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1214 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 15, NO. 5, OCTOBER 2006 Thin-Film Piezoelectric Unimorph Actuator-Based Deformable Mirror With a Transferred Silicon Membrane Eui-Hyeok (EH) Yang, Senior Member, IEEE, Yoshikazu Hishinuma, Jian-Gong Cheng, Susan Trolier-McKinstry, Senior Member, IEEE, Eric Bloemhof, and B. Martin Levine Abstract—This paper describes a proof-of-concept deformable mirror (DM) technology, with a continuous single-crystal silicon membrane reflecting surface, based on PbZr0:52 Ti0:48 O3 (PZT) unimorph membrane microactuators. A potential application for a terrestrial planet finder adaptive nuller is also discussed. The DM comprises a continuous, large-aperture, silicon membrane “transferred” onto a 20 20 piezoelectric unimorph actuator array. The actuator array was prepared on an electroded silicon substrate using chemical-solution-deposited 2-thick PZT films working in a d31 mode. The substrate was subsequently bulk-micromachined to create membrane structures with residual silicon acting as the passive layer in the actuator structure. A mathematical model simulated the membrane microactuator performance and aided in the optimization of membrane thicknesses and electrode geometries. Excellent agreement was obtained between the model and the experimental results. The resulting piezoelectric unimorph actuators with patterned PZT films produced large strokes at low voltages. A PZT unimorph actuator, 2.5 mm in diameter with optimized PZT/silicon thickness and design showed a deflection of 5.7 at 20 V. A DM structure with a 20-thick silicon membrane mirror (50 mm 50 mm area) supported by 400 PZT unimorph actuators was successfully fabricated and optically characterized. The measured maximum mirror deflection at 30 V was approximately 1 . An assembled DM showed an operating frequency bandwidth of 30 kHz and an influence function of approximately 30%. [1738] m m m m Index Terms—Deformable mirror, large-area mirror, PZT thinfilm, unimorph actuator. I. INTRODUCTION EQUIREMENTS on optical instrumentation for future astronomical observations from the ground and in space will place rigorous demands on wavefront quality. As an example, the Terrestrial Planet Finder (TPF) Mission [1] has sought to R Manuscript received January 1, 2006; revised February 20, 2006. This work was supported in part by the National Aeronautics and Space Administration. The work of J.-G. Cheng was conducted while he was with the Materials Research Institute, Pennsylvania State University, University Park, PA 16802 USA. Subject Editor N. F. de Rooij. E.-H. Yang is with Stevens Institute of Technology, Hoboken, NJ (e-mail: [email protected]). E. Bloemhof and B. M. Levine are with the Jet Propulsion Laboratory, Pasadena, CA 91109 USA. Y. Hishinuma is with the Fuji Photo Film Company, Ltd., Kanagawa 2588538, Japan. J.-G. Cheng is with the Shanghai Institute of Microsystem and Information Technology, Chinese Academy of Sciences, Shanghai 200050, China. S. Trolier-McKinstry is with the Materials Research Institute, Pennsylvania State University, University Park, PA 16802 USA. Digital Object Identifier 10.1109/JMEMS.2006.880208 Fig. 1. Large-area continuous membrane DM concept. The mirror membrane is backed by an array of piezoelectric unimorph microactuators. The advantage of this approach is that the small strains obtainable from a piezoelectric material at modest voltages are translated into relatively large displacements. image Earth-like planets orbiting in “habitable zones” around nearby stars and to characterize their atmospheres, if any, in the visible to infrared (IR) bands. The telescope is a two-mirror, off-axis Cassegrain. The coronagraph inside the thermal instrument enclosure requires wavefront correction over the full aperture of the primary mirror and a deformable mirror (DM) with a large number of actuators and low stroke, located at a conjugate surface. This task requires imaging with wavefront fidelity equivalent to the phenomenally high dynamic range of – , depending on the approach taken. Future groundbased observatories with 30–100-m apertures also seek to detect and characterize Earth-like exoplanets in addition to other very demanding observations [2]. Large-stroke actuators will be needed on the primary mirror in order to form an image. There may also be a DM in a conjugate plane to enable diffraction-limited imaging. Similarly, missions such as the Single Aperture Far-Infrared (SAFIR) Observatory [3] and associated interferometric missions [4] demand extreme wavefront quality at cryoK. The SAFIR telescope is conceived genic temperatures of as a larger and colder version of the segmented James Webb Space Telescope point-design. Wavefront correction will be on each of the segments instead of the conjugate plane. Because the wavelength range of this telescope is between 20 and 1 mm, 1057-7157/$20.00 © 2006 IEEE YANG et al.: THIN-FILM PIEZOELECTRIC UNIMORPH ACTUATOR-BASED DM 1215 Fig. 2. Unimorph actuator concept. An electric field applied perpendicular to the membrane-mounted piezoelectric thin film induces a contraction in the lateral direction, converted by the membrane geometry to a large out-of-plane deflection. The vertical deflection acts on the portion of the mirror membrane mounted over the microactuator. Piezoelectric unimorph actuators will provide: 1) large wavefront correction, with a highly localized influence function; 2) scalability, potentially up to 10 actuators; 3) fast response and low power (30 s=cycle, 4 nF); and 4) functionality over a wide temperature range. the actuators will need to have much larger stroke; however, there will be fewer of them than would be required on a visible wavelength telescope, for instance. Laser communication is another area