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List of Publications Prof. Ing. Michal Holčapek, Ph.D. Papers - International Journals (114): 1/ P. Jandera, M. Holčapek, G. Theodoridis, J. Chromatogr. A 813 (1998) 299-311. Investigation of Chromatographic Behaviour of Ethoxylated Alcohol Surfactants in Normal-Phase and Reversed-Phase Systems Using High-Performance Liquid Chromatography - Mass Spectrometry. 2/ M. Holčapek, H. Virelizier, J. Chamot-Rooke, P. Jandera, C. Moulin, Anal. Chem. 71 (1999) 2288-2293. Trace Determination of Glycols by HPLC with UV and Electrospray Ionization Mass Spectrometric Detections. 3/ M. Holčapek, P. Jandera, Rapid Commun. Mass Spectrom. 13 (1999) 1423-1426. Interpretation of Electrospray and Atmospheric Pressure Chemical Ionization Mass Spectra of 10-Formyl-7,8-Dihydrofolic Acid and 5-Formyl-5,6,7,8-Tetrahydropteroic Acid. 4/ M. Holčapek, P. Jandera, J. Přikryl, Dyes Pigm. 43 (1999) 127-137. Analysis of Sulphonated Dyes and Intermediates by Electrospray Mass Spectrometry. 5/ M. Holčapek, P. Jandera, J. Fischer, B. Prokeš, J. Chromatogr. A 858 (1999) 13-31. Analytical Monitoring of the Production of Biodiesel by High-Performance Liquid Chromatography with Various Detection Methods. 6/ P. Jandera, M. Holčapek, L. Kolářová, J. Chromatogr. A 869 (2000) 65-84. Retention Mechanism, Isocratic and Gradient-Elution Separation and Characterization of (co)Polymers in Normal-Phase and Reverse-Phase High-Performance Liquid Chromatography. 7/ K. Lemr, M. Holčapek, P. Jandera, A. Lyčka, Rapid Commun. Mass Spectrom. 14 (2000) 1881-1888. Analysis of Metal Complex Azo Dyes by High-Performance Liquid Chromatography/Electrospray Ionization Mass Spectrometry and Multistage Mass Spectrometry. 8/ K. Lemr, M. Holčapek, P. Jandera, Rapid Commun. Mass Spectrom. 14 (2000) 18781879. Oxygen Attachment to the Metal Complex Ions during their Collision Induced Dissociation in the Ion Trap. 9/ M. Sedlák, J. Hanusek, M. Holčapek, V. Štěrba, J. Phys. Org. Chem. 14 (2001) 187-195. Kinetics and Mechanism of the Methanolysis and Cyclisation of 1-Acyl-3-(2-halogeno-5nitrophenyl)thioureas. 10/ M. Holčapek, P. Jandera, J. Fischer, Crit. Rev. Anal. Chem. 31(1) (2001) 53-56. Analysis of Acylglycerols and Methyl Esters of Fatty Acids in Vegetable Oils and in Biodiesel. 11/ P. Jandera, M. Holčapek, L. Kolářová, Int. J. Polym. Anal. Charact. 6 (2001) 261-294. Retention Behavior of Oligomers and Cooligomers in Reversed-phase and in Normalphase Interactive Liquid Chromatographic Systems. 12/ M. Holčapek, P. Jandera, P. Zderadička, J. Chromatogr. A 926 (2001) 175-186. High Performance Liquid Chromatography - Mass Spectrometric Analysis of Sulphonated Dyes and Intermediates. 13/ A. Lyčka, D. Luštinec, J. Holeček, M. Nádvorník, M. Holčapek, Dyes Pigm. 50 (2001) 203-209. -1- 27 14/ 15/ 16/ 17/ 18/ 19/ 20/ 21/ 22/ 23/ 24/ 25/ Al, 15N, 13C and 1H NMR Spectra and Negative-ion Electrospray Mass Spectra of the 2:1 Aluminium(III) Complexes of Azo Dyes Derived from Anthranilic Acid. M. Sedlák, V. Buchta, L. Kubicová, P. Šimůnek, M. Holčapek, P. Kašparová, Bioorg. Med. Chem. Lett. 11 (2001) 2833 - 2835. Synthesis and Characterisation of a New Amphotericin B-methoxypoly(ethylene glycol)conjugate. A. Růžička, L. Dostál, R. Jambor, V. Buchta, J. Brus, I. Císařová, M. Holčapek, J. Holeček, Appl. Organometal. Chem. 16 (2002) 315 - 322. Structure and in vitro antifungal activity of [2,6bis(dimethylamino)phenyl]diphenyltin(IV) compounds. R. Jambor, L. Dostál, A. Růžička, I. Císařová, J. Brus, M. Holčapek, J. Holeček, Organometallics 21 (2002) 3996 - 4004. Organotin(IV) Derivatives of some O,C,O-chelating