrium (5 Lectures): Reversible reactions, law of mass action, different forms of equilibrium constants, Le-Chatelier’s principle, effect of pressure, temperature, concentration and addition of inert gas on the position of equilibrium, some industrial applications of the principle. Of the four PH and APE courses, students are required to take either two PH or two APE courses. Examination of the theory courses of 75 marks (1.0 unit, 4 credit) shall be of 4 (Four) hours duration, of 50 marks (0.5 unit, 2 credit) 3 (three) hours duration and of the practical course of 75 marks (1.0 unit, 4 credit) shall be of 18 (eighteen) hours duration (3 days). Marks of the practical course (Chem-101LF) include 25 marks for continuous Lab. assessment. The students are required to submit a report after each practical class to the class teacher(s) for evaluation. After evaluation the report shall be returned to the students. The class teacher(s) shall submit the average marks of all Lab. evaluation in sealed envelopes to the chairman of the relevant examination committee within three weeks from the last class held. The examination committee shall send a copy of each of the consolidated practical and lab. Evaluation marks to the controller of examinations. 4. Bonding and energy changes (6 Lectures): Covalent bond ( and bond), bond length, bond energy, hybridisation of orbitals; sp, sp 2 and sp3 orbitals, heat of reaction, heat of hydrogenation, heat of combustion, energy changes during a reaction, energy of activation, progress of reaction, transition state and intermediates. 5. Detection of elements and functional groups (5 Lectures): Criteria of purity and calculation of formula of organic compounds, determination of degree of unsaturation, detection of elements and functional group analysis of organic compounds and their reactions. 6. Isomerism (5 Lectures): Classification, optical isomerism due to one/two chiral centres. Enantiomers, diastereomers and meso compounds, cistrans isomerism and their nomenclature. 7. Principles of qualitative inorganic analysis (7 Lectures): Solubility and solubility product, common ion effect and their application in the precipitation reactions, analytical group classification of metal ions. Principles and reactions involved in the detection of acid radicals, interfering radicals and their separation. 8. Theories of acids and bases (5 Lectures): Arrhenius, protonic, Lewis and Usanovich concepts of acids and bases, pH and buffer solution, hydrolysis of salts, indicators. 9. Chemical hazards (5 Lectures): Hazardous materials, disposal of hazardous materials with special reference to H2S gas, HCl fume, HNO3 fume, lead, arsenic, benzene and carbon tetrachloride. Recommended Books: 1. Darrell D. Ebbing 2. H. Anderson 3. D.A. Mc Quarrie & P.A. Rock 4. Paul Ander & A.J. Sonnessa 5. P.W. Atkins 6. R.T. Morison and R.N. Boyd 7. I.L. Finar 8. A. I. Vogel 9. O.D. Tyagi & M. Mehra : : : : : : : : : General Chemistry Chemical Calculations General Chemistry General Chemistry Elements of Physical Chemistry Organic Chemistry Organic Chemistry, Vol. 1 Inorganic Qualitative Analysis A Textbook of Environmental Chemistry ------------- Course: Chem-111F States of Matter, Thermodynamics and Phase Equilibria Examination - 4 hours Full Marks: 75 (1 unit, 4 credit) (60 lectures, 3 lectures per week, total 20 weeks) 1. The gaseous state (real gases) (14 Lectures): Ideal gas equation and its presure-volume behaviour, pressure-volume behaviour of real gases and the causes of deviation from the ideal gas equation. van der Waals’ equation and its limitations, other equations of state, virial equation. Behaviour of gases near liquefaction temperature, critical phenomena, continuity of state, law of corresponding state and the reduced equation of states, liquefaction of gases. 