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LASER ULTRASONIC STUDY OF CRACK TIP DIFFRACTION M. Ochiai1, D. Levesque2, R. Talbot2, A. Blouin2, A. Fukumoto1 and J.-P. Monchalin2 1 Power and Industrial Systems R&D Center, Toshiba Corp., Yokohama 235-8523 Japan 2 Industrial Materials Institute, National Research Council Canada, Boucherville, PQ, J4B6Y4 Canada ABSTRACT. Ultrasonic diffraction pattern at a crack tip and crack depth sizing based on the diffraction are studied by using laser-generated bulk waves. Directivity patterns oriented essentially along the normal for the diffracted longitudinal wave and essentially at 45 (deg) for the diffracted shear wave for any incident angles is obtained. A laser-ultrasonic system combined with time-offlight (TOFD) analysis is produced and demonstrates accurate crack sizing on an artificial slot having a variable depth from 0 mm to 10 mm. An improvement of signal-to-noise ratio by split spectrum processing (SSP) is also suggested. INTRODUCTION Regarding defect inspection, not only detecting but also sizing of cracks is desirable because a depth of the crack is one of the most important parameter to evaluate deteriorations of the materials. Ultrasonic testing (UT) is an inspection technique widely used in a field of non-destructive evaluation (NDE) and some UT methods based on detection of diffraction waves from a crack tip are considered as the most reliable technique to measure a depth of the crack in a material. The time-of-flight diffraction (TOFD) is a technique sensing the crack tip diffraction, in which the depth and the location of the crack are analyzed by the time-of-flight analysis [1]. On the other hand, laser technique offers non-contact remote maintenance and is suitable to be used for components having complicated shape installed in narrow space. Compact and flexible optical fibres easily deliver laser beams into such narrow space and also simple optical mechanisms easily scan small laser spots following onto such contour surfaces. In general, TOFD is a technique based on two-probes pitch-catch measurement and piezoelectric transducers (PZTs) are utilized for both the generation CP657, Review of Quantitative Nondestructive Evaluation Vol. 22, ed. by D. O. Thompson and D. E. Chimenti © 2003 American Institute of Physics 0-7354-0117-9/03/$20.00 1489 and the detection of ultrasonic waves. One technique that enables laser-based TOFD is to use a laser-ultrasonics, which means an ultrasonic wave generation by a laser pulse and its detection by an optical interferometer [2]. Recently, a few techniques to size surfacebreaking cracks have been proposed by using laser-generated surface wave [3-5], although these can be useful only for the shallower cracks, say a depth of less than a few mm, in principle. TOFD technique combined with laser-ultrasonics has been also attempted by using surface-skimming wave [6] and bulk waves [7]. These successes are however limited by relatively poor sensitivity of the laser-based detection systems. This paper will describe a performance of complete laser ultrasonic TOFD system on realistic tight cracks. Details of diffraction patterns at a crack tip measured by a highly sensitive laser-based detection system will be presented. Then sizing capability of laser ultrasonic TOFD system will be demonstrated by using a surface-breaking artificial slot. Finally, stress corrosion cracking (SCC), which is one of the most severe and potentially dangerous deteriorations in nuclear plants, in a stainless steel plate are examined by using the laser ultrasonic TOFD method. A typical B-scan containing diffraction signals from SCC and a result will be presented. A further signal processing to improve a signal-to-noise ration (SNR) of diffraction indication will be proposed. EXPERIMETAL METHODS FOR LASER ULTRASONIC TOFD An experimental configuration of laser ultrasonic TOFD is outlined in Fig.l. Ultrasonic waves were generated by Q-switched Nd:YAG laser pulses having a wavelength of 532nm, a pulse duration of about 10ns and a repetition rate of lOHz. Pulse energies of 75mJ were delivered to the sample surface. These energies are quite intense but are still below the threshold for optical fibre delivery [8]. A lens mounted on a 1dimensional scanning stage (x'- direction) was used to focus the laser pulses onto the sample surface with a diameter of about 100jj,m. The fluence at