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AL-FARABI KAZAKH NATIONAL UNIVERSITY Faculty of Chemistry and Chemical Technology Education programme on specialty «6М072100 – chemical technology of organic compounds» Approved at the meeting of Academic Council of Chemistry and Chemical Technology Faculty (the protocol № 1, August 28, 2014) Dean of Chemistry and Chemical Technology Faculty _______________E.K. Ongarbayev SYLLABUS Base elective module №1 MPOT «Modern technologies of processing of organic substances» STPOV 5503 «Modern technologies of processing of organic substances» I year magistracy, e/g, spring semester, 3 credits Lecturer: Chopabayeva Nazira Nabievna, doctor of chemical sciences, associated professor Department of chemistry and technology of organic substances, natural compounds and polymers. Mob.: +7 701 2332837 e-mail: [email protected] room: 525 Teacher of seminar lessons: Chopabayeva Nazira Nabievna, doctor of chemical sciences, associated professor, Department of chemistry and technology of organic substances, natural compounds and polymers. Mob.: +7 701 2332837 e-mail: [email protected] room: 525 Aim and tasks of discipline: Aim: studying of technological features of industrial methods of synthesis and processing of various organic compounds. Tasks: giving knowledge about various sources of obtaining of industrially important organic compounds, up-to-date methods of their obtaining and processing, general and special chemical properties of these compounds and methods of manufacturing control on each technological stage. Competences: instrumental: possession of ability to use and transform of cognitive abilities and innovative technologies for searching nonstandard, creative decisions in professional activity; interpersonal: ability to generate innovative creative ideas, promot reasoned conclusions; system: ability to be guided and adapt to new working conditions. object: ability to describe open scientific researches and projects on chemistry of synthetic and natural organic compounds. Prerequisites: organic chemistry, chemistry of natural and high molecular compounds, physical chemistry, chemical technology and catalysis. STRUCTURE AND CONTENT OF DISCIPLINE Title of subject Week Hours Ball Module 1 1 Lecture. Introduction. Sources of organic compounds. Current development of organic synthesis. Fundamental and practical significance. 1 2 2 Seminar. Methods of industrial processing of organic compounds. Updated classical and novel synthetic methods. Retrosynthetic analysis. Lecture. Strategy and tactic of organic synthesis. Seminar. Technological processes and devices. 2 Lecture. 12 Principles of green chemistry. 1 Seminar. “Green” chemical processes and technologies. 2 9 SWM 1. Use of computer programs in organic synthesis. 1 6 4 Lecture. Application of microwave methods in green chemical 1 5 technologies. Seminar. "Green chemical technologies” part 1. Green chemistry of silicon-containing compounds. Lecture. Technology of application of green mechanochemical methods. 3 Seminar. "Green chemical technologies” part 2. Green chemistry of nitrogencontaining compounds: achievements and application. SWM 2. Chemistry of acetylene: achievements and prospects. 6 Lecture. Application of ultrasonic methods in green chemical 7 technologies. Seminar. "Green chemical technologies” part 3. Green chemistry of oxygen-containing compounds: achievements and application. Lecture. New ways of phosphorus activation. Seminar. "Green chemical technologies” part 4. Phosphorus-containing compounds. Traditional and “green” methods of synthesis, application and significance for development of Kazakhstan economy. SWM 3. Sulphur-, phosphorus-containing compounds: thiophosphates, 9 1 2 9 9 1 2 9 1 1 6 2 9 1 2 9 1 6 phosphorus pentasulphides. Colloquium 8 19 100 Lecture. New ways of sulfur activation: mechanical, microwave, using superbasic medium. Seminar. "Green chemical technologies” part 5. Green chemistry of 1 2 8 sulphur-containing compounds: achievements and application. 100 MidTermExam Module 2 Lecture. Nanochemistry and nanomaterials: classification, preparation, stabilization, investigation and application. 1 Seminar. Nanotechnology. 2 8 SWM 4. Carbon nanotubes: synthesis, investigation and application. 1 5 Lecture. Supramolecular chemistry. 1 Seminar. Supramolecules: synthesis and properties. 2 Lecture. Chemistry and technology of dendrimers. 