of great current interest, and it too levies challenging requirements, not only on the wavefront quality but also on the speed at which the wavefront is corrected [5], [6]. For many of these applications, the availability of high-performance DMs will play a critical enabling role. Space-based planet finders like over TPF require residual wavefront errors of less than the full aperture [7]. Although SAFIR has no formal requirement for DM performance, its long wavelength range makes it likely that adaptive correction actuators operating at cryogenic temperatures will be integrated into the primary or secondary mirrors rather than a conjugate surface. This minimizes the number of optical surfaces in the beam train, thus reducing thermal background. Given the variety of applications relevant to astronomical observations and space operations, one sees there is no single ideal DM architecture. Electrostrictive lead magnesium niobate (PMN) actuators have achieved a surface stability of 1 and a surface figure of [8]. However, although these technologies are in widespread use, they have only limited acstroke at actuator tuator stroke (approximately 0.5 density, for PMN-based mirrors). Micromachined continuous membrane DMs have been fabricated [9]–[13]; however, such devices are based on electrostatic actuation and, conse. Currently, the quently, have limited mirror stroke large-aperture technology development being pursued under the Gossamer program has yet to demonstrate the potential for diffraction-limited wavefront quality over large apertures. We believe that our large-actuator-stroke device is well suited to correct the large wavefront errors associated with space-based telescope apertures. The unique approach of combining uni(PZT) actuator technology with morph mirror-quality membrane transfer technology [8] provides flexible capabilities in fabricating DM structures. Therefore, a class of DM architectures can be adapted to meet specific operating requirements. Part of the motivation for developing both the PZT unimorph DM and membrane transfer techniques is precisely because they are so adaptable. Our DM concept is shown in Fig. 1. For instance, the stroke of the DM and the density of actuators can be traded, that is, large stroke is obtained with larger actuator separation using our fabrication technology. With this in mind, our devices are fabricated with a very high-fidelity process for the transfer of the silicon face-sheet, which is grown on a separate wafer for superior optical quality. In this paper, we present the development results of thin-film PZT fabrication process, the PZT unimorph actuators, a proof-of-concept continuous membrane DM using the PZT actuators, and the membrane transfer process. We also discuss potential future application for a TPF adaptive nuller. II. PZT UNIMORPH ACTUATOR-BASED DM The DM described in this paper comprises a continuous membrane mirror supported by an array of PZT unimorph actuators. The unimorph actuation principle is illustrated in Fig. 2. The actuation principle details are as follows: an electric field applied perpendicular to the membrane-mounted PZT thin film induces a contraction in the lateral direction, converted by the membrane geometry to a large out-of-plane deflection. The vertical deflection acts on the mirror membrane that is mounted over the microactuator. Compared with the bulk piezoelectric or electrostrictive stack actuators widely employed in commercial DMs, thin films require far lower voltages and less power to produce the same mirror deflection. To avoid stress concentration which might induce cracking in the actuator, circular diaphragm elements were chosen. In order to optimize the geometry of the unimorph actuator structure, a mathematical model was developed using an energy minimization method [14]. In this model, the total energy of the unimorph membrane under deflection is calculated using a deflection profile predicted by thin plate deflection theory. Subsequently, the total energy, consisting of the elastic energy due to the bending of the membrane, the potential energy stored by the film stresses, and the work done by the piezoelectric actuation, is minimized with respect to a Lagrange multiplier. The detailed explanation of the mathematical modeling and the method of energy minimization are available in [15]. The energy minimization calculation was performed for both continuous and patterned piezoelectric films. 1216 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 15, NO. 5, OCTOBER 2006 III. FABRICATION AND CHARACTERIZATION Here, the fabrication and characterization processes are described. The membrane transfer process [8] is used to transfer a silicon membrane onto the PZT unimorph actuator array. Section III-A describes the PZT film development process including its fabrication and analysis. The actuator array is prepared on an electroded substrate using the chemical-solution-deposited PZT films. Section III-B describes the fabrication and characterization processes for the unimorph actuator arrays using the PZT film technology described in Section III-A. Section III-C describes the wafer-scale transfer process of single-crystal silicon mirror membranes onto the fabricated actuator array described in Section III-B, as well as the results of surface figure characterization for the mirror membrane. A. Thin Film PZT: Deposition and Characterization For this study, thin PZT films were prepared using a chemical solution deposition process. The procedure has been described in detail elsewhere [16]. Briefly, the procedure used was a modification of that first introduced by Budd et al. [17] for processing of PZT films thick. Lead acetate trihydrate, zirconium -propoxide, and titanium isopropoxide were used as the precursors, while 2-methoxyethanol (2-MOE) was the