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DEGREE COURSE IN CHEMISTRY Academic Year 2003/04 INDEX General Structure Socrates/Erasmus Coordinator Description of the Degree Course List of the Courses Programs of the Courses General Structure The degree course in Chemistry has changed its structure from a five years Course (code F11) to a two levels scheme: a first level degree of three years (Laurea in Chimica, code F45) with a program of basic studies, and a second level degree of specialisation studies of two years (Laurea Specialistica in Scienze Chimiche) . With regard to proficiency, the credits have been introduced, with one credit being equivalent to 25 hours of student activities, according to the following scheme: - 8 hours of lesson, plus 17 hours of individual study - 16 hours of laboratory activity, plus 9 hours of individual study - 25 hours of practical training or preparation for the final thesis. The minimum number of credits to be acquired for the first level degree is 180. Other 120 credits are required to reach the second level degree. The academic year is organised in two semesters: the first one starts the 29 th of September 2003 and terminates the 16th of January 2004, the second one starts the 1 st of March 2004 and terminates the 4th of June 2004. Socrates/Erasmus Coordinator Prof. Gian Franco Tantardini Dipartimento di Chimica Fisica ed Elettrochimica Via Golgi 19 - 20133 Milano Tel: +39 02 50314278 Fax +39 02 50314300 E-mail address: [email protected] Description of the Degree Course Academic Requirements The admission to the courses of the first level degree is open to all students graduated from any High School Course. The admission of foreign students intending to follow the entire Chemistry Course at the University of Milan, is as well fully open, provided they pass a test foreseen to ascertain their knowledge of Italian language. Requirements for Socrates/Erasmus Students Socrates/Erasmus students who intend to follow courses for one or more semesters are accepted without any formal examination. The only requirement is that they are registered at their home University and that their home University guarantees recognition of the studies performed at the Milan University. Teaching Methods All courses of the first level degree are mainly composed of lectures, but many of them include exercises and/or laboratory practice. The official language is Italian, however particular assistance is given to incoming Erasmus/Socrates students, so that they can attend the lessons. Assessment Methods Each course has a final examination. The assessment is oral for most of the courses, although written or practical exercises are requested for some courses. In certain cases, teachers submit to students some written tests during the semester. Local Grading System The local grading system, as in all the Italian Universities, is expressed in fractions of 30, with a minimum of 18/30 to pass the examination. The best grade is 30/30 with honour. List of the Courses FIRST LEVEL DEGREE (LAUREA) 1st YEAR First semester Code F45001 F45002 F45002 F45003 Course Calculus General and Inorganic Chemistry Laboratory of General and Inorganic Chemistry Physics I Credits 9 7 5 7 Second semester Code F45004 F45004 F45005 F45005 F45007 F45008 Course Organic Chemistry I Laboratory of Organic Chemistry I Analytical Chemistry I Laboratory of Analytical Chemistry I Numerical Analysis Laboratory of Informatics Credits 7 5 7 5 5 3 2nd YEAR First semester Code F45009 F45009 F45010 F45010 F45011 Course Physical Chemistry I Laboratory of Physical Chemistry I Inorganic Chemistry I Laboratory of Inorganic Chemistry I Physics II Credits 7 5 7 5 7 Second semester Code Course Credits F45012 F45012 F45013 F45013 F45018 Analytical Chemistry II Laboratory of Analytical Chemistry II Organic Chemistry II Laboratory of Organic Chemistry II Safety and Legislation within Chemistry 6 4 7 5 6 3rd YEAR First semester Code F45015 F45016 F45017 F45017 F45018 Course English language test Quality Control Physical Chemistry II Laboratory of Physical Chemistry II Biological Chemistry Credits 3 6 7 5 7 Second semester Code F45019 Course Environmental Chemistry First Optional Course Second Optional Course Practical Training Final Test Credits 6 6 6 9 6 List of Optional Courses Code F44019 F45020 F45021 F45022 F45023 F45024 F45025 F45026 F45027 F45029 F46031 F45030 Course Methods of Structural Investigation of Inorganic Compounds Heterocyclic Chemistry Chemistry of Coordination Compounds Structural Chemistry Physical Chemistry (Complements) Computational Chemistry Theoretical (Quantum) Chemistry Electrochemistry Organic Chemistry (Applied) Chemistry of Natural Products Macromolecular Chemistry Physical Methods in Organic Chemistry Credits 6 6 6 6 6 9 6 6 6 6 6 6 SECOND LEVEL DEGREE (LAUREA SPECIALISTICA) 1st