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X-ray particle image velocimetry for measuring quantitative flow information inside opaque objects Sang-Joon Lee and Guk-Bae Kim Citation: Journal of Applied Physics 94, 3620 (2003); doi: 10.1063/1.1599981 View online: http://dx.doi.org/10.1063/1.1599981 View Table of Contents: http://scitation.aip.org/content/aip/journal/jap/94/5?ver=pdfcov Published by the AIP Publishing Articles you may be interested in Wall-parallel stereo particle-image velocimetry measurements in the roughness sublayer of turbulent flow overlying highly irregular roughness Phys. Fluids 25, 115109 (2013); 10.1063/1.4832377 Optimization of in-line phase contrast particle image velocimetry using a laboratory x-ray source J. Appl. Phys. 112, 074701 (2012); 10.1063/1.4757407 Note: Development of a compact x-ray particle image velocimetry for measuring opaque flows. II. Threedimensional velocity field reconstruction Rev. Sci. 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Downloaded to ] IP: 119.202.87.44 On: Fri, 22 May 2015 02:21:02 JOURNAL OF APPLIED PHYSICS VOLUME 94, NUMBER 5 1 SEPTEMBER 2003 X-ray particle image velocimetry for measuring quantitative flow information inside opaque objects Sang-Joon Leea) and Guk-Bae Kim Department of Mechanical Engineering, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784, South Korea 共Received 6 May 2003; accepted 18 June 2003兲 An x-ray particle image velocimetry 共PIV兲 technique was developed to measure quantitative information on flows inside opaque objects. To acquire x-ray images suitable for PIV velocity field measurements, refraction-based edge enhancement was employed using detectable tracer particles with the object and detector separated by an experimentally determined optimal distance. The x-ray PIV method was applied to a flow in an opaque Teflon tube. The resulting amassed velocity field data were in reasonable agreement with theoretical predictions. © 2003 American Institute of Physics. 关DOI: 10.1063/1.1599981兴 I. INTRODUCTION Flow visualization has become an indispensable tool in the investigation of complex flow structures. Recent advances in digital image processing techniques have made it possible to extract quantitative information from visualized flow images. In contrast to conventional pointwise velocity measurement devices such as hot-wire anemometry or laser Doppler velocimetry, the generation of quantitative flow visualization methods enable the rapid collection of data covering the entire velocity field. Particle image velocimetry 共PIV兲, which uses digital image processing of tracer particles seeded in a flow, has come to be accepted as a reliable and powerful velocity field measurement technique.1 The basic principle of PIV is as follows.1 Tracer particles are seeded into the flow of interest and images of those particles are recorded twice with a short time interval (⌬t) on a recording medium such as a charge coupled device 共CCD兲 camera. Particle displacements are then determined by comparing the two flow images; these displacements are divided by the time interval ⌬t to extract the instantaneous velocity field data. By ensemble averaging many instantaneous velocity fields, the spatial distributions of the mean velocity or turbulent statistics of the flow can be obtained. Because conventional PIV systems use a laser as the light source, they can be applied only to transparent fluids with a transparent window. Therefore, conventional PIV technique is ill suited to measuring the flow characteristics of nontransparent fluids or fluids confined in opaque materials. To overcome these limitations of conventional PIV, we need to use a transmission-type light source such as an x-ray or ultrasonic wave source instead of a laser. In the present study, we developed a PIV velocity field measurement technique in which an x-ray beam is the light source. For measuring flow velocity fields using this technique, we established an x-ray image enhancement method and optimized the experimental conditions such as the object–detector disa兲 Author to whom correspondence should be addressed; electronic mail: [email protected] tance and type of tracer particle. The measurement of the entire velocity field of a single-phase flow enclosed in an opaque material has not been reported yet. To visualize tracer particles inside an opaque tube, third generation synchrotron radiation sources of the Pohang Light Source 共Pohang, Korea兲 were used. The high coherence of this light source offers various approaches to radiology.2– 6 Several imaging techniques utilizing coherent