primary solvent. After dissolution, the lead precursor was dehydrated under vacuum. A mixture of zirconium -propoxide and titanium iso-propoxide in 2-MOE at room temperature was added and the entire solution was refluxed for 2 h under Ar at 120 . After a second vacuum distillation, 2-MOE was added. The solution was then modified with acetylacetone (20 vol%) and acetic acid (5 vol%). The final solution was 0.70M with 20mol% Pb in excess of stoichiometry to compensate for high Pb volatility. The substrates used in this study were /Si wafers (Nova commercially manufactured Pt(111)/Ti/ Electronic Materials, Inc., Richardson, TX) for electrical characterization and platinum-coated silicon on insulator (SOI) wafers for device fabrication. Prior to deposition of the PZT for 60 seconds film, substrates were pre-annealed at 500 to clean the surface. Solutions were dispensed through a syWhatman filter (Aldrich Chemical Co., ringe with a 0.1Milwaukee, WI) and the substrate was spun at 1500 rpm for 30 s using a photoresist spinner (Headway Research, Inc., Garland, TX). The majority of the organics were removed in two pyrolysis steps, each 60 s in duration, on a hot plate at and 500 , respectively. During the second treatment, 350 a 1-mm-thick aluminum plate was positioned parallel to and about 3.5 mm above the film surface to enhance heating. A crystallization anneal was performed after deposition of each layer in a Heatpulse 610 rapid thermal processing unit (AG for 60 s. Each sequence Associates, Sunnyvale, CA) at 700 produced a layer approximately 0.20 in thickness, and the sequence was repeated to obtain the desired film thickness. radiation was X-ray diffraction with Ni-filtered Cu performed to characterize the orientation and crystal structure of the PZT films (Scintag, Inc., Sunnyvale, CA). Microstructural features of the films were examined using an S-3500N scanning electron microscope (SEM) (Hitachi LtD., Tokyo, Fig. 3. SEM micrographs of (a) whole thickness and (b) part of a cross section of a PZT thick film. Japan). To enable electrical characterization, Pt/PZT/Pt capacitors were fabricated by sputtering Pt top electrodes through a shadow mask. The electrodes were circular with an area . Before measurement, the samples were of 1.3 for 1 min to improve the quality of the annealed at 500 film/top electrode interface. To expose the bottom electrode, a two-step wet etching process for PZT thick films was used [18]. The film thickness was measured using an Alpha-Step surface profilometer. The dielectric constant and loss tangent of the PZT films were measured using a HP4192A LF impedance analyzer (Hewlett-Packard, Palo Alto, CA) at 100 kHz and an . Polarization-electric field hysoscillation voltage of 30 teresis behavior of the PZT films was measured using an RT66A standardized ferroelectric test system (Radiant Technologies, Albuquerque, NM) in the virtual ground testing mode. Fig. 3 shows the SEM micrograph cross section of a 7- -thick PZT film. As seen in the cross-sectional micrographs, a boundary including some porosity is apparent between each crystallized layer, and layers appear to be one grain thick. Because each layer was crystallized separately, it is likely that the top surface YANG et al.: THIN-FILM PIEZOELECTRIC UNIMORPH ACTUATOR-BASED DM 1217 Fig. 4. XRD patterns for PZT films with different thickness. The peaks are indexed in terms of a pseudocubic perovskite structure. Fig. 6. Flowchart for the preparation of doped PZT films. m Fig. 5. Polarization-Electric field hysteresis loop for a 1- -thick PZT film. Good saturation is apparent. of each layer provided nucleation sites for the layer above it. The grain size is relatively uniform in plane and is about 150 nm. XRD measurements showed that the films were phase-pure perovskite (i.e., no pyrochlore phase was identified), and had a gradual change in the preferred orientation with increasing , the film thickness (Fig. 4). When the film was thin PZT films had (111) preferred orientation on (111) oriented platinum coated substrates, indicating a predominance of nucleation from the bottom electrode. With increasing film thickness, the films became more and more randomly oriented as the influence of the Pt/PZT interface was reduced [19]. Fig. 5 shows a polarization-electric field hysteresis loop of a 1- -thick PZT film. The polarization versus applied electric field loop shows a good square shape. Remanent polarization and coercive field values extracted from the P-E and 51 kV/cm, respectively. hysteresis loop are 36 The relative permittivity and tangent loss for a 1- -thick PZT film are about 1040 and 2.5% at room temperature, respectively. These values are characteristic of a high-quality film. For Fig. 7. X-ray diffraction patterns for Mg- and Sr-doped PZT thin films. Doping has little influence on either the film crystallinity or orientation. applications of DMs, there is interest in the low-temperature properties of the piezoelectric film. In particular, since the ultimate application of the mirrors will be in space, operation at cryogenic temperatures is important. For this reason, several dopants for the PZT films were investigated to determine if superior low-temperature performance could be achieved. Due to the divergence in the permittivity near a phase transition, the piezoelectric properties increase as the transition is approached, providing that a well-poled state can be maintained. Thus, lower transition temperatures should 1218 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 15, NO. 5, OCTOBER 2006 Fig. 8. Permittivity versus temperature curves for (a) undoped and (b) 16mol% Mg—doped PZT 52/48 films showing that Mg successfully lowers the Curie temperature. enable higher piezoelectric responses at room temperature, ceramics and films and below. Undoped have transition