Ligands. A. Klásek, K. Kořistek, A. Lyčka, M. Holčapek, Tetrahedron 59 (2003) 1283 - 1288. Unprecedented Reactivity of 3-Amino-1H,3H-quinoline-2,4-diones with Urea: An Efficient Synthesis of Novel 2,6-Dihydro-imidazo[1,5-c]quinazoline-3,5-diones. A. Růžička, A. Lyčka, R. Jambor, P. Novák, I. Císařová, M. Holčapek, M. Erben, J. Holeček, Appl. Organometal. Chem. 17 (2003) 168 - 174. Structure of Azo Dye Organotin(IV) Compounds Containing a C,N-chelating Ligand. A. Klásek, K. Kořistek, A. Lyčka, M. Holčapek, Tetrahedron 59 (2003) 5279-5288. Reaction of 1-Alkyl/aryl-3-Amino-1H,3H-quinoline-2,4-diones with Urea. Synthetic Route to Novel 3-Amino-1,3-dihydro-2H-indol-2-ones, 1H-spiro[imidazolidine-5,3'indole]-2,2'-diones, and 3,3a-dihydro-5H-imidazo[4,5-c]quinoline-2,4-diones. M. Nobilis, J. Kopecký, J. Květina, Z. Svoboda, M. Pour, J. Kuneš, M. Holčapek, L. Kolářová, J. Pharm. Biomed. Anal. 32/4-5 (2003) 641-656. Comparative Biotransformation and Disposition Studies of Nabumetone in Humans and Minipigs Using High-performance Liquid Chromatography with Ultraviolet and Massspectrometric Detection. D. Ansorgová, M. Holčapek, P. Jandera, J. Sep. Sci. 26 (2003) 1017-1027. Ion-pairing High-performance Liquid Chromatography - Mass Spectrometry of Impurities and Reduction Products of Sulphonated Azodyes. M. Holčapek, P. Jandera, P. Zderadička, L. Hrubá, J. Chromatogr. A 1010 (2003) 195215. Characterization of Triacylglycerol and Diacylglycerol Composition of Plant Oils Using High-performance Liquid Chromatography - Atmospheric Pressure Chemical Ionization Mass Spectrometry. J. Přikryl, A. Lyčka, V. Bertolasi, M. Holčapek, V. Macháček, Eur. J. Org. Chem. 22 (2003) 4413-4421. Structure and Reactivity of 1-(5-Nitrobenzo[c]-1,2-thiazol-3-yl)-3,3-disubstituted Triazenes. M. Holčapek, K. Volná, P. Jandera, L. Kolářová, K. Lemr, M. Exner, A. Církva, J. Mass Spectrom. 39 (2004) 43-50. Effects of Ion-pairing Reagents on the Electrospray Signal Suppression of Sulphonated Dyes and Intermediates. J.D.J. van den Berg, N.D. Vermist, L. Carlyle, M. Holčapek, J.J. Boon, J. Sep. Sci. 27 (2004) 181-199. Effects of Traditional Processing Methods of Linseed Oil on the Composition of its Triacylglycerols. -2- 26/ 27/ 28/ 29/ 30/ 31/ 32/ 33/ 34/ 35/ 36/ 37/ M. Nobilis, M. Holčapek, L. Kolářová, J. Kopecký, M. Kuneš, Z. Svoboda, J. Květina, J. Chromatogr. A 1031 (2004) 229-236. Identification and determination of Phase II nabumetone metabolites by HPLC-PDA-MS analyses. V. Wsól, B. Szotáková, V. Baliharová, L. Šišpera, M. Holčapek, L. Kolářová, B. Suchanová, M. Kuchař, L. Skálová, Collection Czech. Commun. 69 (2004) 689-702. In vitro biotransformation study of the potential antileukotrienic drug quinlukast in rat. R. Hrdina, D. Luštinec, P. Stolín, L. Burgert, S. Luňák, M. Holčapek, Adv. Colour Sci. Technol. 7 (2004) 6-17. Iron Complexes of Reactive Azo Dyes. L. Kolářová, M. Holčapek, R. Jambor, L. Dostál, A. Růžička, M. Nádvorník, J. Mass Spectrom. 39 (2004) 621-629. Structural Analysis of 2,6-[bis(alkyloxy)methyl]phenyltin Derivatives Using Electrospray Ionization Mass Spectrometry. L. Korecká, Z. Bílková, M. Holčapek, J. Královský, M. Beneš, J. Lenfeld, N. Minc, R. Cecal, J.