the surface was estimated about IkJ/cm2 and this produced ablation plasma at each irradiated spots. This method of excitation simultaneously generated a various ultrasonic modes; surface-skimming longitudinal waves (P), Rayleigh waves (R), bulk longitudinal waves (L), bulk shear waves (S) in the sample medium and shock waves (A) originated from the expansion of ablation plasma in air. These waves except for the shock wave had frequencies of, typically, 0.5MHz to 20MHz and respective particular directivities. Ultrasonic waves generated by the incident laser pulse and travelling in the medium were detected using an optical detection system based on a confocal FabryPerot interferometer [9]. Two multimode optical fibres having a core diameter of 400|Lim were employed; one fibre was used to deliver light from the detection laser to the sample surface, while the other FIGURE 1. Experimental set up for laser ultrasonic TOFD. 1490 one was used to bring scattered light back to the interferometer. The detection laser was a fundamental NdiYAG laser having a wavelength of l,064nm. This detection laser emitted long pulses (typically, 70|us) with highly stabilized frequency and high peak power (typically, IkW). The confocal Fabry-Perot is 1m long and has an optical bandwidth of from 2MHz to 12MHz, approximately. A PIN photodiode detected the light demodulated by the Fabry-Perot. The detected signal was high-pass-filtered with a cut off frequency of 1MHz and amplified by 40dB. The signals were sampled with a sampling rate of lOOMsample/s and stored for the signal processing in a personal computer. This computer also controlled the synchronization between the emissions of two laser sources and the scan of the sample. A sample to be tested was fixed on a 3-dimensional scanning stage (x-, y-, zdirections as shown in Fig.l). A combination of these stages (x-, x'-, y- and z-direction) enabled to adjust focus (z-direction), to change scanning location (y-direction) and to scan the detection and generation spots independently (x- and x'-directions). EXPERIMENTAL RESULTS Amplitude Profiles of Crack Tip Diffraction Theoretical models have been already constructed to describe the diffraction of ultrasound, by considering infinite plane elastic waves incident on a semi-infinite crack having no width [10, 11]. In the case of laser-generated ultrasound, the incident waves can be usually assumed as spherical waves because the generation source, in other words, a laser spot for generation, is very small compared to the generated ultrasonic wavelengths. However, the incident energies of ultrasound to the tip greatly depend upon the incident angle due to the particular emission pattern of laser-generated ultrasound [12]. As it is well known, in ablation regime, directivity of the laser-generated longitudinal wave is essentially normal to the surface and of the laser-generated shear wave is angled typically from 30° to 60°. Diffraction patterns of a tip were interrogated by using the setup. A stainless steel plate having a thickness of 15mm was used. A surface-breaking artificial slot (EDM notch) having a dimension of 15mm(L) x 0.3mm(W) x 10mm(D) was machined in a surface. The generation and detection laser beams were irradiated onto the surface opposite to the slot. Each laser beam was scanned on the surface independently; the generation spot was scanned to cover the incident angle, /?, to the tip from 0° to 76° by 400 points while the detection spot was scanned to cover the receiving angle, 0, from the tip from -63° to +63° by 100 points. Typically, step angles were from 0.6° at ft =0° to 0.03° at /?=76° for the generation and from 2.3° at 0 =0° to 0.47° at 0 =±63° for the detection. Because of the same geometrical reason, it is noted that the difference of travelling distance in both generation and detection should be considered in order to calibrate the amplitude of diffracted. 