temperatures between 350 and 400 . To decrease the Curie temperature, Mg and Sr doping of PZT films was undertaken. However, it is important to note that the morphotropic phase boundary (MPB) in PZT can also shift as dopants are incorporated [20]. Because there is a significant increase in the piezoelectric response at MPB due to the higher polarizabilities, the Zr:Ti ratios in the doped PZT films were adjusted for a given dopant concentration in order to optimize the piezoelectric response. Fig. 6 shows a schematic of the route developed for doped PZT films. Mg ethoxide and strontium acetate were chosen as the Mg and Sr precursors, respectively. The Mg ethoxide had good solubility in 2-methoxyethanol and could be added to the solution after dehydration of the lead precursor. To improve the solubility of the strontium precursor, it was dissolved in acetic acid and was added to the PZT solution at the same time as the acetylacetone modification. Other processing details follow those outlined above. Typically, 0.4-M solutions were made using this approach. The solutions were batched assuming that the dopant would replace Pb on the A-site of the perovskite lattice. All solutions were prepared with 20mol% excess PbO to minimize second phase formation during crystallization. Several doping levels were investigated in order to progressively lower the phase transition temperature. It was found that in general the doped PZT are more susceptible to cracking than undoped PZT thin films prepared with a comparable route. The cracking was particularly severe in the Mg-doped films. To minimize cracking, many of the doped PZT films are comparatively thin relative to the undoped PZT films. Both Mg- and Sr-doped films were single phase perovskite, with some degree of (111) orientation, as seen in Fig. 7. The lattice parameters are somewhat different from those of the undoped films, suggesting that at least some of the dopant is incorporated into the lattice. On films with low crack densities, the electrical properties were measured. The transition temperature was reduced about relative to that for undoped PZT, as seen in Fig. 8. 100 Fig. 9. Permittivity versus temperature curves for 16 mole% Sr-doped PZT films with different Zr:Ti ratios: (a) a sample on the tetragonal side of the MPB and (b) a film with a composition close to the bulk MPB. The Sr-doped PZT films also showed reduced transition temperatures relative to undoped PZT. Fig. 9 shows the permittivity–temperature curves for films with 16mol% Sr-doped PZT YANG et al.: THIN-FILM PIEZOELECTRIC UNIMORPH ACTUATOR-BASED DM 1219 Fig. 10. Hysteresis loops for Sr-doped PZT films. The doped films show significantly smaller remanent polarizations than undoped PZT. films. The morphotropic phase boundary for this Sr-doping level is shifted to a Zr:Ti ratio of 57/43. This film had a transition , more than 120 lower than the untemperature of 223 doped film. All of the Sr-doped films show low dielectric loss values. Clear hysteresis loops were observed for the films (see Fig. 10). As expected, the decrease in transition temperature resulted in lower remanent polarization values than those seen for undoped films. The remanent polarization was also decreased by the tilting of the hysteresis loops, probably due to the tensile stress in the films associated with differences in the film and substrate thermal expansion coefficients. The room temperature permittivity of the films did not increase in all of the doped films, suggesting either the presence of a low permittivity interfacial layer whose influence is more predominant in thinner films and/or the presence of a small amount of second phase material (e.g., unincorporated dopant) that was not detected in the X-ray diffraction patterns. values of both undoped and doped PZT films were The measured as a function of temperature using the wafer flexure method [21]. Films were poled and allowed to age for 1 day prior to the measurements to minimize the effect of aging on determination of temperature dependence. Because the samples Fig. 11. Temperature dependence of the piezoelectric response for (a) undoped PZT 52/48 films of different thickness and (b) 16mol% Sr-doped films on (square) and off (triangle) the morphotropic phase boundary. were poled at room temperature, without hot poling or ultravicoefficients decreased relative to their olet exposure, the coeffias-poled values due to the initial aging. Remanent cients of are achievable at . Fig. 11 shows a comparison of the temperature dependence of the piezoelectric response for a number of different films. In these undoped PZT 52/48 films, the piezoelectric response was somewhat higher for thicker films. It is also apparent that for the Sr-doped samples, the piezoelectric response is larger near the bulk morphotropic phase boundary composition (Sr/Zr/Ti 16/57/43). This suggests that in films, as in bulk, doped PZT, Sr addition stabilized the tetragonal phase [22]. It also demonstrates that it is important, in the doped films to readjust the Zr:Ti ratio to the new MPB. It was also determined that the properties of the doped films are not as high as the undoped PZT. This is probably due to a combination of factors, including: 1) the fact that the doped films were thinner; 2) fine, hairline cracks were observed 1220 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 15, NO. 5, OCTOBER 2006 Fig. 12. Dependence of deflection on silicon membrane thickness for both continuous and patterned PZT films. There is a significant increase in the deflection for the patterned PZT actuator. The data points represent an average of ten separate measurements on two different pixels within an array. The is the electrode size relative to the unimorph membrane. in some areas of the doped films; and 3) the lowered remanent polarization