-L. Viovy, M. Przybylski, J. Chromatogr. B 808 (2004) 15-24. Utilization of newly developed immobilized enzyme reactors for preparation and study of immunoglobulin G fragments. A. Sakalis, D. Ansorgová, M. Holčapek, P. Jandera, A. Voulgaropoulos, Int. J. Environ. Anal. Chem. 84(11) (2004) 875-888. Analysis of Sulphonated Azodyes and Their Degradation Products in Aqueous Solutions Treated with a New Electrochemical Method. A. Klásek, A. Lyčka, M. Holčapek, I. Hoza, Tetrahedron 60 (2004) 9953-9961. Reaction of 3-aminoquinoline-2,4-diones with nitrourea. Synthetic route to novel 3ureidoquinoline-2,4-diones and imidazo[4,5-c]quinoline-2,4-diones. T. S. Basu Baul, W. Rynjah, R. Willem, M. Biesemans, I. Verbruggen, M. Holčapek, D. de Vos, A. Linden, J. Organometal. Chem. 689 (2004) 4691-4701. Dibutyltin(IV) complexes of the 5-[(E)-2-(Aryl)-1-diazenyl]-2-hydroxybenzoic acid ligand: an investigation of structures by X-ray diffraction, solution and solid state tin NMR, electrospray ionisation MS and assessment of in vitro cytotoxicity. A. Lyčka, A. Klásek, K. Kořistek, M. Holčapek, Sci. Pap. Univ. Pardubice, Ser. A 10 (2004) 155 - 164. 1 H- 15 N NMR correlation study of reaction products of some 3-amino-1H,3H-quinoline-2,4-diones with urea. T. S. Basu Baul, K. S. Singh, A. Lyčka, M. Holčapek, A. Linden, J. Organometal. Chem. 690 (2005) 1581-1587. Synthesis of a cyclic dinuclear organotin carboxylate via simultaneous debenzylation and decarbonylation reactions: X-ray crystal structure of [(PhCH2)2{O2CC6H4{N(H)N=(C6H3-4(=O)-5-O)}-o}Sn]2. P. Císař, M. Nobilis, Z. Vybíralová, M. Holčapek, L. Kolářová, M. Pour, J. Kuneš, J. Klimeš, J. Pharm. Biomed. Anal. 37 (2005) 1059-71. Disposition Study of a New Potential Antineoplastic Agent Dimefluron in Rats Using High-performance Liquid Chromatography with Ultraviolet and Mass Spectrometric Detection. T.S. Basu Baul, C. Masharing, R. Willem, M. Biesemans, M. Holčapek, R. Jirásko, A. Linden, J. Organometal. Chem. 690 (2005) 3080-3094. Self-assembly of diorganotin(IV) 2-{[(E)-1-(2-oxyaryl)alkylidene]amino}acetates: An investigation of structures by X-ray diffraction, solution and solid state tin NMR, -3- 38/ 39/ 40/ 41/ 42/ 43/ 44/ 45/ 46/ 47/ 48/ 49/ electrospray ionisation MS. T. S. B. Baul, K. S. Singh, M. Holčapek, R. Jirásko, A. Linden, X. Song, A. Zapata, G. Eng, Appl. Organometal. Chem. 19 (2005) 935-944. Electrospray ionization mass spectrometry of tributyltin(IV) complexes and their larvicidal activity on mosquito larvae; crystal and molecular structure of polymeric (Bu3Sn[O2CC6H4{N=N(C6H3-4-OH(C(H)=NC6H4OCH3-4))}-o])n. M. Holčapek, M. Lísa, P. Jandera, N. Kabátová, J. Sep. Sci. 28 (2005) 1315-33. Quantitation of Triacylglycerols in Plant Oils Using HPLC with APCI-MS, Evaporative Light-Scattering, and UV Detection. T.S.B. Baul, K.S. Singh, M. Holčapek, R. Jirásko, E. Rivarola, A. Linden, J. Organometal. Chem. 690 (2005) 4232-4242. Synthesis, characterization and crystal structures of polymeric and dimeric triphenyltin(IV) complexes of 4-[((E)-1-{2-hydroxy-5-[(E)-2-(2-carboxyphenyl)-1diazenyl]phenyl}methylidene)amino]aryls. A. Klásek, A. Lyčka, M. Holčapek, I. Hoza, J. Heterocycl. Chem. 43 (2006) 203-211. Reaction of 3-aminoquinoline-2,4-diones with isocyanates. Synthesis of novel 3-(3'alkyl/arylureido)quinoline-2,4-diones and their cyclic carbinolamide tautomers. T. S. B. Baul, C. Masharing, S. Basu, E. Rivarola, M. Holčapek, R. Jirásko, A. Lyčka, D. de Vos, A. Linden, J. Organomet. Chem. 691 (5) (2006) 952-965. Synthesis, characterization, cytotoxic activity and crystal structures of tri- and di-organotin(IV) complexes constructed from the beta-{[(E)-1-(2-hydroxyaryl)alkylidene]amino}propionate and beta-{[(2Z)-(3-hydroxy-1-methyl-2-butenylidene)]amino}propionate skeletons J. Vinklárek, H. Paláčková, J. Honzíček, J. Holubová, M. Holčapek, I. Císařová, Inorg. Chem. 45(5) (2006) 2156-2162. Investigation of Vanadocene(IV) alpha-Aminoacid Complexes: Synthesis, Structure, and Behavior in Physiological Solutions, Human Plasma, and Blood. K. Volná, M. Holčapek, P. Suwanruji, H.S. Freeman, Color. Technol. 