1491 (a) LdfL-wave (b) SdfS-wave FIGURE 2. Diffraction pattern at a crack tip. A total of 100 waveforms (100 different angles of detection) was used to reconstruct a 2-dimensional image of B-scan for each incident angle (generation position). The amplitude profiles of the diffraction signals were extracted from the B-scans. Typical patterns are plotted as polar graphs in Fig.2. In each graph, the tip is located at the origin and the direction of the incident wave is shown as a black arrow. Diffraction patterns of the LdfL-waves with incident angles from 0° to 60° are shown in Fig.2(a) and diffraction patterns of the SdfS-waves with the same range of incident angles are shown in Fig.2(b). The maximum amplitude of the LdfL-waves is observed at the reception angle of 0° and the amplitude becomes smaller with the increase of the incident angle. As to the SdfSwaves, the maximum amplitude is observed at the reception angle of about 45° in any incident angles and the amplitude becomes the largest with the incident angle of 45°. These patterns should involve the effects of the emission pattern of laser-generated ultrasound, the diffraction pattern of the tip and the difference of travelling distance. It is noted that the notation of "df' means that the signal was produced by the diffraction at the tip, for example, "LdfS" means a diffraction signal from the tip where the wave was incoming to as L-wave, diffracted and mode-converted at and outgoing from as S-wave. Calibration with Artificial Slots For crack orientation in direction vertical to the surface, the depth and the location of the crack can be evaluated through simple geometrical analysis in TOFD. Although there can be some variations in TOFD, the basic configuration is the scanning transversal to the crack as shown in Fig.3. The generation and detection spots launched onto the same surface of the tested sample with a separation of 2S. Assuming there is a diffraction source, such as a crack tip, at a location of x from the centre of the separation and the depth of d in the medium, the travelling time of the diffraction signal, £diff, is given by ,————————— ,—:——————- ' - x)2 + J(d f diff ~ Generation Detection Separation 25 (D ^ where v is an ultrasonic velocity in the medium. The time ?diff should be always longer than the travelling time of P-wave, tp, and shorter than one of the bottom echo, t\» here b=LL or SS. As 1492 £———1 —— ^.JL^ ^\^ 4 'I $ Depth d .............V..................... Crackl FIGURE 3. TOFD configuration for crack. scanning the generation and detection spots, the time ^iff becomes minimum at the point of jc=0. The center position of the generation and detection shows the location of the crack. In this case, the crack depth, d, is determined by --S2 d= (2) As previously discussed, the maximum amplitude of diffraction signal is given by the LdfL-wave with both the incident and the reception angle of 0°. This however means that the generation and detection spots should be superimposed at the same position on the sample surface. In this case, the R-wave and A-wave, both of which have much larger amplitude than any bulk waves, will arrive during the time to be observed and the relatively small diffraction signals will be hidden by these waves. It is preferable that the arrival of R-wave, £R, which is usually earlier than that of A-wave, should be later than one of the bottom echo of interest. To assess the performance of laser ultrasonic TOFD system, a series of experiments was carried out by using a stainless steel plate (15mm-thick) containing an EDM notch. The depth of the artificial slot varies linearly from Omm to 10mm along the direction of the slot length of 40mm (Fig.4). Some points ranging in depth from Omm to 10mm on the slot were examined by generating each B-scan image from a series of Ascan waveforms. The separation between the generation and the detection spots was fixed in 20mm and the sample, which is equivalent to scanning the laser spots simultaneously, Initial Position Generation Detection Separation: 2Q ran Final Position Generation Detection 120mm m i Position (mm) FIGURE 5. Typical B-scan containing the FIGURE 4. Experimental setting for calibration. diffraction trace. — 1- — _ _| _ |_ _j _ — -\" ~ ~ 1~ — - t- -t - 1- - -t- - — 1- — - h -t - 1- -'•- : - -1 - t- -t - -1 - 1- -1 - 4 - 1- 4 - - 4 - — 4- — _ |_ 4 _ |_ . - 4- - - -t - 1- -t- - -t - 1- -t - p § _ J. _ _ _l _ . 4 _ l_ 4 _ _ J. _ _ 1_ _ _ L _L _ l_ . ~ -' 1 1 I . I I I I I I I . . I | | I 1 1 1 1 I 1 1 1 1 1 A 1 1 1 s M-fch4 *r *r-[ * - T~ ~~ r ~ - r -T - r - - -t - 1- 4 - - 4- _ 4 _ 1- 4 - - +- - - 1- 4 - 1- - t- - _ i_ _f _ i_ _ - i- - — U 4 — 1— - - -\ - r ~r - J 'i 4 - 4 - h- 4 - S1 U 4 _ I I I I 1 1 1 1 1 1 ^1If ^4^ - + - : - 4- - - H - 1- H - H - h- -1 - -1 - U 4 - I . ffi 2 n _ J _ L _L _ _ 1 _ _ L _ _ L J _ L _ 1 1 1 1 I I I . 