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Overbrook Scientific
Overbrook Scientific
 Providers
of Analytical Instrumentation
 Providers
of Instrument Support and
Peripheral Services
 Distributors
of the HTA Line of
Autosamplers
HTA Autosamplers

HT300A Liquid Sampler

HT200H Headspace Sampler

HT250D Liquid/Headspace Sampler

HT280T (SPME) Headspace Sampler
HTA Autosamplers
 “High
Throughput Automation”
 Manufactured
 Reputation
in Italy
for quality workmanship
Overbrook Collaborations
 Restek
 Phenomenex
 Rapid
Tech
HT300A Liquid Autosampler
HT 300A - Key Features

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Replacement sampler- any major manufactured GC
Extremely Rugged
Rotating Turret Design
No picking up of the vial
Handles Front and Back Injectors
Small footprint
Economical - $8,500
Accurate – Reproducibility Typically .3%
Very Easy to use
Nice Looking (Italian)
Control Software Available including Agilent
Chemstation
Headspace
Headspace

Europeans to date have a higher level of
proficiency due to experience

More Widely Used

More Widely Accepted

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Blood Alcohol
Residual Solvents
Environmental
R&D
Advantages of Headspace in the
Environmental Laboratory

Pre-screening for VOC’s – Aqueous and Solids
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EPA 8260 Aqueous and Solids
Methods 624 Waste Water, 524 Drinking Water
Why Gamble on Sample Throughput?
Protecting a Lucrative Revenue Stream
Decrease Downtime From Contamination
Protect your MS System and Sustain Productivity by
Pre-screening
HT200H Headspace Autosampler
HT200H Headspace Sampler
Key Features
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Cost effective ($17,900)
Inexpensive to Operate
Small Footprint
Rotating Turret
Front and Back Injectors - Run Multiple Methods
Direct Injection – No Transfer Line
Leaves Inlet Intact
No Carryover
Very Short Runtime (under 10 min. Including
Naphthalene)
HT250D Dual Autosampler
HT250D Dual Autosampler

Headspace and Liquid Autosampler in one
unit
 All the features of HT200H plus features of
HT300A
 Easy to change from one mode to the other
 All included – no optional extras
 Maximizes the throughput on individual GC’s
 Small Footprint
 Most Economical Dual Unit on the Market
Headspace Methods
EPA Method 8260
Pre-screening
 Volatiles
partition into vial headspace
 1ml gas-tight syringe injection
 GC/FID System
 Use reduced compound list or reference
calibration (aromatic and chlorinateds)
 Dilute appropriately and run by
P&T/GC/MS
Prescreening
Method RSK 175

An umbrella EPA Method for permanent gas
analysis
 USEPA Region 1 application notes applied to
MNA
 Standards readily available from Scott &
Restek
 Analyze Methane/Ethane/Ethene to 2ug/L
 Remember Methane is a Reportable
Compound in MA
Methane Ethane Ethene
CCME Method 1310
 Canadian
Petroleum Hydrocarbon
Method for VPH/GRO
 Performance based method allows for
Headspace Preparation to reduce
carryover contamination
 PBM Criteria require strict alkane/
aromatic ratios
 Pre-screen UST Samples – no reruns
for baseline resolution issues
Volatile Petroleum
Business Opportunities
with Headspace
Business Opportunities
with Headspace
 CCME
1310
 Materials Testing
 USP 467 Residual Solvents
 Raw Materials from China
 VOA’s (Raw production Material that
cannot be prepared by P&T)
Thank You