122(1) (2006) 2226. Mass Spectrometric Analysis of Sulphonated Dyes based on Diaminobiphenyl. F. Bureš, T. Szotkowski, J. Kulhánek, O. Pytela, M. Ludwig, M. Holčapek, Tetrahedron: Asymmetry 17 (2006) 900-907. Novel nitrogen ligands based on imidazole derivatives and their application in asymmetric catalysis. T.S.B. Baul, A. Mizar, X. Song, G. Eng, R. Jirásko, M. Holčapek, R. Willem, M. Biesemans, I. Verbruggen, R. Butcher, J. Organomet. Chem. 691(12) (2006) 2605-2613. Dibenzyltin(IV) complexes of the 5-[(E)-2-(aryl)-1-diazenyl)quinolin-8-olates: synthesis and an investigation of structures by X-ray diffraction, solution and solid state tin NMR, 119 Sn Mössbauer and electrospray ionization MS. M. Nobilis, Z. Vybíralová, K. Sládková, M. Lísa, M. Holčapek, J. Květina, J. Chromatogr. A 1119(1-2) (2006) 299-308. HPLC determination of 5-aminosalicylic acid and its metabolites in biomatrices. M. Holčapek, L. Kolářová, A. Růžička, R. Jambor, P. Jandera, Anal. Chem. 78 (2006) 4210-4218. Structural Analysis of Ionic Organotin(IV) Compounds Using Electrospray Tandem Mass Spectrometry. T. S. B. Baul, A. Mizar, A. Lyčka, E. Rivarola, R. Jirásko, M. Holčapek, D. de Vos, U. Englert, J. Organomet. Chem. 691(16) (2006) 3416-3425. -4- 50/ 51/ 52/ 53/ 54/ 55/ 56/ 57/ 58/ 59/ 60/ Diphenyltin(IV) complexes of the 5-[(E)-2-(aryl)-1-diazenyl)quinolin-8-olates: Synthesis and multinuclear NMR, 119Sn Mössbauer, Electrospray ionization MS, X-ray characterization and assessment of in vitro cytotoxicity. D. Vaněrková, A. Sakalis, M. Holčapek, P. Jandera, A. Voulgaropoulos, Rapid Commun. Mass Spectrom. 20(19) (2006) 2807-2815. Analysis of electrochemical degradation products of sulphonated azodyes using HPLC/MS/MS. T.S.B. Baul, W. Rynjah, E. Rivarola, A. Lyčka, M. Holčapek, R. Jirásko, D. de Vos, R.J. Butcher, A. Linden, J. Organomet. Chem. 691 (2006) 4850-4862. Synthesis and characterization of bis[dicarboxylatotetraorganodistannoxane] units involving 5-[(E)-2-(Aryl)-1-diazenyl]-2-hydroxybenzoic acids: An investigation of structures by X-ray diffraction, NMR, electrospray ionisation MS and assessment of in vitro cytotoxicity. A. Klásek, A. Lyčka, M. Holčapek, M. Kovář, I. Hoza, J. Heterocyclic Chem. 43 (2006) 1251-1260. Molecular Rearrangement of 1-Substituted 3-Aminoquinoline-2,4-diones in Their Reaction with Urea and Nitrourea. Synthesis and Transformations of Reaction Intermediates. M. Lísa, M. Holčapek, T. Řezanka, N. Kabátová, J. Chromatogr. A 1146 (2007) 67-77. HPLC/APCI-MS and GC/FID Characterization of )5-Olefinic Fatty Acids in Triacylglycerols From Conifer Seed Oils. M. Nobilis, T. Jira, M. Lísa, M. Holčapek, B. Szotáková, J. Lamka, L. Skálová, J. Chromatogr. A 1149(1) (2007) 112-120. Achiral and chiral high-performance liquid chromatographic determination of flubendazole and its metabolites in biomatrices using UV photodiode-array and mass spectrometric detection. A. Sakalis, D. Vaněrková, M. Holčapek, P. Jandera, A. Voulgaropoulos, Chemosphere 67 (2007) 1940-1948. Electrochemical Treatment of a Simple Azodye and Analysis of the Degradation Products Using High-performance Liquid Chromatography - Diode Array Detection Tandem Mass Spectrometry. M. Holčapek, K. Volná, D. Vaněrková, Dyes Pigm. 75(1) (2007) 156-165. Effects of Functional Groups on the Fragmentation of Dyes in Electrospray and Atmospheric Pressure Chemical Ionization Mass Spectra. M. Nobilis, M. Pour, J. Pavlík, P. Šenel, J. Kuneš, M. Vopršalová, L. Kolářová, M. Holčapek, J. Chromatogr. B 853 (2007) 10-19. Metabolic profiling of a new potential antifungal drug, 3-(4-bromophenyl)-5acetoxymethyl-2,5-dihydrofuran-2-one, in mice urine using