YEAR First semester Code Courses Calculus (Complements) A Course of Tab. 1 Informatics Pharmaceutical Chemistry or Mineralogy A Course of Tab. 2 Credits 5 9 3 4 6 Second semester Code Courses A Course of Tab. 1 Experimental Thesis Work (first part) Credits 9 25 Table 1 Code Courses Physical Chemistry (A) with Laboratory Physical Chemistry (B) with Laboratory Inorganic Chemistry (A) with Laboratory Credits 9 9 9 Sem. 1st 2nd 1st Inorganic Chemistry (B) with Laboratory Organic Chemistry (A) with Laboratory Organic Chemistry (B) with Laboratory Structural Characterization of Organic Compounds Environmental Analytical Techniques 9 9 9 6 6 2nd 1st 2nd 1st 1st Table 2 Code Courses Credits Physical Chemistry (Crystal Chemistry) 6 Physical Chemistry of Dispersed Systems and Interfaces 6 Physical Chemistry of Solid State and Surfaces 6 Theoretical Chemistry 6 Electrochemistry (Organic) 6 Photochemistry 6 Bioinorganic Chemistry 6 Inorganic Stereochemistry 6 Inorganic Chemistry (Applications) 6 Inorganic Chemistry (Complements) 6 Inorganic Chemistry (Crystal Chemistry) 6 Inorganic Chemistry (Reactivity of Organometallic Compounds) 6 Metallorganic Chemistry (Homogeneous Catalysis) 6 Solid State Chemistry 6 Advanced Techniques in Organic Synthesis 6 Bioorganic Chemistry 6 Chemistry of Organometallic Compounds 6 Advanced Physical Methods in Organic Chemistry 6 Organic Chemistry (Complements) 6 Environmental Electrochemical Techniques 3 Hydrogen Energy 3 Chemometrics 3 Supramolecular Chemistry (Synthesis) 3 Supramolecular Chemistry (Applications) 3 Industrial Organic Chemistry 3 Magnetic Resonances (Applications) 3 Food Chemistry and Quality of Life 3 Sem. 1st 2nd 2nd 2nd 2nd 1st 1st 2nd 1st 2nd 1st 1st 2nd 2nd 1st 1st 1st 1st 2nd 1st 2nd 2nd 2nd 2nd 2nd 2nd 2nd 2nd YEAR The 2nd year of the second level degree will be activated in the academic year 2004/05. In the academic year 2003/04, the 5th year of the old Laurea in Chemistry will be still active. Programs of the Courses First Level Degree - 1st YEAR Calculus (F45001) - lecturer: Stefania De Stefano - lectures with classroom exercises - 1st semester - credits: 9 Real numbers. Linear algebra: vectors and matrices, linear systems. Sequences and series. Functions of one variable. Differential calculus in one variable. Integral calculus in one variable Multivariate functions. Ordinary differential equations. General and Inorganic Chemistry (F45002) - lecturer: Sergio Cenini - lectures with classroom exercises - 1st semester - credits: 7 Atoms and their structure The chemical bond. The gaseous and solid states. Chemical thermodynamics. Liquid state and solutions. Chemical kinetics. Acids and bases. Electrochemistry. Coordination chemistry. Radiochemistry. Inorganic chemistry. Laboratory of General and Inorganic Chemistry (F45002) - lecturer: Fabio Ragaini - lectures with classroom exercises and laboratory experiments - 1st semester - credits : 5 The course is devoted to the solution of typical stoichiometric problems, such as determination of chemical formulas, titrations, homogeneous and heterogeneous equilibria, acid-base equilibria, electrochemical equations. Laboratory practice includes synthesis, purification and characterisation of simple inorganic compounds. Physics I (F45003) - lecturer: Michelangelo Fazio - lectures with classroom exercises - 1st semester - credits: 7 Physical quantities and their measurement. The International System. Error theory. Kinematics: Position and displacement vectors. Motion laws. Velocity and acceleration. Kinematic rotational quantities. Fundamental laws of dynamics. Collisions. Linear momentum. Energetics: work , kinetic and potential energy. Energy conservation principle. Simple harmonic motion. Dynamics of rigid bodies. Mechanics of fluids. Periodic motions. Waves. Wave propagation. General solution of the wave equation. Organic Chemistry I (F45004) - lecturer: Francesco Sannicolò - lectures with classroom exercises - 2nd semester - credits : 7 Chemical bonding in organic molecules. Organic reactions. Functional groups. Different classes of organic compounds. IUPAC nomenclature. Organic stereochemistry. Static and dynamic stereochemistry. Laboratory of Organic Chemistry I (F45004) - lecturer: Giovanna Speranza - lectures and laboratory experiments - 2nd semester - credits : 5 Laboratory safety. Organic characterisation procedures: determination of melting point, crystallization, extraction with solvents, simple and fractional distillation, thin layer and column chromatography, infrared spectroscopy, etc. Laboratory practice on some common organic reactions . Analytical Chemistry I (F45005) - lecturer: - lectures with classroom exercises - 2nd semester - credits : 7 The principles and practical applications of chemical analysis. Statistical evaluation of analytical data. Equilibrium in homogeneous and