2. The liquid state (16 Lectures): Liquid vs. gases and solids, liquid-vapour equilibrium, molecular interpretation of vapour pressure. Boiling point, critical temperature and the heat of vaporization (Trouton’s law), Craft’s rule, surface tension of liquids and molecular interpretation of surface free energy, temperature dependence of surface tension and parachor, determination of surface tension, wetting characteristics of liquids. Viscosity and viscosity coefficient, flow of liquid through a narrow tube, measurement of viscosity coefficient, effect of temperature and pressure on viscosity, molecular interpretation of viscosity and rheochor, factors affecting the viscosity of a liquid, viscosity of liquid mixtures, refractive index, optical activity. 3. Thermodynamics and thermochemistry (20 Lectures): Scope and limitations of thermodynamics, state, system and surrounding, properties of thermodynamic functions, IUPAC convention for sign of work and heat, the first law of thermodynamics, reversible and irreversible processes, isothermal and adiabatic changes, enthalpy and its temperature dependence, Joule-Thompson effect. Thermochemistry: Thermochemical laws and thermochemical calculations, different types of heat of reaction, Kirchhoff’s equation, bond enthalpy. 4. The phase equilibria (10 Lectures): Phase, components and degrees of freedom, conditions of equilibrium in a heterogeneous system, phase rule and phase diagram. One component system: water, CO 2 and sulphur systems, enantiotropy and monotropy, phosphorous system. Recommended Books: 1. Darrell D. Ebbing 2. P.W. Atkins 3. N. Kundu and S.K. Jain 4. Klotz and Rossenberg 5. B.H. Mahan 6. P.W. Atkins 7. K.L. Kapoor : : : : : : : General Chemistry Physical Chemistry Physical Chemistry Chemical Thermodynamics Elementary Chemical Thermodynamics Elements of Physical Chemistry Physical Chemistry Vol. I Course : Chem-121F Organic Chemistry-I Examination - 4 hours Full Marks : 75 (1 unit, 4 credit, 60 lectures) 1. Aliphatic Hydrocarbons: (i) The alkanes (paraffins) (6 Lectures): Structure, conformation of ethane and butane, nomenclature, preparations and reactions, photo-chemical halogenation with mechanism (free radical mechanism). Recommended Books: 1. 2. 3. 4. 5. 6. 7. (iv) The cycloalkanes (alicyclic compounds) (8 Lectures): Nomenclature, preparations, reactions. Baeyer strain theory; SachseMohr modification, conformation of alicyclic compounds, angle strain, torsional strain, Vander Waals strain. 2. Aromatic Hydrocarbons (10 Lectures): Nomenclature, structure of benzene (Kekule structure, resonance structure, M.O. structure), aromaticity (Huckel rule), mechanism of electrophilic aromatic substitution: halogenation,nitration, sulphonation, Friedel-Crafts alkylation and acylation. Orientation in benzene ring in its derivatives, activation and deactivation in aromatic di-substitution. 3. Halides (8 Lectures): Nomenclature, preparation, halide exchange. SN2 and SN1 mechanism; reactions, general SN2 reactions of halides, the Grignard reagent, quat. ions. 4. Alcohols and Phenols (10 Lectures): Nomenclature, classification (1°/2°/3° and mono-di-trihydric), preparations, reactions, association (hydrogen bonding) of alcohols, test of alcohols, distinction between different types of alcohol, preparation and reactions of phenols. 5. Ethers and Epoxides (4 Lectures): Nomenclature, preparation and reaction. Sulfur analogues of ethers, sulfides, crown ethers, host-guest interaction. : : : : : Organic Chemistry Organic Chemistry, Vol. I Organic Chemistry A Textbook of Organic Chemistry Organic chemistry, Vol. I : A Textbook of Organic Chemistry : Organic Chemistry ----------------- (ii) The alkenes (olefins) (10 Lectures): Structure, nomenclature, preparations, reactions, mechanism of addition to double bonds. Regioselective reactions: E1 & E2 reactions, Markownikoff and antiMarkownikoff addition; the peroxide effect; oxidation and reduction of olefins. (iii) The alkynes (acetylenes) (4 