high-performance liquid chromatography with photodiode-array and mass spectrometric detections. J. Maláková, M. Nobilis, Z Svoboda, M. Lísa, M. Holčapek, J. Květina, V. Palička, J. Chromatogr. B 853 (2007) 265-274. HPLC Method with Fluorescence and Mass Spectrometric Detection for Simultaneous Determination of Galantamine and Its Phase I Metabolites in Biological Samples. B. Barrett, M. Holčapek, J. Huclová, V. Bořek-Dohalský, P. Fejt, B. Němec, I. Jelínek, J. Pharm. Biomed. Anal. 44 (2007) 498-505. Validated HPLC–MS/MS method for determination of quetiapine in human plasma. R. Jirásko, M. Holčapek, L. Kolářová, T.S. Basu Baul, J. Mass Spectrom. 42(7) (2007) 918-928. -5- 61/ 62/ 63/ 64/ 65/ 66/ 67/ 68/ 69/ 70/ 71/ 72/ Electrospray Ionization Mass Spectrometry of Complex Organotin Compounds Containing More Tin Atoms. T.S.B. Baul, W. Rynjah, E. Rivarola, C. Pettinari, M. Holčapek, R. Jirásko, U. Englert, A. Linden, J. Organometal. Chem. 692 (2007) 3625-3635. Di-n-octyltin(IV) complexes with 5-[(E)-2-(Aryl)-1-diazenyl]-2-hydroxybenzoic acid: Syntheses and assessment of solid state structures by 119Sn Mössbauer and X-ray diffraction, and further insight into the solution structures using electrospray ionization MS, 119Sn NMR and variable temperature NMR spectroscopy. A. Klásek, A. Lyčka, M. Holčapek, Tetrahedron 63(30) (2007) 7059-7069. Molecular rearrangement of 1-substituted 9b-hydroxy-3,3a,5,9b-tetrahydro-1Himidazo[4,5-c]quinoline-2,4-diones - an unexpected pathway to new indole and imidazolinone derivatives. A. Popkov, M. Nádvorník, V. Langer, R. Jirásko, M. Holčapek, T. Weidlich, A. Lyčka, J. Labelled Comp. Rad. 50(2007) 554-555. New Chiral Synthons of 13C- and 15N-Labelled "-amino Acids. T.S.B. Baul, C. Masharing, G. Ruisi, R. Jirásko, M. Holčapek, D. de Vos, A. Linden, J. Organomet. Chem. 692 (2007) 4849–4862. Self-assembly of extended Schiff base amino acetates 2-{[(2Z)-(3-hydroxy-1-methyl-2butenylidene)]amino}phenylpropionate and 2-{[(E)-1-(2hydroxyaryl)alkylidene]amino}- phenylpropionate skeletons incorporating organotin(IV) moiety: Synthesis, spectroscopic characterization, crystal structures, and in vitro cytotoxic activity. M. Lísa, F. Lynen, M. Holčapek, P. Sandra, J. Chromatogr. A 1176 (2007) 135-142. Quantitation of Triacylglycerols in Plant Oils Using Charged Aerosol Detector. M. Holčapek, M. Lísa, K. Volná, J. Přikryl, N. Almonasy, J. Mass Spectrom. 42(12) (2007) 1645. Occurrence of Radical Molecular Ions in Atmospheric Pressure Chemical Ionization Mass Spectra of Heterocyclic Compounds. K. Volná, M. Holčapek, L. Kolářová, K. Lemr, J. Čáslavský, P. Kačer, J. Poustka, M. Hubálek, Rapid Commun. Mass Spectrom. 22 (2008) 101-108. Development of electrospray ionization mass spectral library of sulfonated dyes and comparison of MS/MS spectra obtained using various mass spectrometers. Š. Frebort, N. Almonasy, R. Hrdina A. Lyčka, M. Lísa, M. Holčapek, Collection Czech Chem Commun 73 (2008) 107-115. Synthesis and characterization of dialkyl esters of 1,2,4,5-tetrazine-3,6-dicarboxylic acid. H. Sovová, M. Lísa, M. Holčapek, Eur. J. Lipid Sci. Technol. 