in the doped films. All of these factors reduce the in-plane piezoelectric response. The first two difficulties could probably be eliminated with improvements in the film pyrolysis conditions. Due to the superior properties, DM devices were made with undoped PZT 52/48 films. B. PZT Unimorph Actuator Arrays A major part of the PZT unimorph actuator technology has already been developed. The detailed fabrication process of the unimorph actuators is described in a previous paper [23]. In this section, the top-level fabrication sequence is given as follows. The fabrication of unimorph actuators started using a thermally oxidized SOI wafer. Ti/Pt layers were subsequently evaporated on the front surface of the wafer. Then, PZT films were prepared using a chemical-solution deposition process as described in the previous section. Undoped PZT films were used in all of the actuators reported here. Cr/Pt/Au layers were evaporated onto the PZT layer, and patterned to form top electrodes and contact pads. A wet etching process for the PZT thick films was used to expose the bottom electrode. Finally, backside cavities were formed by deep reactive ion etching (DRIE) until the buried silicon dioxide was exposed. After this layer was removed in a buffered HF solution, further RIE was performed to thin the silicon membrane as needed. A Kapton tape-based masking approach was used to cover some areas of the wafer for selective etching of the cavities, thus allowing several different silicon membrane thicknesses on a single wafer. A WYKO RST Plus Optical Profiler was used to analyze the deflections of the actuator membranes. We observed a significant increase in the deflection when the PZT film surrounding the actuator was removed, as shown in Fig. 12. Three different Fig. 13. Actuator stroke as a function of voltage for three different types of actuators. Significant improvement in stroke is achieved using unimorphs with patterned PZT with optimized geometry. unimorph actuator structures have been designed, fabricated, modeled, and tested. In Fig. 12, Case A shows a schematic of a typical unimorph actuator previously developed (described in detail in [23]). It consists of a patterned top electrode (Au) on top of a PZT layer. This stack was prepared on a bottom electrode (Pt) deposited on the silicon layer (membrane). The size of the top electrode and the thicknesses of the PZT and silicon layers were optimized using based on modeling, which employs the energy minimization approach [15]. Case B shows a schematic of a unimorph actuator with a “patterned” PZT layer. The size of the PZT pattern was optimized using the modeling method previously developed [14]. Case C presents a schematic of an actuator with patterned PZT and patterned silicon layers. Modeling was not performed for this case, since the modeling code YANG et al.: THIN-FILM PIEZOELECTRIC UNIMORPH ACTUATOR-BASED DM 1221 Fig. 14. Process schematic for fabrication and transfer of a mirror membrane. was not optimized for patterned (noncontinuous) silicon structures. Finite-element model (FEM) analysis may be required in order to accurately assess the actuator behavior for Case C, but this would be beyond the scope of the work described in this paper. The measured deflection for an optimized actuator is at 20 V (for an actuator with a 2.5-mm diameter, PZT/Si - -thick, PZT patterned over 60% of the membrane diameter, and silicon membrane patterned). This deflection increase is believed to be due to a decrease in the residual stress in the actuator. 5.7 1222 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 15, NO. 5, OCTOBER 2006 In order to maximize the deflection, unimorph actuators with different silicon membrane thicknesses were characterized. Actuators with different membrane thicknesses were obtained on the same wafer by selectively etching the silicon membrane to different final thicknesses using the Kapton tape-masked backside etching process [23]. Fig. 13 compares the measured actuator strokes with the modeled values. The actuation results from using 2.5-mm-diameter membrane actuators with: 1) continuous PZT film (i.e., Case A) and 2) patterned PZT film (i.e., Case B) are shown as a function of membrane thickness. The experimental results are superimposed over their respective predicted deflection curves from the simulation model. As predicted by our model, the maximum deflections were obtained at intermediate silicon-membrane thicknesses of approximately: with the continuous PZT film and 2) 10 with 1) 15 the patterned PZT film. C. Deformable Mirror A proof-of-concept DM structure was fabricated using typical unimorph actuators (Case A in Fig. 12), and its actuation performance was characterized using the WYKO RST Plus Optical Profiler. For fabrication of the mirror membrane, we utilized the membrane transfer process [8] developed at JPL in order to transfer the mirror membrane onto the fabricated actuator arrays. The membrane transfer process is briefly described as follows. The mirror membrane transfer process involves transfer of the single-crystal silicon layer from the SOI wafer following the metallization, bonding, and etching processes. SOI carrier wafers were used for the fabrication of the single-crystal silicon mirror membrane. The thickness of the transferred membrane is determined by the thickness of the SOI top silicon layer. A 20- -thick single-crystal silicon mirror membrane was transferred onto the actuator wafer. The actuator wafer and the SOI carrier wafer were prepared [see Fig. 14(a)]. Cr/Pt/Au metal layers were deposited and patterned to form bonding pad arrays on both the carrier and actuator wafers. A 1- -thick In layer and a 100-Å-thick Au layer were subsequently deposited and patterned on both the carrier and actuator wafers using a lift-off process [see Fig. 14(b)]. The