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Transcript
RFMax
RF Ion Sources
Sample Cleaning
Ion Milling
Ion Beam Assisted Deposition
Thin Film Densification
Control of Film Chemical
Composition
MEMS
RF Ion Series
Beams of accelerated ions are often used to modify and erode surfaces under vacuum conditions. By carefully selecting
the energy and composition of an ion beam, this can be used, for example, to significantly improve the characteristics of
a growing film by both, densifying the film and modifying the chemical composition of the film.
Alternatively, ion beams can be used to erode (mill) existing films or sputter target material to project a plume of material
for deposition onto a substrate. In the latter case, the growing films can have an excellent quality for many applications
owing to the elevated kinetic energy of the sputtered material.
Source Construction
Layout Schematics
The RFMax ion sources are designed for use in UHV or
HV deposition systems for applications where a broad,
energetic beam of ions is required with a moderately low
energy spread. The sources can generate ion beams from
as low as 50eV up to 1000eV and with beam currents
between 10mA and 150mA. The beams have a typical
divergence of several degrees when using nominally flat
grids.
RFMax60 Ion Source Layout
The ion source contains a helical coil wrapped around a
ceramic discharge tube. RF power at 13.56MHz is applied
to this coil with a power between 100 and 600W at the
same time as a gas is introduced into the discharge tube.
The RF field generates a plasma within the discharge
tube, thus supplying the charged particles which form the
basis of the ion beam.
The discharge tube is enclosed by a pair of hightransparency grids. The grid material can be carbon
(graphite), molybdenum or titanium. For most applications
molybdenum or graphite grids are recommended.
The inner grid (beam grid) has a voltage applied which
is equal to the energy of the ion beam the user wishes
to generate. The outer grid is held at earth potential.
This potential difference between the grids creates a
field gradient which acts to draw ions from the plasma
and through the holes in the outer grid. The multiple
'beamlets' combine to form one broad ion beam which
emerges into the chamber.
Shutter
(optional)
Source head
(water cooled)
NW100CF (6" O.D.)
mounting flange
Manual or
motorised shutter
(optional)
NW16CF
(1.33" O.D.)
viewport
96mm
290mm
Bias/extraction
grids feedthrough
Water cooled
RF connection
(protected)
Automatic tuning unit
Operation
In the RFMax ion source the relationship between RF
power and beam current is close to linear. Thus, by
changing RF power, it is possible to make small changes
to the beam current for a fixed beam energy.
Operation at high RF power requires efficient water
cooling. The MANTIS ion sources have the induction coil,
the gas inlet and the tip of the source internally water
cooled. The cooling prevents overheating of the source
components and additionally, it eliminates impurities
from being outgassed into the deposition environment
and keeps UHV environment clean.
140
Beam Current [mA]
Beam Current [mA]
120
100
80
60
40
20
0
100
150
200
250
300
350
400
RF Power [W]
RF Power [W]
This image shows a RFM30 Ion source in operation.
Beam current vs. RF power at 500V beam energy and 9sccm
oxygen flow.
Designed for use in UHV or HV Deposition Systems
Tuning
120
Tuning provides a mechanism to couple RF power
correctly to the plasma discharge. The RFMax ion
sources come with automatic tuning units as standard.
The automatic matching unit provides quick and precise
tuning for matching the impedance of the source and
the impedance of the RF power supply when plasma
conditions change.
60
40
20
0
0
500
1000
Beam Energy [V]
Beam Energy [V]
Beam current vs. RF Beam Energy at 230W beam power and 9sccm
oxygen flow.
Gas Compatibility
The source can be operated with oxygen, nitrogen or
argon gas. The table below shows gas compatibility with
various materials. The source can also be used with
some organic gases such as methane, but these should
be heavily diluted with hydrogen gas to avoid carbon
deposits forming on the inside of the discharge tube.
Please contact MANTIS for recommendations on nonstandard gases.
Grid Material
Gas Compatibility
Carbon
Ar, N2
Molybdenum
Ar, O2, N2
Titanium
Ar, N2
Gas Control
Generally, the gas is introduced into the ion source through
a mass flow controller (MFC) which can be calibrated for
a variety of discharge gases. MANTIS manufactures a four
channel controller that can operate up to four MFCs to
control the gas flow rate into the discharge tube.
The compact unit mounts in a standard electronics rack
and has four digital displays indicating the flow setting for
each unit.
Shutter Control
The MANTIS RFMax sources can be fitted with either a
manual or motor driven shutter. Shutters are constructed
of refractory metals to ensure UHV compatibility.
Matched with the MANTIS Titanium control software, the
RFMax sources can be integrated into fully automated
deposition systems. Available functions of the software
package include automatic plasma ignition, automatic gas
flow control and recipe process control. The automation
package is suitable for both research and industrial
applications.
Beam Neutraliser
A beam neutraliser can be added to the end of the source
to inject electrons into the ion beam to ensure that the
total charge arriving at the sample is near zero. This
allows ion beam sputtering of dielectrics and better beam
optics to be achieved.
Faraday cup current density [mA/cm2]
80
Ion Energy [eV]
Ion current density measured using a Faraday cup (0.02cm² area) for
different RF Powers at a working distance of 73mm.
Lateral ion beam current profile [mA/cm2]
Beam Current [mA]
Beam Current [mA]
100
Lateral ion beam current profile [mA/cm2]
1
0.9
100W
0.8
200W
0.7
250W
0.6
0.5
0.4
0.3
0.2
0.1
0
-10
-8
-6
-4
-2
0
distance [cm]
2
4
6
8
10
Distance [cm]
Argon ion beam current profile [mA/cm²] at 1keV and 5sccm gas flow,
measured with a Faraday cup across the ion source, distance between
source and Faraday cup is 150mm.
Specifications
RFM30
RFM60
Mounting flange
NW63CF (4.5" O.D.)
NW100CF (6" O.D.)
UHV compatible
Yes, bakeable up to 250°C
In-vacuum length
290mm - special length on request
In-vacuum diameter of source head
60mm
96mm
Beam diameter
30mm
50mm
Gas compatibility
O2, N2, H2, Ar
Discharge tube material
Quartz:
PBN:
suitable for oxygen, nitrogen, hydrogen
suitable for nitrogen
Extraction grids material
Molybdenum:
Graphite:
Titanium:
suitable for oxygen, nitrogen, argon
suitable for nitrogen, argon
suitable for nitrogen, argon
Beam energy
100eV - 1keV
100eV - 1keV
Current density
Up to 5mA/cm2
Up to 6mA/cm2
Gas flow
8 - 10sccm (typical)
10 - 15sccm (typical)
Applicable RF power
100 - 300W
100 - 600W
Power supply
600W RF power supply
RF Tuning
Automatic
Cooling
Minimum water flow of 0.5 I/min
Shutter
Integral manual or motorised shutter (optional)
Beam thermaliser
Optional
Optical plasma monitoring
Optional
RF atom source conversion kit
Optional
Power Supplies (Optional)
Cable length
5m - special length on request
RF power supply
13.56MHz, 600W (35Amps @ 4.5KV peak)
Automatic matching network including controller
Forward power metering: +/-1% full scale, +/-1% reading
Output power stability: +/0.5% long term, +/-1% Watt
Single phase, 100-240VAC, 50/60Hz
DC power supply
(beam energy)
Up to 1kV, up to 300mA
Single phase, 100-240VAC, 50/60Hz
For further information please contact:
[email protected]
www.mantisdeposition.com