Lectures): Structure, nomenclature, preparations, reactions, and mechanisms, acidity of alkynes. R. T. Morrison and R.N. Boyd I.L. Finar J.D. Roberts and M.C. Casserio B.S. Bahl and Arun Bahl S.M. Mukherjee, S.P. Singh & R.P. Kapoor Raj K. Bansal R.J. Fessenden & J.S. Fessenden Course : Chem-131F Inorganic Chemistry-I Examination - 4 hours Full Marks : 75 (1 unit, 4 credit, 60 lectures) 1. Atomic Structure (8 Lectures): Fundamental particles, nuclear charge, atomic spectra, Bohr atomic model, four quantum numbers, distribution of electrons in atoms, Pauli exclusion principle, Hund’s rule of maximum multiplicity. 2. Atomic Spectra (9 Lectures): Spectroscopic levels in multielectronic system, term multiplicities, Russel-Saunder's coupling, spectra of higher elements, fine structure of spectral lines. 3. Basic Quantum Mechanics (9 Lectures): Dual nature of electromagnetic radiation, black body radiation, photoelectric effect and compton effect, particle and wave nature of electron; de Broglie relation; Heisenberg uncertainty principle; preliminary idea about orbitals; physical significance of s,p and d orbitals. 4. Chemical Bonding (12 Lectures): Covalent bond; formation of hydrogen molecule, potential energy diagram and its interpretation; sigma- and pibonds; bond energy, bond length and bond angle; ionic characteristics of covalent bond; polarity of bonds and electric dipole moments; the concept of hybridization of bond orbitals. Fundamental ideas of the Molecular Orbital Theory (MOT); electronic configurations of simple molecules in terms of MO concept -- such as He2, N2, O2, F2, HF, CO and NO. 5. Periodic Table (12 Lectures): Periodic law, classification of elements, modern periodic table in the light of electronic configurations of elements, different types of elements, periodic properties, atomic, covalent and ionic radii, ionization potential, electronegativity, electron affinity, effective nuclear charge. 6. Oxidation-reduction Reactions (10 Lectures): Combination, decomposition, displacement and complicated types of reactions, oxidation number, method of balancing redox reactions, ionic representation of the equations of redox reaction, redox potential, electrochemical series and its application in oxidation-reduction reactions. Recommended Books: 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. F.A. Cotton and G.Wilkinson J.E. Huheey : Basic Inorganic Chemistry : Inorganic Chemistry: Principles of Structure and Reactivity H.V. Anderson : Chemical Calculations D.K. Sabera : Electronic Structure and Chemical Bonding. W.L. Jolly : Principle of Inorganic hemistry B.R. Puri and L.R. Sharma : Principles of Inorganic Chemistry S.Z. Haider : Modern Inorganic Chemistry M.C. Day and J. Selbin : Theoretical Inorganic Chemistry Satya Prakash, Tuli, Basu and Madan : Advanced Inorganic Chemistry Manas Chanda : Atomic Structure and Chemical Bond Course : PH-111F Mechanics, Properties of matter and Sound Examination - 4 hours Full Marks: 75 (1 unit, 4 credit, 60 lectures) (Three lectures per week; total: 20 weeks) 4. Oscillatory Motions: Hooke’s law and vibration; simple harmonic motion; combination of harmonic motions; damped harmonic motion; forced oscillation and resonance. 5. Gravitation: Center of gravity of extended bodies; gravitational field, potential and their calculations; escape velocity. 6. Surface Tension: Surface tension as a molecular phenomenon; surface tension and surface energy; capillary rise or fall of liquids; pressure on a curved membrane due to surface tension. 7. Elasticity: Moduli of elasticity, Poisson’s ratios; relations between elastic constants and their determination; cantilever. 8. Fluid Dynamics: Viscosity and coefficient of viscosity, Poiseuille’s equation; Bernoulli’s theorem and its applications, Torricell’s theorem; venturimeter. Recommended Books: 1. 2. 3. 4. 5. 6. 7. 8. 