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Anelva RF Magnetron Sputtering UnitModel SPF-332H Sabiha Sultana Equipment technologist CEN,IISc Overview Tool specifications Reasons for sputtering Simple working diagram Operating parameters Materials available @ CEN Regularly used processes Process developed @ CEN New Sputtering unit Tool Specifications: Make Cathode Ultimate pressure Medium Power source Substrate-target distance Substrate heater Anelva Sputtering unit model SPF 332H 3 numbers 3” planar magnetron cathodes 2x10-6 mbar Argon plasma DC and RF 5-10 cm RT to 350°C Reasons for sputtering: Use of sufficiently large area targets give uniform thickness over the wafer. Precise control of thickness through operating parameters. Control of film property. Ex: Grain structure (substrate temperature) Simple working diagram: Operating parameters: Argon pressure Substrate voltage Substrate to target distance Deposition time Substrate temperature Materials currently available @ CEN: Chromium Gold Titanium Platinum Nickel Silver ITO Silicon P-type Silicon N-type Silicon-di-oxide Silicon Nitride PZT Zirconium Aluminum High K dielectrics: Europium Oxide Gadolinium Oxide Other materials sputtered: Tungsten Niobium Tantalum Yttrium Oxide Germanium Silicon Application of sputtered films: Metal contact Lift off High K capacitors Seed layer for electroplating Masking layer SEM imaging of non conducting films Chrome used as hard mask for etching SiO2 in RIE- Renil Kumar (INUP) 200nm lines masked by Chrome Metal Nano particles as charge-trapping nodes- Girish M (Chemical eng dept) 7nm Au nano particles with 2nm spacing Gadolinium oxide film Gold nano particles embedded in Gd2O3 Sputtered metal films used for surface plasmon resonance- Nityanand Kumawat (ECE) Sputtered Silicon film Depoition rate 2nm/min heated @300°C- Sindhuja Sridhar (ECE) FLEXLAB Flexible configurable sputtering system RF and DC sputter source. Deposits metallic, inorganic, di-electric and organic materials. Multilayer and Co-deposition. Downstream sputtering. System specification: Deposition of metals like Au, Ag, Ni, Cr, Cu, Pt and dielectrics like Eu2O3, Gd2O3, TiO2, Al2O3, SiO2, Ta2O5, HfO2, etc. These coatings should be deposited on glass/semiconductor substrates. Coating uniformity of ±1% on 4” diameter substrate. Provision of operating: Vacuum system RF magnetron and DC power supply Substrate heating Substrate rotation Variable substrate to target distance Thickness monitor and control in both manual and automatic mode of operation Vacuum system: Low vacuum pumping system: Make: Edward gv 80 dry pump Ultimate pressure: <10-2mbar High vacuum pump: Make: pfeiffer Vacuum turbo pump Pumping speed: 1200 l/s Ultimate pressure: <2x10-10Torr Measuring gauges: Low vacuum gauge: Atmospheric pressure- 5x10-4 mbar Pirani guage(accuracy-1%) High vacuum gauge: 0.01- 2x10-9 mbar Compact cold cathode guage(accuracy-1%) Full range gauge: Compact full range pirani/ cold cathode gauge 5x10-9 – 1000 mbar Process gauge: Compact capacitance gauge Gas distribution system: Inlet for N2, O2 and Ar with MFC Fourth line for additional gas Cathodes: 3” cathodes- 3 numbers with confocal arrangement. DC and RF magnetron system. Power supplies RF power supply: 1500W 13.56MHz 50Ω DC power supply: 1000W DC Split biasing: 300V , 5amps Substrate holder: 6” diameter substrate holder RF and DC bias cleaning of the substrates Distance between substrate and target variable from 5cm to 15cm Substrate holder rotation speed can be varied between 0-20rpm DC substrate bias provided (split biasing) Substrate heating system provided Split biasing Provision for split biasing between anode and cathode electrodes DC power supply of 300Volts, 5Amps capacity is provided to substrate holder For simultaneous sputtering deposition with substrate etching This is to achieve high packing density and quality coating Substrate heating Maximum temperature: 350°C Radiant heaters/ quartz lamp-type Regulated by digital PID type temperature controller, interfaced to PLC Digital thickness monitoring: 3 water cooled dual head adjustable quartz crystal monitor Sensor-AT-CUT Plano convex quartz crystal sensor Oscillation frequency of 6MHz Accuracy better than 1% of nominal value and deposition better than 0.1nm/sec Magnetron sputtering sources: 3 numbers of water cooled sources of 3” diameter Compatible with DC and RF power supply Provision for co-deposition provided Target shutter provided to prevent cross contamination. Control system: System has provision of working in: Completely manual mode Fully automatic mode Automatic mode with manual override Stand by mode Coating control system: Magnetron source controlling mechanism and shutter will be connected to thickness controller. Thank You