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Principles of Instrumental Analysis 5th Edition Douglas A. Skoog - Stanford University F. James Holler - University of Kentucky Timothy A. Nieman - University of Illinois Douglas A. Skoog and F. James Holler Table of Contents 1. Introduction. Section I: Measurement Basics. 2. Electrical Components and Circuits. 3. Operational Amplifiers in Chemical Instrumentation. 4. Digital Electronics and Microcomputers. 5. Signals and Noise. Web Resources Introduction Treatment of data Section II: Atomic Spectroscopy. Gravimetry 6. An Introduction to Spectrometric Methods. Aqueous solutions 7. Components of Optical Instruments. Equilibrium calculations 8. An Introduction to Optical Atomic Spectrometry. Titrimetry 9. Atomic Absorption and Atomic Fluorescence Spectrometry. Precipitate formation 10. Atomic Emission Spectrometry. Complex-formation 11. Atomic Mass Spectrometry. Acid/Base titrations 12. Atomic X-Ray Spectrometry. Complex AB titrations Section III: Molecular Spectroscopy. Non-aqueous titrations 13. An Introduction to Ultraviolet/Visible Molecular Absorption Spectrometry. Kinetic methods 14. Applications of Ultraviolet/Visible Molecular Electrochemistry Absorption Spectrometry. REDOX titrations 15. Molecular Luminescence Spectrometry. 16. An Introduction to Infrared Spectrometry. Potentiometry 17. Applications of Infrared Spectrometry. Coulometry 18. Raman Spectroscopy. Voltammetry 19. Nuclear Magnetic Resonance Spectrophotometry Spectroscopy. 20. Molecular Mass Spectrometry. Molecular spectroscopy 21. Surface Characterization by Spectroscopy and Spectroscopy equipment Microscopy. Atomic spectroscopy Section IV: Electroanalytical Chemistry. 22. Introduction to Electroanalytical Chemistry. Mass Spectroscopy 23. Potentiometry. Solvent extraction 24. Coulometry. 25. Voltammetry. Chromatography Section V: Separation Methods. Gas chromatography 26. An Introduction to Chromatographic Liquid chromatography Separations. Hyphenated methods 27. Gas Chromatography. 28. High-Performance Liquid Chromatography. 29. Supercritical Fluid Chromatography and Extraction. 30. Capillary Electrophoresis and Capillary Electrochromatography. Section VI: Miscellaneous Methods. 31. Thermal Methods. 32. Radiochemical Methods. 33. Automated Methods of Analysis. Appendix A: Evaluation of Analytical Data. Appendix B: Activity Coefficients. Appendix C: Some Standard and Formal Electrode Potentials. Appendix D: Compounds for Preparing Standard Solutions of Some Common Elements. Appendix E: Common Acronyms Encountered in Chemical Instrumentation. Appendix F: Answers to Selected Problems Index.