light sources, such as holography and interferometry, have been intensively studied, and some phase contrast imaging methods have been announced recently.7–10 In conventional PIV, velocity vectors are extracted by flow images of tracer particles illuminated with a laser beam. In x-ray PIV, however, the refraction or Fresnel edge diffraction mechanism of an x-ray beam can be used to improve the image quality.2– 6 The relative weights of refraction and Fresnel edge diffraction in x-ray imaging depend on the experimental conditions, the type of specimen, and the information to be extracted.11 II. EDGE ENHANCEMENT BY REFRACTION An x-ray beam of sufficient coherence can induce the classic Fresnel edge diffraction pattern in radiological images. In general, the fringe pattern by edge diffraction becomes clearer as the object–detector distance is increased. The performance of diffraction-based edge detection depends on several factors such as beam monochromaticity, source size, and lateral resolution of the detector.11 However, the details of the diffraction mechanism are beyond the scope of this paper because refraction-based imaging was mainly used in this study. Refraction-based edge enhancement occurs because specimen regions with different real parts of the refractive index induce different lateral displacements of a collimated x-ray beam. Figure 1 shows a schematic diagram of a refraction-based mechanism of edge enhancement in radiographs. When an object with a tapered edge is illuminated by a plane-wave x-ray beam, absorption of the x-ray beam by the object decreases the beam intensity and refraction at the 0021-8979/2003/94(5)/3620/4/$20.00 3620 © 2003 American Institute of Physics [This article is copyrighted as indicated in the article. Reuse of AIP content is subject to the terms at: http://scitation.aip.org/termsconditions. Downloaded to ] IP: 119.202.87.44 On: Fri, 22 May 2015 02:21:02 J. Appl. Phys., Vol. 94, No. 5, 1 September 2003 FIG. 1. Schematic diagram of a refraction-based method of edge enhancement. edge displaces the beam by a small angle ␣. The angle ␣ is determined by the slope of the taper at the edge and the real part of the refractive index of the object. The angular displacement leads to the formation of a highly illuminated area and a darker area on the detector. This fringe effect enhances the visibility of the edge in the recorded x-ray image. The distance A between the dark and bright fringes on the detector depends on the width of the tapered edge. The width B of each fringe is given by B⬇r 0 ␣ , where r 0 is the distance between the object and the detector. As indicated by this relation, the refraction-based edge enhancement becomes blurred at large r 0 . If r 0 is very small, on the other hand, the lateral resolution of the fringe on the detector is too small to identify the edge. Thus, the refraction-based method is effective only over a certain range of object–detector distances. In contrast to the diffraction method, the refraction method does not require that the x-ray beam be longitudinally coherent 共monochromatic兲. The refraction-based method therefore depends on the morphology of body to be measured and the object–detector distance.11 III. EXPERIMENTAL PROCEDURE AND RESULTS In this study, we fixed the object–detector distance at a value at which refraction-based edge enhancement occurs but diffraction-based edge enhancement is not detected. One of the main motivations for using this approach is that, in comparison to the diffraction-based method, the refractionbased method can be available without a monochromatic device and this means that we can acquire higher intensity of x-ray beam. Although PIV based on x rays is theoretically feasible, it was not easy to find suitable tracer particles that satisfy the requirements of both x-ray imaging and PIV. For tracer particles to be suitable for x-ray PIV, they must have two characteristics, including the tendency to closely track the working fluid and to be detectable by x-ray beam with the edge enhancement. To find particles with suitable characteristics, we tested several particle types including polystyrene, glass bead, microcale bubbles as well as polymer and alumina (Al2 O3 ) microspheres. In this research, we selected microspheres of alumina (Al2 O3 ), a strong absorber of x rays, as the tracer particles. When an alumina particle is imaged using refraction-based edge detection, the highly illuminated S. Lee and G. Kim 3621 FIG. 2. Schematic diagram of experimental setup for x-ray PIV measurements. fringe gets buried in the absorptive area inside the