SOI carrier wafer was subsequently bonded to the substrate wafer [see Fig. 14(c)]. The backside etching was conducted in a 25 wt% solution of tetramuntil the buried ethylammonium hydroxide (TMAH) at 80 oxide was exposed. A specially designed Teflon fixture was used to protect both the backside of the bonded substrate wafer as well as the bonded interface [see Fig. 14(d)]. The exposed oxide was removed by using 49% HF droplets [see Fig. 14(e)]. An plasma etch was incorporated, as necessary, to selectively etch the transferred membrane in order to release membrane structures [see Fig. 14(f)]. Fig. 15 contains a cross-sectional view of the DM structure and photographs of a fabricated DM with a 20- -thick silicon membrane mirror (50 mm 50 mm area) supported by 400 PZT unimorph actuators. Fig. 16 shows the local surface deformation of a DM created by the underlying actuators (i.e., typical unimorph: Case A). The measured maximum mirror deflection at . This deflection for a DM shows 30 V is approximately 1 that the stroke of the mirror membrane is approximately 40% of the stroke of actuator alone. The measured influence function 2 Fig. 15. Fabricated deformable mirror with 20 20 piezoelectric unimorph actuator array. (a) Cross-sectional schematic. (b), (c) Photographs of the actuator arrays and the DM. (interactuator coupling) was approximately 30%. The full-scale measurement (up and down) of the mirror and actuator combination was not performed due to a lack of reference area on the mirror membrane. Hence, the measurements on the mirror membrane were made in the “differential mode” only [23]. The full-scale optical measurement protocol as well as the software and driver electronics for a DM device have to be established in the future in order to fully characterize the DM performance. For the actuator alone, the measurements were made with respect to reference electrodes. The stroke reduction can be minimized by varying the mechanical compliance (by optimizing the PZT/ actuator membrane/ mirror membrane thickness ratio). The frequency responses for the unimorph actuator, with and without the mounted mirror membrane, were obtained using a laser-doppler vibrometer (shown in Fig. 17). The resonance frequency of a 2-mm-diameter, 2- -thick PZT/15- -thick silicon membrane, and 60% electrode actuator was measured at 63 kHz, which far exceeds the bandwidth requirement for most [23]. The bandwidth of the DM in this paper DMs far exceeds the bandwidth requirement for most DMs that are applicable to several space and Earth science missions being envisioned by NASA. The future development plan includes demonstration of the DM technology by: 1) flattening the mirror under a Michelson interferometer setup; 2) measuring the gains of all actuators; 3) measuring the temporal frequency response of several actuators; and 4) measuring the influence function of all actuators. IV. APPLICATIONS: PRESENT AND FUTURE Large ground-based observatories will need a combination of integrated wavefront correction with correction at conjugate pupils to produce diffraction-limited imagery. The use of such control systems may greatly ease the tolerances on the primary mirror, which are generally a major cost driver. At high frequencies, as are relevant for ground-based telescopes exposed to atmospheric turbulence, correction of the primary mirror is referred to as adaptive optics; at quasi-static frequencies of perhaps 1 Hz and below, as are typically required by space-based YANG et al.: THIN-FILM PIEZOELECTRIC UNIMORPH ACTUATOR-BASED DM 1223 Fig. 16. Deflection of a DM with a single actuator activated. From this profile, the measured influence function (crosstalk between pixels) is approximately 25%. Fig. 17. Measured frequency response of the piezoelectric unimorph actuator alone and with a mounted mirror membrane. These plots demonstrate that the DM is capable of wide-bandwidth operation. missions, such corrections are called active optics. The DM technology reported here is appropriate to a wide range of image correction applications, active or adaptive, on the ground or in space. The achievement of large-actuator stroke is particularly important for projects targeting observations at longer wavelengths and/or in strong turbulence. Scalability to large formats generally results in reduction of fitting errors and achievement of high correction (Strehl ratio), and it has additional benefits for imaging related to suppressing speckle noise by reducing the intensity of typical remnant speckles. Furthermore, it can be important to produce physically large DMs, because extreme reduction of scale from the pupil to the reimaged pupil can create excessive optical aberrations. The coronagraphic version of the TPF project that has been studied at JPL required adaptive correction of a coronagraphic imager in a mode in which individual speckles, due to either phase or amplitude imperfections across the aperture, are targeted and removed. Interferometric planet finders require nulling interferometry in which the two arms of a Michelson interferometer are fed with beams that are very precisely matched in intensity and phase, in each polarization and at each wavelength over a broad band, so that a deep null results when one arm is given an extra achromatic phase shift of rad. The required intensity match is on the order of 0.1%; the required phase match is about 1 mrad. To ease the requirements on the optical components, JPL is developing an “adaptive nuller” device, based on a DM, that quasi-statically adjusts the intensity and phase in each of about a dozen or so wavelength channels [24]. The adaptive nuller is a scheme for balancing the two arms of a nulling interferometer, in both amplitude and phase, independently in each linear polarization, in each of perhaps a few dozen spectral