9. Vector Analysis: Vectors and scalars; addition and multiplication of vectors; triple scalar and vector products; derivatives of vectors; gradient, divergence, and curl and their physical significance. 2. Conservation of Energy and Linear Momentum: Conservative and non-conservative forces and systems; conservation of energy and momentum; center of mass. 3 Rotational Motions: Rotational variable; rotation with constant angular acceleration; relation between linear and angular kinematics; torque on a particle; angular momentum of a particle; kinetic energy of rotation and moment of inertia; combined translational and rotational motion of a rigid body; conservation of angular momentum. : : : : : : : : : Mechanics and Properties of Matter Theoretical Physics (part I) General Properties of Matter Physics ( I and II) General Physics Elements of Properties of Matter General Properties of Matter Vector Analysis Mechanics Group B : Sound (Marks : 25) 1. Wave in Elastic Media: Mechanical waves; types of waves, superposition principle, wave velocity; power and intensity in wave motion; interference of waves; complex waves; standing waves and resonance. 2. Sound Waves: Audible, ultrasonic, and infrasonic waves; propagation and speed of longitudinal waves; vibrating systems and sources of sound; beats; Doppler Effect. Group A : Mechanics & properties of Matters (Marks: 50) 1. Ahmed and Nath Constant Emran, et al Halliday and Resnick Haque Mathur Newman and Searle Spiegel Symon Recommended books: 1. 2. 3. 4. 5. Halliday and Resnick Emran Coulson Saha Wood : : : : : ------------- Physics (I and II) Textbook of Sound Waves Textbook of Sound Textbook of Sound Course : PH-112F Electricity and Magnetism Examination - 4 hours Course : Math-112F (Algebra, Trigonometry & Vector) Examination - 4 hours Full Marks : 75 (1 unit, 4 credit, 60 lectures) (Three lectures per week. Total : 20 weeks) Full Marks : 75 (1 unit, 4 credit, 60 lectures) (Three lectures per week; Total : 20 weeks) 1. Electrostatistics: Electric dipole: electric field due to a dipole, dipole on external electric field, Gauss’s law and its applications. 1. 2. Capacitors: Parallel plate capacitors with dielectrics, dielectrics and Gauss’s law, susceptibility, permittivity and dielectric constant, energy stored in an electric field. 2. 3. Electric Current: Electron theory of conductivity, conductor, semiconductors and insulators, superconductors, current and current density, Kirchhoff’s law and its applications. 4. Magnetism: Magnetic dipole, field due to a dipole, mutual potential energy of two small magnets, magnetic shell, energy in a magnetic field, magnetometers. 5. Electromagnetic Induction: Faraday’s experiment, Faraday’s laws, Ampere’s law, motional e.m.f., self-and mutual inductance, galvanometers - moving cell ballistic and deadbeat types. 6. Thermoelectricity: Thermal e.m.f., Seebeck, Peltier and Thomson effects, laws of addition of thermal e.m.f., thermoelectric power. 7. DC and AC circuits: DC circuits with LR, RC, LC and LCR in series, AC circuits with LR, RC, LC and LCR in series. 8. AC and DC meters: Ammeter, voltmeter, ohmmeter, watt meter, frequency meter, AC/DC bridge, digital voltmeter. Recommended Books: 1. Acharyya 2. Admas and Page 3. Constant 4. Din 5. Emran et al. : : : : : 6. 7. : : Halliday and Resnick Kip Electricity and Magnetism Principles of Electricity Theoretical Physics Electricity and Magnetism Textbook of Magnetism, Electricity and Modern Physics Physics (I & II) Fundamentals of Electricity and Magnetism ------------ 3. 4. 5. 6. 7. (a) Algebra of sets: De Morgan’s rule, relation & function. (b) Determinants: Properties and Cramer’s rule. Theory of equations: (a) Theorems and relation between roots and coefficients. (a) De Moiver’s theorem; (b) Deduction from De Moiver’s theorem. (a) Functions of complex arguments ; (b) Gregory’s series. (a) Summation of series. (b) Hyperbolic functions. Vector addition, multiplication & differentiation. Vector differential operator - grad., div. and curl. Recommended Books: 1. 