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CP620, Shock Compression of Condensed Matter - 2001 edited by M. D. Furnish, N. N. Thadhani, and Y. Horie © 2002 American Institute of Physics 0-7354-0068-7/02/$ 19.00 ON THE HEL AND THE "RAMPING" ABOVE HEL E. Bar-on1, Y. Partom1, M. B. Rubin2 and D. Z. Yankelevsky3 1 2 RafaelBallistics Center, P.O. Box 2250, Haifa 31021, Israel. Faculty of Mechanical Engineering, Technion-Israel Institute of Technology, Haifa 32000, Israel. 3 Faculty of Civil Engineering, Technion-Israel Institute of Technology, Haifa 32000, Israel. Abstract. Unlike in metals, stress and particle velocity histories of shock waves in ceramic materials show a typical "ramping" above the Hugoniot Elastic Limit (HEL). Under the assumption that the HEL signifies the beginning of failure of the material, this "ramping" has been described by viscoplasticity or by moduli degradation. However, there is ample experimental evidence to rule out plastic flow at the HEL level of stress, and it seems improbable that the moduli would degrade significantly during the compressive phase of a plate-impact. The proposed micro-mechanical mechanism for the HEL, and for the ramping beyond the HEL, is based on the process of porous compaction due to pressure above a threshold pressure pcri4sh - Although the pore volume of high-grade ceramics is quite small, it is sufficient to cause the ramping observed in Hugoniot measurements from the seventies. Additional evidence for the effect of porosity on the HEL stress has been given in recent years. The experimental evidence is supported by simulations, in which a simple model for porous compaction was used. These simulations suggest that porous compaction is the main micro-mechanical mechanism causing the "ramping" and other features related to the HEL. INTRODUCTION <a> The concept of the HEL (Hugoniot Elastic Limit) is used extensively in high velocity impact dynamics. For metals under impact the material undergoes a compression phase, which at first causes elastic deformations and at a specified value of stress causes inelastic deformations to evolve. This point on the Hugoniot curve is denoted as the HEL and for the case of metals it is related to the yield stress and to the onset of plastic deformations. The HEL in the compressive phase curve of metals is recognized by the sharp break of the stress-strain curve, which continues to increase to higher values of stress as a concave function (Fig. la). In brittle materials behavior, the concept of the HEL is not so clear. For brittle materials the transition from the elastic phase to the inelastic phase occurs gradually, and the compressive phase curve describes a convex function (Fig. Ib). 1 V V*» «J __ "*** """"* FIGURE 1. Typical compressive phase: (a) In metals; 739 (b) In ceramics Many researchers (e.g. works by Longy and Cagnoux [1], Beachump et al [2], Lankford [3], [4] and Lankford et al. [5]) suggest that micro-plasticity plays a major role as a limiting factor in the compressive failure of high strength ceramics. It is possible, that under high hydrostatic pressures due to confinement, or near crack tips due to highpressure singularity points, one can find dislocations, which are associated with plasticity. However, the difference in the behavior at the transition between the elastic phase and the inelastic phase in ceramics, as compared with metals, suggests that there is a different physical mechanism acting in ceramics. Specifically, in the present work, the HEL characterizes a transition phase between elastic phase and the phase of inelastic strains due to pore crushing. This conclusion is based on the following experimental observations. However, it is also consistent with the fact that the proposed model, which assumes pore collapse but no plasticity in the regular sense, produces results that are in good agreement with experimental data. about 300 kbar, the value obtained for u 2 from impedance matching was consistently greater than Ufs2/2. This is the opposite of results obtained for metals and is consistent with a model in which the porosity is permanently crushed out of the material by the shock compaction". ALUMINUM OXIDE (A1203) Co.-HOT Pness U,,/2 IMP. MATCH X W E S G O -995 OIAMONITC " U,,/2 P-3J42-1 . Q COOHS AD-85 . U,,/2 . l(-|> MATCH UM//2 IMP. MATCH V SINGLE CRYSTAL.MSauEEN and MAMSH EXPERIMENTAL PROOF FOR THE POROSITY EFFECT Hugoniot data for several ceramics were measured by Gust and Royce [6] who applied shock waves using explosives. The tested aluminas were distinguished according to their initial porosity, starting with 6.6% porosity AD-85 and ending with 0.2% porosity Lucalox. In Fig. 2, the measured steady-state Hugoniot stress and the best-fit curves for four of these ceramics (from [6]) are plotted. Studying this figure, one can conclude that as the value of porosity decreases (going from right to the left in the graph) - (1) the HEL value increases, and (2) the HEL cusp becomes indistinguishable and the curve converges to the Hugoniot of a single crystal A12O3 (sapphire). Another conclusion from these results is that the measured Hugoniots do not follow one curve in the stress-volume plane (like in a p-a model), but there is a family of curves, where each curve