Download Statistics and chemometrics for analytical chemistry

Faculty of Science
Department of
science
Time of lectures:
Instructor:
Office hours:
Instrumental Analysis 1
1 ‫التحليل االلي‬
111111
Prerequisite (s): 111231
2015/2016
Semester: 1st
Lecture room (s) :
Text books & References:
1) Principles of Instrumental Analysis Fifth Edition,
Skoog Holler. Nieman (Harcourt)
Text Book
2) Statistics and Chemometrics for analytical chemistry
J. N. Miller
Other
References
Course Description:
Course outline:
Week
Topic details
1.
Statistics and chemometrics for analytical chemistry
1.
Errors in quantitative analysis Chapter 1
Types of error
planning and design of experiments. (Experimental
Design)
2.
Calibration methods in instrumental analysis / Regression
and correlation. Chapter 5
2.1 Introduction: instrumental analysis 107
2.2 Calibration graphs in instrumental analysis.
2.3 The product-moment correlation coefficient.
2.4 The line of regression of y on x.
2.5 Errors in the slope and intercept of the regression
line.
2.6 Calculation of concentration and its random error.
2.7 Limits of detection.
2.8 The method of standard addition.
2.9 Weighted regression lines.
3. Principles Spectrophotometric methods of analysis
Chapter 6:
An Introduction to Spectrometric Methods
116
6A
General Properties of Electromagnetic Radiation
116
6B
Wave Properties of Electromagnetic Radiation
117
6C
Quantum-Mechanical Properties of Radiation
128
6D
Quantitative Aspects of Spectrochemical
Measurements
138
Chapter 7
Components of Optical Instruments
143
General Designs of Optical Instruments
Sources of Radiation
Wavelength Selectros
Sample Containers
Radiation Transducers
Types of Optical Instruments
143
145
154
166
167
181
7A
7B
7C
7D
7E
7H
-2Chapter 8
8A
8B
8C
An Introduction to Optical Atomic
Spectrometry
Optical Atomic Spectra
Atomization Methods
Sample Introduction Methods
192
192
200
201
Chapter 9
9E
Atomic Absorption and Atomic
Fluorescence Spectrometry
Sample Atomization Techniques
Atomic Absorption Instrumentation
Interferences in Atomic Absorption
Spectroscopy
Atomic Absorption Analytical
Techniques
Atomic Fluoresence Spectroscopy
Section III
Molecular spectroscopy
Chapter 13
An introduction to ultraviolet / visible
molecular absorption spectrometry.
Chapter 14
Application of ultravioleted / visible
molecular absorption spectrometry.
Chapter 15
Molecular luminescence spectrometry.
Chapter 16
An Introduction to Infrared spectrometry
9A
9B
9C
9D
206
206
213
217
223
225
Section V
4. Separation Methods
673
Chapter 26
674
26A
26B
26C
26D
26E
Chapter 27
27A
An Introduction to Chromatographic
Separations
A General Description of
Chromatography
Migration Rates of Solutes
Zone Broadening and Column
Efficiency
Optimization of Column Performance
Summary of Important Relationships for
Chromatography
Gas Chromatography 701
Principles of Gas-Liquid
675
678
680
687
695
702
27B
27C
Chapter 28
28A
28B
28C
Chromatography
Instruments for Gas-Liquid
Chromatography
Gas Chromatographic Columns and
Stationary Phases
High-Performance Liquid
Chromatography 725
Scope of HPLC
Column Efficiency in Liquid
Chromatography
Instruments for Liquid Chromatography
Applications of HPLC
703
711
726
726
728
Attendance Policies:
 Be Punctual.
 Attendance is mandatory. Students are not allowed to miss more than 15% of the
lectures, without acceptable real cause.
 If a student misses more that 15 % of the course lectures, she/he will forfeit the course
credits. After this, medical reports may be submitted for evaluation, for a total absence
of no more than 20%. If student misses more than 20% of lectures, regardless of the
cause, the course will be failed.
Grading system:
Assessment
First Exam
Second Exam
Activities and Evaluation
Final Examination
Total
Grade
25%
25%
10%
40%
100%