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0 2 4 - . J _L _ 1_ 1 1 1 1 1 1 I I 1 6 8 J _ 1 1 I - - - -t- -\ *•> - — K -/-f ,\| 4I 1 A? 1 \- -t- H - — 1 - - ~ Q 1 fc 1 1 * 0 i^H !* 1 I if -\ h 1 t- - ~7 ^ \A /\ ( i i t- 1- - - h/i } 1 - - --- *4 00 0 1 o 1 1- -t 1 1 L» / L i. L J. . 1 1 | 2 t- 4 e a 10 Nominal Depth (mm) FIGURE 6. Propagation times of the Nominal Depth (mm) FIGURE 7. Relation between measured diffraction the wave at the peak. and designed depths. 1493 was scanned by 40mm along the direction perpendicular to the slot length. A-scan waveforms were obtained with an interval of 0.05mm so that a total of 800 waveforms were used to reconstruct a 2-dimensional image of B-scan. A typical B-scan, which x-axis corresponds to the position of the generation spot, y-axis corresponds to the time and plotted colour corresponds to the signal amplitude, are shown in Fig.5. Each image contains an arc-shape tracing the LdfL diffraction signal. The trace should appear between the arrival of P-wave and LL-wave and the peak of it gives the slot depth according to the equation (2) as well as the slot location. The minimum arrival time of each arc was measured in each B-scan and was plotted as a function of the designed slot depth in Fig.6. By using a proper ultrasonic velocity (in this case v=5,850m/s is used as the velocity of longitudinal wave), the slot depth was estimated for each measurement with enough accuracy as shown in Fig.7. Results on SCC Samples The laser-ultrasonic TOFD technique was used to inspect a stainless steel plate (100mm(L) x 50mm(W) x 10mm(D)) that contained a few stress corrosion cracks. These SCCs have less than O.lmm wide. The generation and detection spots were separated by 15mm and were irradiated onto the surface opposite to the opening of SCCs. The sample was scanned for 40mm with a step size of 0.05mm. The unprocessed B-scan, Fig.8, shows the presence of the SCC as an arc-shape indication, even though it is not as clearly distinguished as the artificial slots as shown in Fig.5. The crack depth was estimated as 4mm as it is expected by the microscopic observation from the sidewall. To improve SNR and to enhance the crack image in the B-scan, split spectrum processing (SSP) [13] was attempted. SSP is a method where one wideband ultrasonic pulse is filtered through a digitally implemented filter bank. The filter outputs are fed through some nonlinear operation to create a final signal where the coherent noises have been eliminated. The filter bank consists of a certain number of band pass filters of different centre frequencies but constant bandwidth. The output signals are normalized and compounded using algorithms such as minimization or polarity thresholding. The result is shown in Fig.9. » li Position (mm) FIGURE 8. A result of TOFD analysis FIGURE 9. A result of TOFD analysis on SCC sample (unprocessed). on SCC sample (SSP). 1494 DISCUSSION As discussed, although the best SNR is obtained when the detection and generation spots are superimposed, the detection should be separated from the generation by a certain distance. On the contrary, the depth evaluation becomes very difficult if on uses too wide separation (too large incident and detection angle). In fact, even the artificial slot, it was impossible to find an indication and to evaluate the slot depth on the slot of 9mm and 10mm deep, corresponding to the incident angles of more than 60°, by using LdfL-wave mode. From this point of view, the shear wave, which has an angled emission pattern, seems to be an alternative. It should be however noted that the diffraction patterns of shear wave (dfS-wave) have null amplitude at some diffraction angles. Therefore, the separation should be determined based on the assumed crack depth when the shear wave is used on TOFD. In the present approach, the dominant noise is originated from ultrasonic propagation, such as backscattering from grains; it means sensitivity of the detection system is not essential for the detectability. To eliminate this kind of coherent noise, we focused on the frequency dependence of the noises. SSP and laser ultrasonics are good combination because laser ultrasonics is a broadband generation and detection technique that what SSP requires. As shown in Fig.8 and 9, SSP is an effective method to improve SNR; however good results can be obtained only if all parameters, such as number of filters and bandwidth of individual filters, are