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Optics for next generation light sources Anton Barty Centre for Free Electron Laser Science Hamburg, Germany Tuesday, March 2, 2010 Key issues • Optical specifications • Metrology (mirror surfaces) • Metrology (wavefront, focal spot) • Coatings and damage • Novel optical structures Tuesday, March 2, 2010 Overview of the LCLS front-end optics Source Beamline Offset mirrors Endstation - ~30 µm Gaussian electron beam near undulator exit - Can easily incorporate a variety of source models - Apertures - Slits - etc. - Measured figure - Measured PSD - Known geometry - Intensity at endstation - Intensity at focus - Total wavefront error Tuesday, March 2, 2010 LCLS front end mirrors direct the beam into different end stations l Near experiment hall Front end enclosure LCLS X-ray beam M1S e - Soft X-ray offset mirrors (SOMS, 0.8 to 2 keV) Tuesday, March 2, 2010 M2S 0.8 - 2 keV 0.8 - 2 keV M3S2 M3S1 2 - 24 keV M1H M2H Hard X-ray offset mirrors (HOMS, 2 to 24 keV) Hutch 1 (AMO) Hutch 2 (SXR) Hutch 3 (XPP) Tunnel 2- Hu (X A wave optics formalism is must be used for coherent X-ray beams M1S M2S M3S/M4S Source Beamline + (Gaussian profile) Tuesday, March 2, 2010 Offset mirrors + (Apertures) + (Measured 1D figure) Endstation = (Statistical roughness) ???? (Intensity at focus) Complete mirror PSD is obtained from interferometry, surface microscopy and AFM data Interferometer Si test substrate by Vendor 1 Si test substrate by Vendor 2 ~ 0.16 µrad rms! ~ 0.3 µrad rms! ! = 0.19 nm rms! ! = 0.19 nm rms! ! = 0.16 nm rms! ! = 0.36 nm rms! Tuesday, March 2, 2010 Zygo 2x Zygo 20x AFM AFM 2.95 mm 0.37 mm 10 µm 2 µm Regina Soufli, LLNL [email protected] Tuesday, March 2, 2010 Interferometry measurements are used to create composite mirror surfaces Interferometer data Zygo Figure Model surface (Measured 1D figure) PSD Model surface AFM (Statistical roughness) Tuesday, March 2, 2010 Grazing incidence optics lead to a dilation of the mirror surface power spectrum Incident wavefront Reflected wavefront (x’, y’) W=2h sin(!) y’ = y x’=x sin(!) ! Mirror surface h(x,y) fy ymirror Mirror surface height (viewed normal to surface) Tuesday, March 2, 2010 Mirror surface PSD (isotropic distribution) fy ybeam fx xmirror z fx xbeam Wavefront error (mirror reflecting at angle !) Wavefront PSD (elliptical distribution) Coherent X-rays demand wavefront propagation to model the optical system At M1S At M2S At M3S Intensity Intensity Intensity (0.0139 radian from grazing) (0.0417 radian from grazing) (0.0417 radian from grazing) SOMS #4 Figure (phase) SOMS #4 Figure (phase) SOMS #4 Figure (phase) Source (Not to scale) (colour = phase) ~1cm Note: For testing purposes the same figure and PSD was used for all SOMS mirrors. This is trivial to change when we have new metrology data - the use of beamline scripting simplifies changes (although some format checking is still required). Tuesday, March 2, 2010 Mid spatial frequency range gives rise to additional beam structure At AMO endstation no MSFR At AMO endstation with measured MSFR ~5 mm at enstation Tuesday, March 2, 2010 Beam structure is affected by the mid spatial frequency components Figure only (no MSFR) Tuesday, March 2, 2010 With MSFR included We expect measurable intensity variation at the entrance to the AMO endstation 1.0 0.8 keV 0.8 0.6 0.4 0.2 0.0 0 100 200 300 400 500 600 1.0 2.0 keV 0.8 0.6 0.4 0.2 Without MSFR 0.0 0 With measured MSFR ~5 mm at endstation Tuesday, March 2, 2010 100 200 300 400 500 600 Specifications for SOMS mirrors Table 1. Surface specifications within the clear aperture (CA) of the SOMS mirror substrates. § Spatial frequency range -3 -1 CA to 10 µm MSFR HSFR 10 µm ! 0.5 µm -1 -1 0.5 µm ! 50 µm -3 Mirror # SN1 SN2 SN3 SN4 SN5 Tuesday, March 2, 2010 -1 -1 Spatial wavelength range CA to 1 mm 2 µm ! 1 mm 20 nm ! 2 µm Figure (nm RMS) 1.8 1.3 1.2 0.64 1.4 Specification <2 nm RMS and <0.25 µrad RMS < 0.25 nm RMS < 0.4 nm RMS Slope error (µrad RMS) 0.19 0.2 0.37 0.14 0.37 Fig. 3. Figure (left) measured at LLNL for the five SOMS mirror substrates available to be installed at LCLS. Measured PSD curve (right) for SOMS sn4 mirror, with the PSD in the HSFR range shown Tuesday, March 2, 2010 SOMS system (dashed line). Because metrology data are not yet available for the AMO focusing optics this calculation likely places an upper bound on the focusing spot properties given the predicted SOMS front-end performance. One point that is immediately apparent is that the focal spot is likely to vary in shape with energy due to the dependence of wavefront error and propagation properties on the photon energy, for different optical path errors and footprints on the mirrors across the SOMS energy range. Tuesday, March 2, 2010 Fig. 4. Calculated intensity distribution of the FEL beam at the last pop-in intensity monitor before the endstation in hutch 1 (at z=120 