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Principles of Instrumental Analysis
5th Edition
Douglas A. Skoog - Stanford University
F. James Holler - University of Kentucky
Timothy A. Nieman - University of Illinois
Douglas A. Skoog and F. James Holler
Table of Contents
1. Introduction.
Section I: Measurement Basics.
2. Electrical Components and Circuits.
3. Operational Amplifiers in Chemical
Instrumentation.
4. Digital Electronics and Microcomputers.
5. Signals and Noise.
Web Resources
Introduction
Treatment of data
Section II: Atomic Spectroscopy.
Gravimetry
6. An Introduction to Spectrometric Methods. Aqueous solutions
7. Components of Optical Instruments.
Equilibrium calculations
8. An Introduction to Optical Atomic Spectrometry.
Titrimetry
9. Atomic Absorption and Atomic
Fluorescence Spectrometry.
Precipitate formation
10. Atomic Emission Spectrometry.
Complex-formation
11. Atomic Mass Spectrometry.
Acid/Base titrations
12. Atomic X-Ray Spectrometry.
Complex AB titrations
Section III: Molecular Spectroscopy.
Non-aqueous titrations
13. An Introduction to Ultraviolet/Visible
Molecular Absorption Spectrometry.
Kinetic methods
14. Applications of Ultraviolet/Visible Molecular
Electrochemistry
Absorption Spectrometry.
REDOX titrations
15. Molecular Luminescence Spectrometry.
16. An Introduction to Infrared Spectrometry. Potentiometry
17. Applications of Infrared Spectrometry.
Coulometry
18. Raman Spectroscopy.
Voltammetry
19. Nuclear Magnetic Resonance
Spectrophotometry
Spectroscopy.
20. Molecular Mass Spectrometry.
Molecular spectroscopy
21. Surface Characterization by Spectroscopy and
Spectroscopy equipment
Microscopy.
Atomic spectroscopy
Section IV: Electroanalytical Chemistry.
22. Introduction to Electroanalytical Chemistry.
Mass Spectroscopy
23. Potentiometry.
Solvent extraction
24. Coulometry.
25. Voltammetry.
Chromatography
Section V: Separation Methods.
Gas chromatography
26. An Introduction to Chromatographic
Liquid chromatography
Separations.
Hyphenated methods
27. Gas Chromatography.
28. High-Performance Liquid
Chromatography.
29. Supercritical Fluid Chromatography and
Extraction.
30. Capillary Electrophoresis and Capillary
Electrochromatography.
Section VI: Miscellaneous Methods.
31. Thermal Methods.
32. Radiochemical Methods.
33. Automated Methods of Analysis.
Appendix A: Evaluation of Analytical Data.
Appendix B: Activity Coefficients.
Appendix C: Some Standard and Formal Electrode
Potentials.
Appendix D: Compounds for Preparing Standard
Solutions of Some Common Elements.
Appendix E: Common Acronyms Encountered in
Chemical Instrumentation.
Appendix F: Answers to Selected Problems Index.