particle and the dark fringe becomes distinct at the surface of the particle. With some preliminary testing, we found the optimum object–detector distance for the specific morphology of alumina microspheres. The experiments were performed at the ‘‘white beam’’ line 共1B2兲 of the Pohang Light Source. Figure 2 shows a schematic diagram of the experimental setup used for the x-ray PIV measurements. X-ray particle images were recorded on a CCD camera after converting the x rays to visible light with a thin CdWO4 scintillator crystal. The lateral resolution (⌬x) was better than 5 m when the CCD camera was coupled to a 10⫻ objective lens. Because the x-ray beam was continuous, we installed a mechanical shutter to generate double x-ray pulses for the PIV velocity field measurements. A delay generator was used to synchronize the mechanical shutter and the CCD camera. The time interval between consecutive images was fixed at 20 ms. The x-ray PIV technique was applied to a vertical liquid flow in an opaque Teflon tube with an inner diameter of 750 m. The tracer particles 共alumina microspheres兲 had a mean diameter of 3 m and a density of 3.965 g/cm3 . To match the specific weight of the alumina particles, glycerin (1.260 g/cm3 ) was used as the working fluid. The working fluid seeded with tracer particles was injected into the microtube by a syringe pump at a mean velocity of 0.5 mm/s. The field of view was about 1.5⫻1.5 mm2 and the spatial resolution was 12.3 ⫻12.3 m2 . A two-frame cross-correlation PIV algorithm was applied to each pair of consecutive x-ray particle images to obtain the corresponding instantaneous velocity field. Figure 3 shows a typical raw image acquired using the x-ray imaging technique based on the refraction method. The object-detector distance was fixed at 30 cm in consideration of the morphology of the alumina microspheres. The tiny dark points densely filling the vertical tube indicate the alumina seed particles. The large dark stains and small bright spots are artifacts caused by flaws on the scintillator surface. This particle image is suitable for PIV analysis to extract the instantaneous velocity vector field. Figure 4 shows the streamwise mean velocity field obtained by ensemble averaging 100 instantaneous velocity fields. The bright area near the wall indicates low velocity [This article is copyrighted as indicated in the article. Reuse of AIP content is subject to the terms at: http://scitation.aip.org/termsconditions. Downloaded to ] IP: 119.202.87.44 On: Fri, 22 May 2015 02:21:02 3622 J. Appl. Phys., Vol. 94, No. 5, 1 September 2003 S. Lee and G. Kim FIG. 5. Amassed velocity distribution for circular pipe flow. FIG. 3. A typical particle image acquired using the x-ray imaging technique. and the dark area at the tube center indicates high velocity. The bright spots observed in the ensemble averaged velocity field are artifacts due to flaws on the scintillator surface. The velocity data obtained by x-ray PIV contain amassed flow information in the direction of x-ray propagation, because the x-ray image contains all particles located inside the pathway of the x-ray beam. Such amassed flow information gives x-ray PIV the remarkable ability to directly measure amassed volumetric flow information. Thus, x-ray PIV can be used to measure the volumetric flow rate of any liquid enclosed within an opaque material, for example the rate of blood flow in a living organism. For twodimensional or axisymmetric flows, the velocity field information in a cross section of the flow can be obtained using a mathematical formula derived based on a simple assumption. The three-dimensional particle displacement data in a volume can be obtained by utilizing a tomography technique in x-ray PIV. Figure 5 shows a schematic diagram of the amassed flow velocity distribution in a circular tube. For laminar flow in a circular tube installed in the vertical direction, the velocity distribution can be expressed as follows using the Navier– Stokes equations and Poiseuille’s law U共 r 兲⫽ 冉 R 2 ⌬p ⫹g 4 l 冊冋 冉 冊 册 1⫺ r R 冋 冉 冊册 2 r R ⫽V max 1⫺ 2 , where R is the radius of circular tube, is dynamic viscosity of fluid, ⌬ p is the pressure drop, l is a length along the tube, is density of fluid, and g is the local acceleration of gravity. The following amassed velocity distribution can then be obtained from the relationship r 2 ⫽x 2 ⫹y 2 and integration of the velocity profile. 