carefully tuned. There will be another approach that uses averaging techniques. Although both temporal and spatial averaging techniques may improve the SNR, spatial averaging with different propagation paths is superior because temporal averaging cannot eliminate coherent noises. The synthetic aperture focusing technique (SAFT) [14- 16], which collects many contributions with proper calibrations from different propagation paths, offers an attractive alternative, although this technique usually requires relatively much time to acquire many data and to execute complex signal processing. CONCLUSION TOFD linked with laser-ultrasonics offers a well understood method based on relatively simple data acquisition and processing to size a crack. We have reported that the technique is capable to size slot depths from 0.2mm to 8.5mm in a type 304 stainless steel plate having a thickness of 15mm without any averaging and/or filtering. However, in the cases when the ultrasonic noises in the material to be inspected are large or the crack is small, SNR becomes poor and this causes a problem on TOFD evaluation. The particular emission pattern of laser-generated ultrasounds is one of the reasons of this poor SNR. The interrogated diffraction patterns of a slot tip have shown that the diffracted L-wave appears the direction normal to the sample surface while the diffracted S-wave appears at the diffraction angle of about 45°. The best SNR was obtained with the incident and diffraction angles of 0°; however, this configuration was not convenient for TOFD processing. The use of narrower separation or the use of shear 1495 wave can be alternatives; these however sometimes make the measurements unreliable because the signal can be overlapped by the other waves or disappeared. To overcome SNR problem, the use of SSP was suggested. Although results of SSP were very sensitive to the parameters in the processing, it has been shown that the SNR is improved by using carefully tuned parameters. SSP is a method essentially based on the frequency domain analysis; the results should be therefore similar to one obtained by a band pass filter. The other possibility is to use temporal or spatial averaging technique, such as SAFT. REFERENCES 1. Silk, M.G., Research Techniques in Non-destructive Testing, Vol.III, Academic Press, New York, 1977 2. Scruby, C.B., et al., Laser Ultrasonics, Technique and Applications, Hilger, Bristol, 1990 3. Cooper, J.A., et al., "Surface acoustic wave interactions with cracks and slots: a noncontacting study using lasers" IEEE Trans. Ultrason. Ferroelectr. Frequency Contr., UFFC-33, 5, (1986) 462 4. Scala, C.M., et al., "Laser ultrasonics for surface-crack depth measurement using transmitted near-field Rayleigh waves," Rev. Prog, in QNDE (QNDE'99), Montreal, PQ, 1999,19A. (1999) 327 5. Ochiai, M., et al., "Sizing of micro cracks using laser-induced broad-band surface waves," J. At. Energy Soc. Japan, 43, 3 (2001) 275 (in Japanese) 6. Shan, Q., et al., "Surface-breaking fatigue crack detection using laser ultrasound," /. Appl Phys. Lett., 62, 21, (1993) 2649 7. Mihara, T., et al., "Laser ultrasonic TOFD method," Rev. Prog, in QNDE (QNDE'OO), Ames, IA, 2000, 20A. 255 8. Schmidt-Uhlig, T. et al., "Laser shock processing with 20 MW laser pulses delivered by optical fibers," Eur. Phys. J. AP., 9 (2000) 235 9. Monchalin, J.P., et al., "Optical detection of ultrasound," IEEE Trans. Ultrason. Ferroelectr. Frequency Contr., UFFC-33, (1986) 485 10. Ogilvy, J.A. et al., "Diffraction of elastic waves by cracks: application to time-offlight inspection," Ultrasonics, 21 (1983) 259 11. Temple, J.A.G., "Time-of-flight inspection: theory," Nucl. Energy, 22 (1983) 335 12. Hutchins, D.A., "Directivity patterns of laser-generated ultrasound in aluminum," /. Acoust. Soc. Am. 70 (1981) 1362 13. Karpur, P., et al., "Split spectrum processing: determination of the available bandwidth for spectral splitting," Ultrasonics, 26 (1988) 204 14. Blouin, A., et al., "SAFT data processing applied to laser-ultrasonic inspection," Rev. Prog, in QNDE (QNDE'97), San Diego, CA, 1997,17A. 611 (1997) 15. Levesque, D., et al., "Improved performance of laser-ultrasonic F-SAFT imaging," Rev. Prog, in QNDE (QNDE'98), Snowbird, UT, 1998, ISA, 309 (1998) 16. Ochiai, M., et al., "Visualization of surface-breaking tight cracks by laser-ultrasonic F-S AFT,"to be presented in QNDE (QNDE' 02) 1496