1 Seminar. Synthetic methods for dendritic molecules. Special chemical 2 8 1 5 12 reactions of dendritic molecules. Special properties and potential application. SWM 5. Rotaxanes and polyrotaxanes: synthesis and supramolecular structures. Lecture. Chemistry of calixarenes. 2 13 Seminar. Thiacalixarenes, calixarenes: synthesis, structure, application in chemistry and biology. Lecture. Combinatorial synthesis: principles, tools and advantages. Seminar. Design of pharmaceuticals molecules. Combinatorial synthesis 2 8 1 1 5 2 8 9 10 11 14 15 of acyclic structures. SWM 6. Single molecular chemistry. Lecture. Ionic liquids: structure, activation, application in science, biotechnology, energy, chemistry. Seminar. Laboratory and industrial methods of preparation and purification of ionic liquids. Lecture. Superacids and superbases: structure, activation mechanisms and application. Seminar. Superacids and superbases for organic synthesis. SWM 7. Femtochemistry. Colloquium Exam 8 1 8 1 1 2 8 1 5 16 100 100 REFERENCES Basic 1. Смит В.А., Дильман А.Д. Основы современного органического синтеза. М.: Бином, 2009. – 750с. 2. Смит В.А., Бочков А., Кейпл Р. Органический синтез. М.: 2001. 3. Tsutomu Ishikawa. Superbases for Organic Synthesis: Guanidines, Amidines, Phosphazenes and Related Organocatalysts. John Wiley & Sons, 2009. – 340 р. 4. Guozhong Cao, Ying Wang. Nanostructures and Nanomaterials: Synthesis, Properties & Applications (2nd edition). Singapore: World Scientific Publishing Co. Pte Ltd, 2010. – 520 p. 5. Vogtle F., Richardt C., Werner N. Dendrimer chemistry. Wiley-WCh Verlag, 2009. – 350p. 6. Лебедев Н.Н. Химия и технология основного органического и нефтехимического синтеза. М.: Химия, 1975. 7. Балоян Б.М., Колмаков А.Г., Алымов М.И., Кротов А.М. Наноматериалы. Классификация, особенности свойств, применение и технологии получения. Москва, 2007. – 125с. 8. Гусев А.И. Наноматериалы, наноструктуры, нанотехнологии. – М.: Физматлит, 2005. – 416с. 9. Cергеев Г.Б. Нанохимия. М.: МГУ, 2003. – 288с. 10. Тимохин Б.В., Дмитриченко М.Ю. Основы комбинаторного синтеза: теоретическое пособие. – Иркутск: Иркут. ун-т, 2003. – 40с. 11. Федорова О.А. Супрамолекулярная химия: учеб. пособие.– М.: РХТУ им. Д.И. Менделеева, 2010. – 204 с. 1. 2. 3. 4. 5. 6. Кобояси Н. Введение в нанотехнологию. М.: 2008. Успехи химии. 1998-2010 гг. Журнал органической химии. 2000-2010 гг. Журнал Россииского общества им. Д.И. Менделеева. 1999-2008 гг. Нефтехимия. 1998-2010 гг. Толстиков А.Г., Толстиков Г.А. и др. Современные проблемы асимметрического синтеза. Екатеринбург. 2008. 207 с. ACADEMIC POLICY OF COURSE All types of works need to be done in time. Master students, who have not done task or have got less than 50% of balls can fulfill task according to additional schedule. Master students, who missed laboratory lessons due to good reason, need to fulfill these lessons after admission of teacher in an extra time in the presence of laboratory assistant. Master students, who did not carry out all types work, are not allowed to exam. Master students activity and lessons attendance are evaluated. Tolerance and respecting of other person’s opinion are requested. Correct formulation of objections is also needed. Plagiarism and other forms of dishonest activity are unacceptable. Writing off during pass the SWM and exam, copying of tasks by other persons, passing an exam instead of other master students are inadmissible. Master student, convicted of falsification of any information, unauthorized access to the Internet, using cribs will be evaluated "F". Consultations on SWM, exam and other questions will be given by teacher during his working time. Evaluation by alphabetic system А АВ+ В ВС+ С СD+ DF I P Digital ball equivalent 4,0 3,67 3,33 3,0 2,67 2,33 2,0 1,67 1,33 1,0 0 - Percentage 95-100 90-94 85-89 80-84 75-79 70-74 65-69 60-64 55-59 50-54 0-49 0-60 65-100 Evaluation by traditional system Excellent Good Satisfactory Unsatisfactory Incomplete Pass NP - W AW AU АT. - Not AT R - 0-29 0-64 30-60 50-100 0-29 0-49 - No Pass Withdrawal Academic Withdrawal Audit Attested Not attested Retake Syllabus is approved at the meeting of department of chemistry and technology of organic substances, natural compounds and polymers, protocol № 1, August 28, 2014. Chair of department of chemistry and technology of organic matters, natural compounds and polymers G.A. Mun Lecturer N.N. Chopabayeva