2. 3. 4. 5. 6. 7. Barnside and Panton Bernard and Child Hall and Knight Das and Mukherjee M.A. Sattar M.R. Spiezel M.A. Sattar : : : : : : : -------------------- Theory of Equations Higher Algebra Higher Algebra Higher Trigonometry Higher Trigonometry Vector Analysis Vector Analysis Course : Math -115F Differential & Integral Calculus Examination - 4 hours Full Marks : 75 (1 unit, 4 credit, 60 lectures) (Three lectures per week, Total : 20 weeks) 1. 2. 3. Functions: Domain, range, inverse function and graphs of functions; limits, continuity and indeterminate form. Ordinary differentiation: Differntiability, differentiation, successive differentiation and Leibnitz theorem. (a) Expansions of functions: Rolle’s theorem, mean value theorem, Taylor’s and Maclaurin’s formulae. (b) Maximum and minimum of functions of one variable. 4. 5. 6. 7. (a) Partial differentiation: Euler’s theorem, tangents and normals ; (b) Asymptotes. Indefinite Integrals: Method of substitution, integration by parts, special trigonometric functions and rational fractions. Definite Integrals: Fundamental theorem, general properties, evaluation of definite integrals and reduction formulae. Multiple Integrals: Determination of length, areas and volumes. The total marks for the practical course shall be obtained by adding the above two marks (i) & (ii). The examination committee shall send a copy of the consolidated marks to the controller of examinations. Section A : Physical Chemistry Practical 1. Recommended books: 1. 2. 3. 4. 5. 6. 7. Ayres Das and Mukherjee Das and Mukherjee Edwards Williamson Muhammad and Bhattacherjee Muhammad and Bhattacherjee : : : : : : : Calculus Differential Calculus Integral Calculus Differential Calculus Integral Calculus Differential Calculus Integral Calculus 2. 3. 4. 5. ------------6. Course : Chem-101L (Chemistry Practical-I) Examination - 18 hours (63) Full Marks : 75 (1 unit, 4 credit) Section A: Physical Chemistry Practical Section B: Organic Chemistry Practical Section C: Inorganic Chemistry Practical (i) Experiment: 50* (Section : A+B+C), (ii) Continuous Lab. Assessment: 25** (Section : A+B+C) * The examiners in all the three sections shall assess the experiment(s) out of 50 marks and submit them to the chairman of the relevant examination committee. Average marks shall be computed by dividing the total marks of three sections by three. ** The relevant teachers of the three sections shall evaluate continuously the Lab. classes out of 25 marks and submit the average marks of Lab. evaluation in sealed envelopes to the Chairman of the relevant examination committee within three weeks from the last Lab. held. The average marks shall be computed by the examination committee. 7. 8. 9. 10. 11. 12. 13. (a) Laboratory procedures, safety regulations, scientific notations, plotting of data and finding of slope and intercept. (b) Significant figures, rounding off numbers and practice exercises for the use of calculator. Determination of formula and composition of a suitable hydrate. (CuSO 4, 5H2O; NiSO4, 7H2O; CoCl2, 6H2O). Studies on the (i) stoichiometry of the lead nitrate and potassium chromate system, (ii) decomposition of the metal halate (KClO3). Determination of empirical formula of copper sulphide. Determination of the molecular weight of a suitable (a) monobasic and (b) dibasic salt of organic acids by chemical method. Mass and density measurements: (a) Determination of the density of a solid by (i) dimensional and (ii) water displacement (Archimedes’ principle) method. (b) Determination of the density of a liquid / solution by (i) Finagles, (ii) density bottle / pycnometer method. (c) Measurement of density of solution at different molar concentration and determination of the unknown concentration of a solution. Calibration