channels. A device like this can substantially ease the requirement for matching optics in the two arms of the interferometer. The heart of the device is a DM that applies the required piston to adjust phase and, in the orthogonal axis, tilt to adjust amplitude of the incident beam that has been spectrally dispersed and separated by polarizations. Optimized versions of the prototype DM described above will be well suited to the adaptive nulling task, particularly due to their low influence function, which allows clean, independent correction of nearby spectral channels. This example illustrates how new applications result when the capabilities of DMs become available and known to optical designers. It is likely that many currently unforeseen applications will be developed when the technology is more widely available. V. CONCLUSION We have successfully fabricated, assembled, and characterized a large-aperture DM composed of a continuous single-crystal silicon membrane supported by PZT unimorph actuator arrays. A mathematical model based on an energy 1224 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 15, NO. 5, OCTOBER 2006 minimization method was used to assist the optimization of membrane thickness and electrode sizes. Excellent agreement with experiment was obtained. Improved PZT unimorph actuators with patterned PZT film designed with optimized PZT/Si thicknesses can produce large strokes at low voltages. DMs consisting of 20- -thick single-crystal silicon membranes 20 actuator arrays were fabricated and supported by 20 optically characterized. Application in an adaptive nulling task has been discussed. Our devices have a low influence function of 30%, which is desirable for closed-loop adaptive optics applications. The PZT actuators have sufficiently high piezoelectric coefficients that use of the mirrors at cryogenic temperatures should be possible at modest applied voltages. In all of the key parameters, the unimorph MEMS DMs described here can be optimized for delivery of high-quality image correction. Improvements in the fabrication process for better optical quality mirror membranes and optimization of the DMs for larger strokes are underway. Optimized devices should be well suited to the adaptive nulling task, particularly in their low influence function, which allows clean independent correction of nearby spectral channels. ACKNOWLEDGMENT Some of the research described in this paper was carried out at the Jet Propulsion Laboratory, California Institute of Technology. The research described here was performed under the Director’s Research and Development Fund at JPL. REFERENCES [1] D. Coulter, “NASA’s terrestrial planet finder missions,” Proc. SPIE, vol. 5487, pp. 1207–1215, Oct. 2004. [2] R. Gilmozzi, “Science and technology drivers for future giant telescopes,” Proc. SPIE, vol. 5489, Ground-Based Telescopes, pp. 1–10, 2004. [3] D. F. Lester, D. J. 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Reaney, “Effects of strontium substitution in Nb-doped PZT ceramics,” J. Eur. Ceram. Soc., vol. 21, pp. 1371–1375, 2001. [23] Y. Hishinuma and E.-H. Yang, “Piezoelectric unimorph microactuator arrays for single-crystal silicon continuous membrane deformable mirror,” J. Microelectromech. Syst., vol. 15, no. 3, pp. 686–696, Jun. 2006. [24] O. Lay, M. Jeganathan, and R. Peters, M. Fridlund and T. Henning, Eds., “Adaptive nulling: A new tool for interferometric exo-planet detection,” in Proc. Conf. Towards Other Earths: DARWIN/TPF and the Search for Extrasolar Terrestrial Planets, Heidelberg, Germany, Apr. 22–25, 2003, pp. 503–506. Eui-Hyeok (EH) Yang (S’90–A’95–M’03–SM’06) received the B.S., M.S., and Ph.D. degrees from the Department of Control and Instrumentation Engineering, Ajou University, Korea, in 1990, 1992, and 1996, respectively. Presently, he is an Associate Professor in the Mechanical Engineering Department, Stevens Institute of Technology, Hoboken, NJ. He joined the Fujita MEMS Research Group at the Institute of Industrial Science, University of Tokyo, Japan, as a Visiting Postdoctoral Researcher in 1996. He received a research fellowship from the Japan Society for the Promotion of Science from 1996 to 1998. In 1999, he joined NASA’s Jet Propulsion Laboratory (JPL), Pasadena, CA, where he initiated the development of MEMS actuator-based adaptive optical devices. He was then a Senior Member of the Engineering Staff and the task manager for several technology development projects at JPL in the area of micro- and nanotechnologies. He initiated and led the development of MEMS-based deformable mirrors and actuators for future large aperture telescopes, and also led the development of MEMS-based piezoelectric valves for future microspacecraft applications. He participated in the technical evaluation YANG et al.: THIN-FILM PIEZOELECTRIC UNIMORPH ACTUATOR-BASED DM of MEMS mirror array technologies developed for the Multi Object Spectrometer (MOS) project for the James Webb Space Telescope (JWST). He was a technical monitor for a NASA SBIR project. He was a Research Adviser for National Research Council (NRC) in the area of piezoelectric microactuators for active-mirror technologies. He has been successful in winning extremely competitive major research grants which represents an exceptional achievement and productivity within NASA. He has extensive experience in microactuator, deformable mirror, and optical membrane fabrication. His current research interests include all aspects of microsensors/actuators, microfluidics, adaptive optics, micro/nano energy conversion, and nano-manufacturing technologies. He has published over 90 papers in the field of MEMS, and has six patents issued or pending. Dr. Yang is a member of the Technical Program Committee (TPC) of the IEEE Sensors Conference. He is Topic Organizer of the Micro and