110 (2008) 266-276. Estimation of stereospecific fatty acid distribution in vegetable oils from liquid chromatography data. A. Klásek, A. Lyčka, M. Holčapek, I. Hoza, Helv. Chim. Acta 91 (2008) 354-370. New Approaches to the Synthesis of 4-(2-Aminophenyl)imidazolin-2-ones and 3Ureidoindoles and a Study of their Interconversion. M. Holčapek, L. Kolářová, M. Nobilis, Anal. Bioanal. Chem. 391 (2008) 59-78. High-performance liquid chromatography - tandem mass spectrometry in the identification and determination of phase I and phase II drug metabolites. M. Lísa, M. Holčapek, J. Chromatogr. A 1998-1999 (2008) 115-130. Triacylglycerols Profiling in Plant Oils Important in Food Industry, Dietetics and Cosmetics Using High-Performance Liquid Chromatography - Atmospheric Pressure Chemical Ionization Mass Spectrometry. -6- 73/ 74/ 75/ 76/ 77/ 78/ 79/ 80/ 81/ 82/ 83/ 84/ 85/ D. Kahoun, S. Rezková, K. Veškrnová, J. Královský, M. Holčapek, J. Chromatogr. A 1202 (2008) 19-33. Identification and quantification of phenolic compounds and hydroxymethylfurfural in meads using RP-HPLC with coulometric-array and UV detection. R. Jirásko, M. Holčapek, L. Kolářová, M. Nádvorník, A. Popkov, J. Mass Spectrom. 43 (2008) 1274-1284. Characterization of Ni(II) Complexes of Schiff Bases of Amino Acids and (S)-NBenzylproline (2-Benzoylphenyl)amide Using Ion Trap and QqTOF Electrospray Ionization Tandem Mass Spectrometry. T.S.B. Baul, A. Mizar, A.K. Chandra, X. Song, G. Eng, R. Jirásko, M. Holčapek, D. de Vos, A. Linden, J. Inorg. Biochem. 102(9) (2008) 1719-1730. Synthesis, crystal structures, cytotoxicity and qualitative structure-activity relationship (QSAR) of cis-bis{5-[(E)-2-(aryl)-1-diazenyl]quinolinolato}di-n-butyltin(IV) complexes, n Bu2Sn(L)2. M. Nádvorník, V. Langer, R. Jirásko, M. Holčapek, T. Weidlich, A. Lyčka, A. Popkov, Polyhedron 27 (2008) 3477-3483. Syntheses, X-ray, MSn, NMR and CD structure determination of nickel(II) complexes of Schiff bases of (S)-N-(2-benzoylphenyl)-1-benzylpyrrolidine-2-carboxamide and aromatic "-amino acids. R. Jirásko, M. Holčapek, E. Rosenberg, Int. J. Mass Spectrom. 280 (2009) 198-203. Characterization of bis-carboxyethyl germanium sesquioxide and its complexes with amino acids using electrospray QqTOF mass spectrometry. M. Lísa, H. Velínská, M. Holčapek, Anal. Chem. 81 (2009) 3903-3910. Regioisomeric Characterization of Triacylglycerols Using Silver-Ion HPLC/MS and Randomization Synthesis of Standards. M. Lísa, M. Holčapek, M. Boháč, J. Agric. Food Chem. 57 (2009) 6888–6898. Statistical Evaluation of Triacylglycerol Composition In Plant Oils Based on HighPerformance Liquid Chromatography - Atmospheric Pressure Chemical Ionization Mass Spectrometry Data. L. Česlová, M. Holčapek, M. Fidler, J. Drštičková, M. Lísa, J. Chromatogr. A 1216 (2009) 7249-7257. Characterization of xanthohumol related compounds and hops bitter acids in various classes of beer and hops varieties using high-performance liquid chromatography atmospheric pressure chemical ionization mass spectrometry. M. Lísa, M. Holčapek, H. Sovová, J. Chromatogr. A 1216 (2009) 8371-8378. Comparison of various types of stationary phases in HPLC/MS analysis of glycerolipids in blackcurrant oil and products of its enzymatic hydrolysis. M. Holčapek, H. Velínská, M. Lísa, P. Česla, J. Sep. Sci. 23 (2009) 3672-3680. Orthogonality of silver-ion and non-aqueous reversed-phase HPLC/MS in the analysis of complex natural mixtures of triacylglycerols. M. Holčapek, M. Lísa, Lipid Technol., 21 (2009) 261-265. Statistical evaluation of triacylglycerol composition by HPLC/APCI-MS. M. Holčapek, R. Jirásko, M. Lísa, J. Chromatogr. A 1217(25) (2010) 3908-3921. Basic rules for the interpretation of atmospheric pressure ionization mass spectra of small molecules. R. Jirásko, M. Holčapek, E. Vrublová, J. Ulrichová, V. Šimánek, J. Chromatogr. A 1217(25) (2010) 4100-4108. Identification of new phase II metabolites of xanthohumol in rat in vivo -7- 86/ 87/ 88/ 89/ 90/ 91/ 92/ 93/ 94/ 95/ 96/ 97/ biotransformation of hop extracts using high-performance liquid chromatography electrospray ionization tandem mass