m from the undulator exit). Calculation takes into account the measured SOMS figure and roughness of all three SOMS mirrors in the beam path. Vertical banding is due to the Intensity at K-B focus is less severely degraded Tuesday, March 2, 2010 Fig. 5. Focal plane intensity structure in the plane of highest intensity, calculated based on the predicted SOMS front-end performance, figure 3. Solid lines represent the predicted intensity profile and dashed lines represent the case of perfect optics. Strehl ratios for the above two discussed in this manuscript. For these reasons, the measured results for surface figure and roughness on the HOMS Si substrates shown in Fig. 6 were used in the wavefront propagation calculations and are expected to be fairly representative of the wavefront results from the final, SiC-coated HOMS mirrors. For the purposes of this study we use the figure and finish data for HOMS substrates sn2 and sn3 respectively for the M1H and M2H optics. A total of 4 HOMS mirror substrates have been fabricated, with the intention to ultimately install 2 and use the remaining 2 as spares. Specifications for HOMS mirrors Mirror # SN1 SN2 SN3 SN4 Figure (nm RMS) 2.4 1.0 2.0 1.5 Slope error (µrad RMS) 0.27 0.27 0.22 0.23 Fig. 6. Figure error (left) measured at LLNL for the four HOMS mirror substrates, and measured PSD (Right) for HOMS #2 Si substrate. . Bottom: rms values for the figure of each HOMS substrate within the central 420 mm-length, derived after subtraction of the best-fit sphere. Tuesday, March 2, 2010 HOMS performance at CXI endstation Tuesday, March 2, 2010 Fig. 7. Calculated intensity distribution of the FEL beam at the last pop-in intensity monitor before the CXI endstation in hutch 5 (at z=383 m from the undulator exit). Intensity images at at 0.8 and 2.0 keV are shown on the top and horizontal intensity profiles through the maximum are plotted on the bottom Solid lines represent the predicted intensity profile and dashed lines Predicted focal spot of the CXI instrument Tuesday, March 2, 2010 Fig. 8. Calculated focal plane intensity distribution at the focus of the CXI endstation using the 1m focal length K-B optics. Solid lines are the predicted intensity profile and dashed lines represent the case of perfect optics. Strehl ratios for the above two calculations (actual peak The LCLS mirrors are coated with B4C J.Bozek, R.Soufli Tuesday, March 2, 2010 A compromise must be drawn between surface roughness and stress J.Bozek, R.Soufli Tuesday, March 2, 2010 Optical mounts must be precision engineered for ultra high stability ~300m to FEH 1 µrad => 0.3 mm 1 nrad => 0.3 µm Tuesday, March 2, 2010 Offset mirrors - Measured figure - Measured PSD - Known geometry J. Krzywinski Tuesday, March 2, 2010 Focal spot size is inferred from crater size and damage models J. Krzywinski Tuesday, March 2, 2010 and now for something completely different.... Tuesday, March 2, 2010 Sasa Bajt, PXRMS 2010 Tuesday, March 2, 2010 Pump-probe geometry with small windows allows us to measure only the delayed diffraction signal i) Drive the sample ii) Probe the sample some time later iii) Collect diffraction from probe Tuesday, March 2, 2010 We demonstrated that a tamper is effective in containing nanoparticle expansion Tampered Untampered Low fluence Tuesday, March 2, 2010 High fluence Aluminium dot Substrate (silicon nitride) Silicon tamper Aluminium dot Substrate (silicon nitride) Multilayer optics for two-colour pump-probe experiments Andy Aquila, PXRMS 2010 Tuesday, March 2, 2010 Multilayers for X-ray two-colour time delay experiments Andy Aquila, PXRMS 2010 Tuesday, March 2, 2010 Disposable zone plates for extreme focussing Anne Sakdinawat, LBNL Tuesday, March 2, 2010 Chirped multilayers for X-ray pulse compression Andy Aquila, PXRMS 2010 Tuesday, March 2, 2010 • Coherent beams demand wavefront propagation for optics analysis and optic specification • • Precision metrology is essential • Some optics are designed to be blown up! Anything in the beam will diffract (apertures, solid attenuators - everything!) • •Credits: • • Tuesday, March 2, 2010 LLNL X-ray optics group Sasa Bajt, Andy Aquila (CFEL) Jacek Kryzwinski (SLAC) Measured HOMS figure error is used to determine the optical surface profiles 10.00 8.00 Figure (nm) 6.00 4.00 2.00 HOMS #1 HOMS #2 0.00 HOMS #3 HOMS #4 -2.00 -4.00 -6.00 -8.00 -250.00 -200.00 -150.00 -100.00 -50.00 0.00 50.00 Position (mm) Tuesday, March 2, 2010 100.00 150.00 200.00 250.00 We expect overfilling of HOMS mirrors to degrade performance in the far experimental hall Intensity at 8.0 keV and z=383 m 1.5 1.5 1.0 1.0 Position (mm) Position (mm) Intensity at 2.0 keV and z=383 m 0.5 0.0 0.5 0.0 -0.5 -0.5 -1.0 -1.0 -1.5 -1.5 -1.0 -0.5 0.0 0.5 Position (mm) -1.5 -1.5 -1.0 -0.5 0.0 0.5 Position (mm) Tuesday, March 2, 2010 1.0 1.5 1.0 1.5 Tuesday, March 2, 2010 Tuesday, March 2, 2010 Tuesday, March 2, 2010