Nano Devices Topic, within the MEMS Division, of the ASME International Mechanical Engineering Congress and Exposition. He has been serving as a referee for several archival journals, international conferences and proposals. In recognition of his excellence in advancing the use of MEMS-based actuators for space applications, he received the Lew Allen Award for Excellence for 2003 at JPL. Yoshikazu Hishinuma received the B.S. degree in applied and engineering physics from Cornell University, Ithaca, NY, in 1997, and the M.S. and Ph.D. degrees in applied physics from Stanford University, Stanford, CA, in 1999 and 2002, respectively. His doctoral work concentrated on experimental and theoretical studies on refrigeration effect of low work function materials during electron tunneling at room temperature. From 2002 to 2005, he was with the Microdevices Laboratory, Jet Propulsion Laboratory, Pasadena, CA where his research focused on the development of micromachined deformable mirrors. Currently, he is with Fuji Photo Film Company, Ltd., Kanagawa, Japan, where he continues to work on various microscale devices. His research interests include microfabrication technologies, MEMS actuator designs, and sensors for small-signal detections. Jian-Gong Cheng received the M.S. degree in condensed-matter physics from Shandong University, Jinan, China, in 1997, and the Ph.D. degree in microelectronics and solid-state electronics from Shanghai Institute of Technical Physics, Chinese Academy of Sciences, Shanghai, China, in 2000. He was a Senior Research Fellow with the Corporate Technology of Siemens AG, Munich, Germany, from 2001 to 2002. He was with the Material Research Laboratory of Pennsylvania State University as a Postdoctoral Fellow from 2003 to 2005. Since April 2005, he has been a Professor with the Shanghai Institute of Microsystem and Information Technology, Chinese Academy Sciences, Shanghai, China. His research covers ferroelectric materials and their applications as pyroelectrics in infrared detectors, dielectrics in capacitors, and as piezoelectric transducers for biosensors. He is pursuing his research interests in developing novel biosensors. Susan Trolier-McKinstry (M’92–SM’01) received the B.S., M.S., and Ph.D. degrees from the Pennsylvania State University (Penn State), University Park, all in ceramic science. After graduation, she joined the faculty at Penn State, where she is currently a Professor of ceramic science and engineering and Director of the W. M. Keck Smart Materials Integration Laboratory. Her main research interests include dielectric and piezoelectric thin films, the development of texture in bulk ceramic piezoelectrics, and spectroscopic 1225 ellipsometry. She has held visiting appointments with the Hitachi Central Research Laboratory, the Army Research Laboratory, and the École Polytechnique Federale de Lausanne. Prof. Trolier-McKinstry is a Fellow of the American Ceramic Society and a member of the Materials Research Society. She is past-president of both Keramos and the Ceramics Education Council and is co-chair of the committee revising the IEEE Standard on Ferroelectricity. She has served as Vice-President for Ferroelectrics of the IEEE UFFC and is now President-Elect of the society. She was the recipient of the Robert Coble Award of the American Ceramic Society, the Wilson Award for Outstanding Teaching in the College of Earth and Mineral Sciences, the Materials Research Laboratory Outstanding Faculty Award, and a National Science Foundation Career grant. Eric Bloemhof received the Ph.D. degree in physics from the University of California, Berkeley, in the Quantum Electronics and Astrophysics group of Prof. C. Townes. He was a Center Postdoctoral Fellow with the Harvard-Smithsonian Center for Astrophysics, Cambridge, MA, and continued work at the Smithsonian Astrophysical Observatory in the area of submillimeter instrumentation, including superconducting tunnel-junction mixers and receivers. He was Chief Physicist for the Palomar Observatory, California Institute of Technology, where he was involved primarily on the PALAO adaptive optics system being built at the Jet Propulsion Laboratory (JPL) for the 5-m Hale telescope. In 2001, he joined JPL to work on various instrumentation connected with space-borne interferometers, including the Space Interferometry Mission (SIM) and the interferometric Terrestrial Planet Finder (TPF-I). He currently leads the collector optics group for SIM, and the mask development effort for JPL’s innovative four-quadrant- phase-mask coronagraph that has demonstrated deep starlight suppression on the Hale telescope. Recent research has concentrated on the behavior of speckles in highly corrected imagers and coronagraphs and inventing techniques for suppressing speckle noise and enhancing companion-detection contrast with an eye toward planet searches. Dr. Bloemhof is a member of the American Physical Society, the American Astronomical Society, and URSI. B. Martin Levine received the B.S. degree from the Rochester Institute of Technology in 1972, the Master’s degree in statistics from the Colorado State University in 1976, and the Ph.D. degree in optics from the University of Rochester, NY, in 1986. He has 20 years experience in the design and construction of adaptive optics systems working as a consultant for the U.S. Air Force and also at Adaptive Optics Associates. Currently, he holds the positions of Deputy Leader, Interferometry Center of Excellence, and also is the Manager of the Advance Telescopes Technologies and Concepts Office at the Jet Propulsion Laboratory, Pasadena, CA, where he is working on developing advanced concepts for future space missions. Dr. Levine is a member of the Optical Society of America, SPIE-The Optical Engineering Society, and the American Astronomical Society.