2 U Amassed共 x 兲 ⫽ 冕 冑R 2 ⫺x 2 0 冋 冉 冊 冉 冊册 V max 1⫺ x R 2 ⫺ y R 2 dy 2 冑R 2 ⫺x 2 冋 冉 冊册 x 2 ⫽ V max 1⫺ 3 R 2 . Thus, the amassed velocity profile is only two-thirds of the theoretical velocity profile for flow in a circular pipe. Figure 6 shows a typical streamwise mean velocity profile extracted from the mean velocity field data along a horizontal line. The theoretical velocity profile at the center section U(r) and the theoretical amassed velocity profile U AmTh(x) are included for comparison. The maxima of the experimental and theoretical amassed velocity profiles (U AmExp(x) and U AmTh(x)) are put on the same position for comparison with each other. The amassed velocity profile obtained using x-ray PIV has a parabolic shape and a magnitude that is about two thirds of the center-sectional velocity profile, as mentioned above. However, the measured amassed velocity profile has slightly higher values than the theoretical profile in the region of large velocity gradient. This discrepancy seems to be due to the density difference between the working fluid and the alumina particles. The effect of the larger gravity of the alumina particles seems to be pronounced in the near-wall region, where the fluid velocity is slower, even though the gravitational acceleration is constant across the entire cross section. FIG. 4. Ensemble-averaged streamwise mean velocity field. [This article is copyrighted as indicated in the article. Reuse of AIP content is subject to the terms at: http://scitation.aip.org/termsconditions. Downloaded to ] IP: 119.202.87.44 On: Fri, 22 May 2015 02:21:02 J. Appl. Phys., Vol. 94, No. 5, 1 September 2003 S. Lee and G. Kim 3623 found to be 30 cm; at this distance the refraction-based edge enhancement was employed for acquiring a clear x-ray particle image. The tracer particles used in x-ray PIV should closely track the working fluid flow and be detectable using the refraction-based method. In the present work alumina microspheres were selected as the tracer particles. However, the density of these alumina particles was higher than that of the working fluid. Despite the difference in density between the particles and working fluid, we measured the quantitative velocity field information inside an opaque tube using the x-ray PIV technique. X-ray PIV has potential applications in diverse research areas and can be used as a powerful tool for resolving many unsolved fluid mechanical problems. One example that would be particularly well suited to study using x-ray PIV is blood flow inside living bodies. FIG. 6. Comparison of streamwise mean velocity profiles: 共—兲 theoretical center-sectional velocity profile; 共 兲 theoretical amassed velocity profile; 共¯"兲 measured amassed velocity profile. IV. CONCLUSION ACKNOWLEDGMENT The present work was financially supported by POSRIP 共POSTECH Research Initiative Program兲 of POSTECH. R. J. Adrian, Annu. Rev. Fluid Mech. 23, 261 共1991兲. A. Snigirev, I. Snigireva, V. Kohn, S. Kuznetsov, and I. Schelokov, Rev. Sci. Instrum. 66, 5486 共1995兲. 3 D. Chapman et al., Phys. Med. Biol. 42, 2015 共1997兲. 4 A. Pogany, D. Gao, and S. W. Wilkins, Rev. Sci. Instrum. 68, 2774 共1997兲. 5 K. A. Nugent, T. E. Gureyev, D. F. Cookson, D. Paganin, and Z. Barnea, Phys. Rev. Lett. 77, 2961 共1996兲. 6 G. Margaritondo and G. Tromba, J. Appl. Phys. 85, 3406 共1999兲. 7 C. Raven, A. Snigirev, I. Snigireva, P. Spanne, A. Souvorov, and V. Kohn, Appl. Phys. Lett. 69, 1826 共1996兲. 8 Z. H. Hu, P. A. Thomas, A. Snigirev, I. Snigireva, A. Souvorov, P. G. R. Smith, G. W. Ross, and S. Teat, Nature 共London兲 392, 690 共1998兲. 9 P. Spanne, C. Raven, I. Snigireva, and A. Snigirev, Phys. Med. Biol. 44, 741 共1999兲. 10 T. E. Gureyev, C. Raven, A. Snigirev, I. Snigireva, and S. W. Wilkins, J. Phys. D 32, 563 共1999兲. 11 Y. Hwu et al., J. Appl. Phys. 86, 4613 共1999兲. 1 In this study we have devised and begun to explore an x-ray PIV velocity field measurement technique. The proposed technique can be used to obtain quantitative information on the entire flow field of flows enclosed by opaque materials. The main contribution of this study is that it establishes the optimum conditions for acquiring good x-ray particle images from which velocity vectors can be extracted. We established the refraction-based edge enhancement method for x-ray particle imaging, conducted experiments to select the suitable material for the tracer particles, and optimized the object–detector distance for the refraction-based edge enhancement method and the chosen tracer particles. The optimal distance between the object and detector was 2 [This article is copyrighted as indicated in the article. Reuse of AIP content is subject to the terms at: http://scitation.aip.org/termsconditions. Downloaded to ] IP: 119.202.87.44 On: Fri, 22 May 2015 02:21:02