spectrometry. A. Popkov, J. Hanusek, J. Čermák, V. Langer, R. Jirásko, M. Holčapek, M. Nádvorník, J. Radioanal. Nucl. Chem. 285 (2010) 621-626. Development of metallocomplex amino acids synthons for the asymmetric preparation of "-amino acids by stereoselective introduction of a side chain. Evaluation of the model asymmetric preparation of alanine and b-13C monolabelled "-aminoisobutyric acid M. Holčapek, H. Dvořáková, M. Lísa, A. J. Girón, P. Sandra, J. Cvačka, J. Chromatogr. A 1217 (2010) 8186-8194. Regioisomeric analysis of triacylglycerols using silver-ion liquid chromatography–atmospheric pressure chemical ionization mass spectrometry: Comparison of five different mass analyzers. R. Jirásko, M. Holčapek, M. Nobilis, Rapid Commun. Mass Spectrom. 25 (2011) 21532162. Identification of Phase I and Phase II metabolites of benfluron and dimefluron in rat urine using high-performance liquid chromatography / tandem mass spectrometry M. Lísa, E. Cífková, M. Holčapek, J. Chromatogr. A 1218 (2011) 5146-5156. Lipidomic profiling of biological tissues using off-line two-dimensional highperformance liquid chromatography - mass spectrometry. R. Jirásko, M. Holčapek, Mass Spectrom. Rev. 30 (2011) 1013-1036. Structural analysis of organometallic compounds with soft ionization mass spectrometry. M. Lísa, K. Netušilová, L. Franěk, H. Dvořáková, M. Holčapek,J. Chromatogr. A 1218 (2011) 7499-7510. Characterization of fatty acid and triacylglycerol composition in animal fats and fish oils using silver-ion and non-aqueous reversed-phase high-performance liquid chromatography - mass spectrometry and gas chromatography - flame ionization detection. I. Vokřál, R. Jirásko, V. Jedličková, H. Bártíková, L. Skálová, J. Lamka, M. Holčapek, B. Szotáková, Vet. Parasitol. 185 (2012) 168-174. The inability of tapeworm Hymenolepis diminuta and fluke Dicrocoelium dendriticum to metabolize praziquantel. Z. Jalový, Z. Padělková, R. Jirásko, R. Matyáš, M. Holčapek, O. Němec, M. Novotná, L. Mišková, Polyhedron 44(1) (2012) 88-100. Syntheses, crystal structures and properties of copper(II) complexes of 1-amidinoisourea and biguanide nitrates. M. Holčapek, R. Jirásko, M. Lísa, J. Chromatogr. A 1259 (2012) 3-15. Recent developments in liquid chromatography - mass spectrometry and related techniques. E. Cífková, M. Holčapek, M. Lísa, M. Ovčačíková, A. Lyčka, F. Lynen, P. Sandra, Anal. Chem. 84 (2012) 10064-10070. Non-targeted quantitation of lipid classes using hydrophilic interaction liquid chromatography - electrospray ionization mass spectrometry using single internal standard and response factor approach. L. Stuchlíková, R. Jirásko, J. Lamka, B. Szotáková, I. Vokřál, M. Holčapek, H. Bártíková, L. Skálová, Anal. Bioanal. Chem. 405 (2013) 1705-1712. Investigation of the metabolism of monepantel in ovine hepatocytes by UHPLC/MS/MS M. Lísa, M. Holčapek, Anal. Chem. 85 (2013) 1852-1859. Characterization of Triacylglycerol Enantiomers Using Chiral HPLC/APCI-MS and -8- 98/ 99/ 100/ 101/ 102/ 103/ 104/ 105/ 106/ 107/ 108/ 109/ 110/ Synthesis of Enantiomeric Triacylglycerols. I. Vokřál, V. Jedličková, R. Jirásko, L. Stuchlíková, H. Bártíková, L. Skálová, J. Lamka, M. Holčapek, B. Szotáková, Parasitology 140 (2013) 361-367. Metabolic fate of ivermectin in host (Ovis aries) and parasite (Haemonchus contortus). M. Nobilis, J. Mikušek, B. Szotáková, R. Jirásko, M. Holčapek, C. Chamseddin, T. Jira, R. Kučera, J. Kuneš, M. Pour, J. Pharm. Biomed. Anal. 80 (2013) 164 -172. Analytical power of LLE-HPLC-PDA-MS/MS in drug metabolism studies: Identification of new nabumetone metabolites. E. Cífková, M. Holčapek, M. Lísa, Lipids 48 (2013) 915-928. Nontargeted lipidomic characterization of various