heterogeneous systems. Ox/redox systems. Gravimetric methods of analysis. Voltammetry. Electroanalytical methods (potentiometry and conductimetry). Laboratory of Analytical Chemistry I (F45005) - lecturer: Vittoria Guglielmi - lectures and laboratory experiments - 2nd semester - credits : 5 The practical application of quantitative analytical chemistry will cover the following topics: gravimetric methods of analysis; titrimetric methods of analysis (acid-base, redox, precipitation and complex formation). Separation by ion exchange chromatography. Dissolution and characterisation of an ore. Potentiometric and conductimetric methods. Numerical Analysis (F45007) - lecturer: Flavia De Tisi - lectures - 2nd semester - credits : 5 Errors. Operators. Equations, linear and non- linear systems. Approximation of functions. Numerical integration. Laboratory of Informatics (F45008) - lecturer: Anna Morpurgo - lectures - 2nd semester - credits : 3 Basic notions. First approach to the use of a computer . Computer networks. Internet applications. Data handling with Excel and Access. First Level Degree - 2nd YEAR Physical Chemistry I (F45009) - lecturer: Maurizio Sironi and Ermanno Gianinetti - lectures with classroom exercises - 1st semester - credits : 7 Basic principles of quantum theory. Electronic structure of atoms. Molecular structure and theories of the chemical bond. Molecular symmetry. Rotational, vibrational and electronic spectroscopy Laboratory of Physical Chemistry I (F45009) - lecturer: Silvia Ardizzone – lectures with classroom exercises - 1st semester - credits : 5 Chemical thermodynamics, with numerical exercises and laboratory experiments. Inorganic Chemistry I (F45010) - lecturer: Gianfranco Ciani - lectures - 1st semester - credits : 7 Atomic structure. Molecular symmetry and molecular shapes. Covalent bond. Molecular orbitals. Solid state and ionic bond. Systematic chemistry of the elements: hydrogen and its compounds, the Groups of B and C, the Groups of N and O, the halogens and noble gases. Coordination chemistry. Laboratory of Inorganic Chemistry I (F45010) - lecturers: Alessandro Ceriotti and Alessandro Pasini - lectures with classroom exercises and laboratory experiments - 1st semester - credits : 5 Acids and bases, the acidic and basic strength of different compounds in aqueous and non- aqueous solvents. Hard-soft theory. Basic notions on oxidation and reduction, stability of different oxidation states of the elements with different solvents. Systematic chemistry of s and p metals , magnetism in complexes. Theoretical aspects of the laboratory experiments, application of the principal synthesis techniques, separation and purification. Physics II (F45011) - lecturer: Lina Zuffi - lectures with classroom exercises –1st semester - credits : 7 Electricity. Magnetism. Electromagnetism. Relativity. Optics. Elements of quantum mechanics. Analytical Chemistry II (F45012) - lecturer: Silvia Bruni - lectures with laboratory experiments - 2nd semester - credits : 6 Techniques of elemental analysis (AAS, AES, XRF, MS). Techniques of molecular analysis (IR, Raman, UVVis, NMR, MS). Techniques of superficial analysis (photon and electronic probe, XRPD). Laboratory of Analytical Chemistry II (F45012) - lecturer: Gian Maria Zanderighi - lectures and laboratory experiments - 2nd semester - credits : 4 Instrumentation in analytical chemistry: generality on components, performances, signal and noise. Calibration of instrumental methods. Designs of optical instruments, characteristic of different components, signal processors and readout. Voltammetry. Chromatographic separation: gas chromatography, HPLC and supercritical fluid chromatography. Laboratory pratice concerns analytical application of potentiometry, conductometry, voltammetry, spectroscopy and chromatography. Organic Chemistry II (F45013) - lecturer: Bruno Danieli - lectures with classroom exercises - 2nd semester - credits : 7 Aminoacids , peptides and proteins. Carbohydrates. Carbocyclic aromatic compounds. Electrophilic and nucleophilic aromatic substitution. Aromatic polycondensate compounds. Heterocyclic compounds. Pericyclic reactions. Laboratory of Organic Chemistry II (F45013) - lecturer: Giordano Lesma - laboratory experiments - 2nd semester - credits : 5 Preparation of some aromatic and heteroaromatic compounds using multistep synthetic procedures. Safety and Legislation within Chemistry (F45018) - lecturer: - lectures - 2nd semester - credits : 6 First Level Degree - 3rd YEAR Quality Control (F45016) - lecturer: - lectures - 1st semester - credits : 6 Physical Chemistry II (F45017) - lecturer: Leonardo Formaro - lectures - 1st semester - credits : 7 Statistical thermodynamics. Electrostatic properties of molecules and of macroscopic bodies. Adsorption. Thermodynamics of solutions. Laboratory of Physical Chemistry