is associated with the initial porosity of a specific ceramic. When they analyzed their data, Gust and Royce noted that (in [6], bottom of page 289) - "For the more porous materials,...it was noted that in the compaction regime, i.e., from the yield point to 020 O.Z1 0.2Z O.M O.t* 0.23 0.2« O.JT O.2« 0.» FIGURE 2: Experimental Hugoniots for A12 O3 ceramics [6] 20 o * AD-85 [1] B4C[7] £ 015 .ts: 5 10 15 20 Porosity <|> (%) FIGURE 3: The effect of porosity on the HEL stress magnitude of AD-85 alumina [1] and Boron Carbide [7] 740 O.SO The effect of porosity on the magnitude of the HEL stress was studied over the years by different researchers. Rosenberg reported the effect of porosity on the HEL stress in Boron Carbide (B 4 C) ceramics [7], and Longy and Cagnoux showed similar behavior in AD-85 alumina [1]. Both works have shown that increasing porosity decreases the magnitude of the HEL stress (Fig. 3). Figure 7 demonstrates the good agreement, which can be achieved in simulating the stress curve in a plate-impact experiment [8], using this model. 2.5 POROSITY IN THE MODEL In many constitutive models, a Representative Volume Element dv of brittle material in the present configuration (at time / ) is decomposed into a solid part whose volume is dvs and a pore volume dv p , such that dv = dvs + dvp, 0.5 1.2 1.4 TIME (jiSec.) dV = d\ FIGURE 4: The effect of varying pcnish in Eq. (4) where dV,dVs,dVp are the values of dv,dvs,dvp in a fixed reference configuration, and the indexes s, p denote the solid and pores, respectively. The porosity <j> and its reference value O are then defined by 1 P J- crush ! —— Pcrush=2-8GPa t4 V p (k = —-, O = —dv dV __ - 2.5r v (2a,b) 7 In the compressive phase, the porosity </> is determined through integration of the following evolution equations: Uto- 1.2 1.4 TIME (uSec.) for p > pcrush far pcrush > p (3a,b) FIGURE 5: The effect of varying C} in Eq. (4) 2.5r Here pcrush is a threshold pressure to begin pore collapse in compaction, v is the current element volume and /3 (p) is given by -P™^ Pcrush ) V Pcrush (4) ) Pcrush9 ^i 9 Q are material parameters to be determined, and are unique for each ceramic. Here they are taken to be constants. However, they are probably functions of the initial porosity and/or other variables. Figs. 4, 5 and 6 show the way that the calculated stress curve is affected according to the varied values of these material parameters. FIGURE 6: The effect of varying C2 in Eq. (4) 741 1.8 100 2.5 AD995-model Dandekar and Bartkowsky Grady and Moody AD85-model Gust and Royce 80 60 -.1.5 f Q_ o CD 40 20 0.5 1.2 1.4 TIME (>iSec.) 1.6 0.22 1.8 0.24 0.26 Volume (Cm3/gm.) 0.28 0.3 FIGURE 8: Experimental data and model simulations, proofs of the porosity effect on the HEL value and the "ramping" in the Hugoniots of two ceramics FIGURE 7: Comparison of the measured compressive phase in a plate-impact experiment [8] with the model calculation DISCUSSION This work shows that porous compaction is the main mechanism active during the compressive phase of shock loading of ceramics. This conclusion has been based on the analysis of experimental data that has been collected over the last 30 years. The proposed model of porous compaction correctly predicted the ramping observed in the compression wave, without causing precursor decay or wave separation, as observed in pseudo-plasticity models. It is important to emphasize that here attention has been focused on the compression phase, and the unloading or tension phases have been omitted. Consequently, it has been possible to consider only a simple model for porous compaction, without the necessity to go into detail of a model to simulate the response of brittle materials to impact loads (compressive and tensile phases). For general material response it is necessary to consider a much more complicated phenomena associated with micro-cracking, and possibly a pseudo "plasticflow" (related to the amount of crushed pores). [2] Beachump E. K., Carr M. J. and Graham R. A., "Plastic Deformation in Alumina by Explosive Shock Loading". J. of Am. Ceramics Soc., Vol. 68, No. 12. PP. 696-699. (1985). [3] Lankford J., "Compressive Strength and Microplasticity in Polycrystalline Alumina". J. of Materials Science, Vol. 12. PP. 791-796. (1990). [4] Lankford J., "High Strain Rate Compression and Plastic Flow of Ceramics". J. of Materials Science, Vol. 15. PP. 745-750. (1996). [5] Lankford J., Predebon W. W., Staehler J. M., Subhash, Pletka B. J. and Anderson C. E., "The Role of Plasticity as a Limiting Factor in the Compressive Failure of High Strength Ceramics". Mechanics of Materials, Vol. 29. PP. 205-218. (1998). [6] Gust W.H., and Royce E.B., "Dynamic Yield Strength of B4 C, Be O and A12 03 Ceramics". J. of Appl. Phys., Vol. 42, No. 1, PP. 276-295. (January 1971). [7] Rosenberg Z., "The Response of Ceramic Materials to Shock Loading". Proceedings of the APS Shock Waves in Condensed Matter Conference, PP. 439446. Williamsburg, VA. (1991). [8] Rajendran A. M. and Grove D. J., "Modeling the Impact Behavior of AD-85 Ceramic". 24th Int. SAMPE Technical Conf. T925-T934. (1992). REFERENCES [1] Longy F., Cagnoux J., "Plasticity and Microcracking in Shock-Loaded Alumina". J. Am. Ceram. Soc., Vol. 72(6), PP. 971-979. (1989). 742