porcine organs tissues using hydrophilic liquid chromatography - electrospray ionization mass spectrometry. R. Jirásko, T. Mikysek, V. Chagovets, I. Vokřál, M. Holčapek, Anal. Bioanal. Chem. 405 (2013) 7181-7193. Structural Characterization of Electrochemically and In Vitro Biologically Generated Atorvastatin Oxidative Metabolites using UHPLC/MS/MS. M. Lísa, R. Denev, M. Holčapek, J. Sep. Sci. 36 (2013) 2888-2900. Retention Behavior of Isomeric Triacylglycerols in Silver-ion HPLC: Effects of Mobile Phase Composition and Separation Temperature. L. Česlová, M. Holčapek, M. Nobilis, J. Pharm. Biomed. Anal. 88 (2014) 221-224. Identification of combined conjugation of nabumetone phase I metabolites with glucuronic acid and glycine in minipig biotransformation using coupling high-performance liquid chromatography with electrospray ionization mass spectrometry. R. Jirásko, M. Holčapek, M. Kuneš, A. Svatoš, Anal. Bioanal. Chem. 406 (2014) 46014610. Distribution study of atorvastatin and its metabolites in rat tissues using combined information from UHPLC/MS and MALDI-Orbitrap-MS imaging. L. Stuchlíková, R. Jirásko, I. Vokřál, M. Valát, J. Lamka, B. Szotáková, M. Holčapek, L. Skálová, Drug Testing Anal. 6 (2014) 1055–1062. Metabolic Pathways of Anthelmintic Drug Monepantel in Sheep and in its Parasite (Haemonchus Contortus). E. Cífková, M. Holčapek, M. Lísa, D. Vrána, J. Gatěk, B. Melichar, Anal. Bioanal. Chem. 407 (2015) 991-1002. Determination of lipidomic differences between human breast cancer and surrounding normal tissues using HILIC-HPLC/ESI-MS and multivariate data analysis. M. Holčapek, E. Cífková, B. Červená, M. Lísa, J. Chromatogr. A 1377 (2015) 85-91. Determination of Nonpolar and Polar Lipid Classes in Human Plasma, Erythrocytes and Plasma Lipoprotein Fractions Using Ultrahigh-Performance Liquid Chromatography Mass Spectrometry. J. Galuszka, J. Vostálová, B. Červená, D. Galuszková, V. Šimánek, M. Holčapek, E. Cífková, M. Lísa, J. Vrbková, M. Bancířová, M. Táborský, D. Novotný, Eur. J. Lipid Sci. Technol. 117 (2015) 601–607. Selection of n 3 fatty acid supplementation candidates using fatty acid profiling. M. Holčapek, B. Červená, E. Cífková, M. Lísa, V. Chagovets, J. Vostálová, M. Bancířová, J. Galuszka, M. Hill, J. Chromatogr. B 990 (2015) 52–63. Lipidomic analysis of plasma, erythrocytes and lipoprotein fractions of cardiovascular disease patients using UHPLC/MS, MALDI-MS and multivariate data analysis. M. Holčapek, M. Ovčačíková, M. Lísa, E. Cífková, T. Hájek, Anal. Bioanal. Chem. 407 (2015) 5033-5043. Comprehensive two-dimensional liquid chromatography -9- 111/ 112/ 113/ 114/ electrospray ionization mass spectrometry of complex lipidomic samples. M. Lísa, M. Holčapek, Anal. Chem. 87 (2015) 7187–7195. New High-Throughput and Comprehensive Approach for Lipidomic Analysis Using Ultrahigh-Performance Supercritical Fluid Chromatography/Electrospray Ionization Mass Spectrometry. E. Cífková, M. Holčapek, M. Lísa, D. Vrána, B. Melichar, V. Študent, J. Chromatogr. B 1000 (2015) 14-21. Lipidomic differentiation of human kidney tumor and surrounding normal tissues using HILIC-HPLC/ESI-MS and multivariate data analysis. L. Stuchlíková, L. Lecová, R. Jirásko, J. Lamka, I. Vokřál, B. Szotáková, M. Holčapek, L. Skálová, Drug Testing Anal. (2015) in press. Comparison of biotransformation and efficacy of aminoacetonitrile anthelmintics in vitro. V. Chagovets, M. Lísa, M. Holčapek, Rapid Commun. Mass Spectrom. (2015) in press. Effects of fatty acyls chain lengths, double bond number and matrix on phosphatidylcholine responses in matrix-assisted laser desorption/ionization mass spectrometry. -10-