II (F45017) - lecturer: Riccardo Destro - lectures and laboratory experiments - 1st semester - credits : 5 Chemical kinetics. Reaction mechanisms. Collision theory. Activated complex theory. Experimental study of the kinetics of four different reactions, with detailed treatment of the experimental data. Biological Chemistry (F45018) - lecturer: Renata Zippel - lectures - 1st semester - credits : 7 Study of the functions and properties of macromolecules, proteins, DNA and RNA; mechanisms governing the information flux from DNA to proteins, enzymatic mechanisms, some aspects of intermediate and energetic metabolism. Fundamental biochemical aspects for the technology of the recombinant DNA. Environmental Chemistry (F45019) - lecturer: Gian Maria Zanderighi - lectures - 1st semester - credits : 6 List of Optional Courses Methods of Structural Investigation of Inorganic Compounds (F44019) - lecturer: Piero Macchi - lectures - 2nd semester - credits : 6 Inorganic materials and their properties. Diffractometric characterisation of crystalline and non crystalline solids. Heterocyclic Chemistry (F45020) - lecturer: Piero Dalla Croce - lectures - 2nd semester - credits : 6 Nomenclature of heterocyclic compounds. Electronrich and electronpoor systems. Synthetic strategies and general reactivity. Exercises of synthesis of heterocyclic compounds. Chemistry of Coordination Compounds (F45021) - lecturer: Alessandro Ceriotti - lectures - 2nd semester - credits : 6 General aspects of complex chemistry, such as coordination geometries, types of ligands and their bonding modes, isomerism, stability, crystal field and molecular orbital theories and reaction mechanisms. Compounds with π ligands, and with Carbon, Nitrogen, Phosphorus, Oxygen and Sulfur ligands. Principal organometallic compounds. Structural Chemistry (F45022) - lecturer: Mirella Sansoni - lectures with classroom exercises - 2nd semester - credits : 6 Crystal symmetry: Point groups and space groups. Unit cell and crystal lattice. Diffraction of X-rays by crystals: theory, instrumentation and structural determinations. Physical Chemistry (Complements) (F45023) - lecturer: Emanuele Ortoleva – lectures and exercises - 2nd semester - credits : 6 Linear spaces and linear operators. Fourier series and Fourier transforms, and their applications in spectroscopy, crystallography and quantum mechanics. Partial differential equations: wave equations, diffusion equations, heat equations, Schroedinger equation. Computational Chemistry (F45024) - lecturers: Maurizio Sironi - lectures, classroom and computer exercises - 2nd semester - credits : 6 Modelling techniques for the study of structure and reactivity of molecules. Analysis of the electron density and of the electrostatic potential. The conformational analysis problem. Theoretical (Quantum) Chemistry (F45025) - lecturer: Ermanno Gianinetti - lectures with classroom exercises - 2nd semester - credits : 6 The foundations of the quantum mechanics. Approximate solution of the Schroedinger equation. The HartreeFock method for the study of the molecular electronic structures. Electrochemistry (F45026) - lecturer: Torquato Mussini - lectures with classroom exercises - 2nd semester - credits : 6 Electrochemical systems, electrolytes and electrolytic solutions, ion-solvent interactions, electrochemical equilibria and energetics, cell thermodynamics, membranes, ion selective electrodes and electroanalysis, electrochemical kinetics. Organic Chemistry (Applied) (F45027) - lecturer: Cesare Gennari and Carlo Scolastico - lectures - 2nd semester - credits : 6 Protection of functional groups. Reduction and oxidation reactions. Difunctionalised 1,2/1,3/1,4/1,5/1,6 compounds. Retrosynthetic analysis and synthesis strategy. Chemistry of Natural Products (F45029) - lecturer: Paolo Manitto and Carlo Morelli - lectures - 2nd semester - credits : 6 Primary metabolites (proteins, carbohydrates, etc.) and secondary metabolites (terpens, steroids, etc.), both from structural and biosynthetic profile. Macromolecular Chemistry (F46031) - lecturer: Paolo Ferruti - lectures - 2nd semester - credits : 6 Synthesis of polymers. Polycondensation and polyadditions. Chain, radical and ionic polymerisations. Copolymerisations. Degradation and stabilisation of polymers. Polymers in solution and determination of the molecular weights of polymers. Biomedical and pharmacological applications of polymers. Physical Methods in Organic Chemistry (F45030) - lecturer: Giordano Lesma - lectures - 2nd semester - credits : 6 The Nuclear Magnetic Resonance: pulsed techniques in NMR. One- and two-dimensional multipulsed NMR techniques. Parameters in NMR. The Mass Spectrometry: instrumental aspects of the MS. Supplemental structural information from each ion: MS-MS. The ionisation process of molecules and the theory of quasiequilibrium.