of volumetric apparatus, viz. pipette, burette, measuring flask, etc. Determination of molar volume of hydrogen gas at S.T.P. Determination of the molar gas constant R Determination of the molar masses of hexane and cyclohexane by Dumas method / Victor Mayers’s method. Determination of the coefficient of viscosity of a liquid/solution by Ostwald’s viscometer method. Measurement of the coefficient of viscosity of Urea solution at different concentrations and determination of the unknown concentration of a given solution. Thermochemistry : (a) Determination of the heat capacity of a supplied calorimeter and measurement of the heat of solution of inorganic salts in water (NaOH / KNO3 in H2O) (b) Determination of the heat capacity of a supplied calorimeter and measurement of the heat of neutralization of an aq. strong acid with an aq. strong base. (aq. HCl+aq. NaOH) (c) Determination of the heat capacity of a supplied calorimeter and measurement of the heat of neutralization of an aq. strong acid with solid strong base. (HCl aq. + NaOHs) and verification of the Hess’s law. (d) Determination of the heat of formation of magnesium oxide. NB: A few more experiments, relevant to the theoretical courses may be done, subject to the availability of the Lab. facilities. Section B: Organic Chemistry Practical Systematic identification of organic compounds: i) Determination of melting point of solid and boiling point of liquid organic compounds. ii) Detection of N, S and halogens in organic compounds. iii) Solubility test and classification of the compound. iv) Identification of functional groups : primary amine, secondary amine, substituted amide, nitro, simple amide and imide, carboxylic, phenolic, carbonyl, aromatic hydrocarbon. etc.; preparation of derivative, conclusion, naming of the compound / structure of compound. Identification of the compound under investigation should be systematic. Section C: Inorganic Chemistry Practical Inorganic qualitative analysis (semi-micro/macro method of analysis) : Systematic qualitative analysis of a mixture of compounds containing not more than four radicals, of which there shall not be more than three basic radicals and more than two acid radicals. i) Basic radicals: Silver, lead, mercury, bismuth, copper, cadmium, tin, arsenic, antimony, iron, aluminium, chromium, manganese, zinc, cobalt, nickel, calcium, barium, strontium, magnesium, potassium, sodium and ammonium. ii) Acid radicals: Carbonate, sulphite, sulfide, sulphate, nitrate, nitrite, chloride, bromide, iodide, phosphate and borate. Recommended Books: 1. D.P. Shoemaker et al 2. G.S. Weiss et al 3 A. Findlay 4. R.C. Das 5. J.N. Gurtu 6. K.K. Sharma 7. J.C. Muhler et al 8. J. Rose 9. J.B. Yadav 10. Newcomb, wilson et al 11. Daniels et al 12. Brennan et al 13. S.R. Palit 14. C.D. Hodgman et al 15. R.C. West et al 16. L.A. Lange 17. A.I. Vogel 18. 19. 20. 21. 22. 23. : : : : : : : : : : : : : : : : : Experiment in Physical Chemistry Experiments in General Chemistry Practical Physical Chemistry Experimental Physical Chemistry Advanced Experimental Chemistry An Introduction of Practical Chemistry Introduction to Experimental Chemistry A Textbook of Practical Physical Chemistry Advanced Practical Physical Chemistry Experiments in Physical Chemistry Practical Physical Chemistry Experiments in Physical Chemistry Practical Physical Chemistry Handbook of Chemistry and Physics CRC Handbook of Physics and Chemistry Handbook of Chemistry Elementary Practical Organic Chemistry, Part-1, Small Scale Preparation A.I.Vogel : A Textbook of Practical Organic Chemistry Shriner, Fusion and Curtin : The Systematic Identification of Organic Compounds. A.B. Garrett, H.H. Sisler, : Semimicro Qualitative Analysis J. Bonk and R.C. Stoufer A.I. Vogel : Inorganic Qualitative Analysis L.J. Curtman : Semi-micro Qualitative Chemical Analysis Gilreath : Inorganic Qualitative Analysis.