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Identification of Aldehydes and Ketones
Identification of Aldehydes and Ketones

... volumes of Fehling’s A and Fehling’s B solution in a 1:1 ratio immediately before use (usually 1 mL of each). Fehling’s A solution is an aqueous solution of copper sulfate pentahydrate (CuSO4.5H2O) with few drops of concentrated sulfuric acid. Fehling’s B solution is an aqueous solution of potassium ...
Direct organocatalytic enantioselective a-aminomethylation
Direct organocatalytic enantioselective a-aminomethylation

Convenient Methods for the Reduction of Amides, Nitriles
Convenient Methods for the Reduction of Amides, Nitriles

... pure ...
Document
Document

... So, the first stage can be viewed as both electrophilic substitution on the ring by the electron – deficient carbon of formaldehyde , and nucleophilic addition of the aromatic ring to the carbonyl group. ...
No Slide Title
No Slide Title

Chapter_Sixteen_lecture
Chapter_Sixteen_lecture

... • The reduction of a carbonyl group occurs with the addition of hydrogen across the double bond to produce an –OH group, a reaction that is the reverse of the oxidation of an alcohol. • Aldehydes are reduced to primary alcohols, and ketones are reduced to secondary alcohols. ...
7. Organic halides
7. Organic halides

... in reactivity from the larger cycloalkanes and acyclic alkanes. Cyclopropane exhibits easy ring opening (see p. 20) instead of substitution characteristic of alkanes. The reactivity of small rings results from their abnormal bond angle (Baeyer strain theory). In cyclopropane the internal bond angle ...
8.4 Weak Acids and Bases, Continued
8.4 Weak Acids and Bases, Continued

Aromatic Compounds
Aromatic Compounds

... Rings: The Friedel-Crafts Reaction Alkylation • The introduction of an alkyl group onto the benzene ring • Called the Friedel-Crafts reaction after its discoverers • Among the most useful electrophilic aromatic substitution ...
C - Deans Community High School
C - Deans Community High School

... pentan-1-ol on losing a molecule of water will form pentene. Two structures are possible. ...
Reactions of Alkenes
Reactions of Alkenes

... The protonation occurs at the least highly substituted end so that the cation produced is at the most highly substituted end (and therefore more stable). Markovnikov’s Rule: The addition of a proton acid to the double bond of an alkene results in a product with the acid hydrogen bound to the carbon ...
Alcohols phenols ethers
Alcohols phenols ethers

... The substitution of a hydrogen atom in a hydrocarbon by an alkoxy or aryloxy group (R–O/Ar–O) yields another class of compounds known as ‘ethers’, for example, CH3OCH3 (dimethyl ether). ethers as compounds formed by substituting the hydrogen atom of hydroxyl group of an alcohol or phenol by an alkyl ...
Chapter 1
Chapter 1

... • Fatty acids which can’t be synthesized by the body are essential fatty acids – Linoleic acid is an essential fatty acid required to make arachadonic acid ...
10.4 Alcohols 10.4 Alcohols
10.4 Alcohols 10.4 Alcohols

Review of Organic Chem II
Review of Organic Chem II

... 3. The types of intermediates involved (cation, anion, or radical) should be consistent with the reaction classification above a. If the reaction is cationic, don’t show anionic intermediates b. If the reaction is anionic, don’t show cationic intermediates 4. Usually conditions are ionic. 5. Use a r ...
synthetic approaches for quinoline and isoquinoline
synthetic approaches for quinoline and isoquinoline

... Quinoline  is  a  heterocyclic  aromatic  organic  compound.  It  has  the  formula  C9H7N  and  is  a  colourless  hygroscopic  liquid  with  a  strong  odour.Aged  samples,if  exposed  to  light,  become  yellow  and  later  brown. Quinoline  is only slightly soluble in cold water but  dissolves  ...
Ligand Exchange Chromatography
Ligand Exchange Chromatography

... discriminated by the action of a chiral selector only. The latter has to be involved in interaction with the enantiomers, resulting in the formation of adducts which, being diastereomeric species, may differ in their stability. These adducts in LEC are ternary complexes composed of the molecule of t ...
Word - icho39.chem.msu.ru
Word - icho39.chem.msu.ru

... P is the total pressure in the system. Taking into account (5), equation (4) can be written in a form: ...
Aldehydes Ketones Carboxylic Acid
Aldehydes Ketones Carboxylic Acid

Caboxylic acid Derivatives
Caboxylic acid Derivatives

... Acid Catalyzed Nucleophilic Acyl Substitution In the previous examples, a nucleophile attacked the carbonyl group to generate a tetrahedral intermediate. However some nucleophiles are too weak to directly attack the carbonyl group (especially in the less reactive acid derivatives). E.g. an alcohol ...
Chapter 12- Alcohols from Carbonyl Compounds, Redox Reactions
Chapter 12- Alcohols from Carbonyl Compounds, Redox Reactions

Catalytic asymmetric carbonyl addition reactions catalysed by group
Catalytic asymmetric carbonyl addition reactions catalysed by group

... Asymmetric reductive coupling of alkynes and aldehydes 10-12 Nickel-catalysed intermolecular reductive coupling (exclusive cis-addition) of aryl-C≡C-alkyl alkynes with aldehydes can be accomplished in the presence of a catalytic amount of the commercially available (+)-(neomenthyl)-diphenylphosphine ...
CHEM120 - ORGANIC CHEMISTRY WORKSHEET 1
CHEM120 - ORGANIC CHEMISTRY WORKSHEET 1

Pincer Complexes. Applications in Catalysis
Pincer Complexes. Applications in Catalysis

FEDERAL OPERATING PERMIT - TECHNICAL REVIEW SUMMARY
FEDERAL OPERATING PERMIT - TECHNICAL REVIEW SUMMARY

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Petasis reaction



The Petasis reaction (alternatively called the Petasis borono–Mannich (PBM) reaction) is the chemical reaction of an amine, aldehyde, and vinyl- or aryl-boronic acid to form substituted amines.Reported in 1993 by Nicos Petasis as a practical method towards the synthesis of a geometrically pure antifungal agent, naftifine, the Petasis reaction can be described as a variation of the Mannich reaction. Rather than generating an enolate to form the substituted amine product, in the Petasis reaction, the vinyl group of the organoboronic acid serves as the nucleophile. In comparison to other methods of generating allyl amines, the Petasis reaction tolerates a multifunctional scaffold, with a variety of amines and organoboronic acids as potential starting materials. Additionally, the reaction does not require anhydrous or inert conditions. As a mild, selective synthesis, the Petasis reaction is useful in generating α-amino acids, and is utilized in combinatorial chemistry and drug discovery.
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