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Test report no. 12-2011 Marit Kjeldsberg, Kjersti Eilertsen and Kirsi Laitala Shrinkage, pilling, stain removal and soil repellence on wool and other fabrics © SIFO 2011 Test report no. 12 – 2011 NATIONAL INSTITUTE FOR CONSUMER RESEARCH Sandakerveien 24 C, Building B P.O. Box 4682 Nydalen N-0405 Oslo www.sifo.no Due to copyright restrictions, this report is not to be copied from or distributed for any purpose without a special agreement with SIFO. Reports made available on the www.sifo.no site are for personal use only. Copyright infringement will lead to a claim for compensation. Test report no. 12-2011 1. PURPOSE In this study we want to investigate the possibilities to fill the washing machine to full capacity and wash woolen products with other fabrics, using wool program and detergent. We will focus on properties such as shrinkage, pilling, stain removal and soil repellence. 2. EQUIPMENT AND TEST MATERIALS Washing machines: Three identical domestic washing machines (Miele W307). The trials were run randomly. Wash program: Wool program at 30 C. Spin speed 1200 rpm Water quality: Tap water approx. 3.0 – 3.5 dH according to Oslo Water and Sewerage Works, temperature 15 2 C. Washing detergent/ Dosage: Wool detergent Milo: 50 ml Test materials: For a full overview se annex 1 and 2. 100% wool, 100 % merino wool, polyester, cotton, silk, acrylic, polyamide, mixture of wool/cotton, wool/acrylic, wool/silk, wool/polyester and wool/polyamide Base load: Polyester textile base load; according to standard ISO 6330:2000 and wool textile base load The results are valid for the tested material only Contract No. 11-2010-11/09/129 2(50) Test report no. 12-2011 Soil: Type of soil Red wine Coffee Olive oil Cocoa Tomato sauce Smoothie, banana and mango From Canepa. Cabernet sauvignon From coffee machine, medium strength Ybarra, cold pressed, extra virgin From coffee machine, medium strength Landlord tomatoes without skin Småfolk Comments Diluted 1:1 with water Diluted 1:1 with water 3. METHODS Two tests have been designed in order to investigate possibilities for reducing environmental effects from textile maintenance. First test focuses on whether wool products can be washed with other fabrics without affecting shrinkage and pilling and the second compares wool with other fibres and fibre mixes for stain removal and soil repellence . 3.1 Dimensional change and pilling Laboratory tests were designed in order to study whether woolen products can be washed with other textile materials without increasing pilling and shrinkage. All textiles were exposed to standard atmosphere 20° C, 65 % RH for 24 hours. Three samples from each textile were cut, labeled with specimen number A and B and one reference. The specimens were marked according to template for dimensional change 500mm x 500mm or 250mm x 200mm depending on available sample size. The edges were parallel to the length and width of the fabric. Edges were overlocked to avoid unravels during the test. The length and width dimensions were determined before washing, after one wash and flat drying and after five washing cycles and flat drying at the end. Four woven and two knitted pure wool samples were washed either together with wool or with textiles made of other materials in the same laundry load. Wool samples labeled A were laundered separately from other fiber types ref. table 1.Textiles of mixed fibers were laundered together with wool samples labeled B table 2. Polyester samples, were both washed separately and with the mixed textiles ref table 3. The mixed textiles were line dried. All wool- and polyester- samples were evaluated, in a viewing cabinet illuminated by a white fluorescent tube D 65 daylight, for pilling and fuzzing according to ASTM D 3512 photographic standard after 1st and 5th wash. In addition, woolen specimens’ dimensional changes were measured according to ISO 5077. The results are valid for the tested material only Contract No. 11-2010-11/09/129 3(50) Test report no. 12-2011 3.2 Stain removal In order to study wool’s stain removal properties, and to compare wool with other textile materials, 19 different types of textiles were soiled, washed and evaluated. The soil selected was; Red wine, coffee, olive oil, hot chocolate, tomato sauce and banana and mango smoothie. This selection was made because soil containing protein, fats and color dyes are known to make problematic stains that are difficult to remove in laundering. The chosen products are known among Norwegian consumers and available in grocery stores. Further there was a desire for soil that was easy to apply by using a micropipette. All textiles were white or very light in colour and washed five times before the test in order to remove nondurable finishes. The same specimens used for dimensional change and pilling were used in this test. Figure1. The left panel shows soil used in the test and the right panel shows stain applying Soiling was conducted at 23°C and 55 % RH. The soil was at room temperature 23°C when applied on the textiles. The test specimens were placed on a smooth horizontal surface with the face-side up. Small drops of soil, 200 µl were placed carefully on the fabric surface using a micropipette and a plastic laminated template. See figure 1. The results are valid for the tested material only Contract No. 11-2010-11/09/129 4(50) Test report no. 12-2011 In most cases penetration or wetting and wicking occurred. Some test specimens showed resistance to wetting indicated by a clear, well-rounded drop with high contact angle. This is characteristic of a fabric whereby it resists absorption of soil. In this test the aim was to compare wool with other fibres and fibre mixes due to stain removal. To help the stain to stick to the fabric, the droplet was carefully stirred with a needle in order to disturb the surface tension for letting the wetting and wicking occur. This was the case of some wool and woollen mixture samples, besides for olive oil that was readily absorbed by all fabric types. The test specimens were line dried overnight and then laundered all together and line dried. Ref figure 2. Figure2. The left panel shows line drying after staining and the right panel shows line drying after laundering After the first and fifth washing cycle with wool program and detergent, four observers rated the test specimens independently. Evaluation was performed in a darkened room in a viewing cabinet illuminated by white fluorescent tube D 65 daylight. The rating took place according to the following scale: 1. 2. 3. 4. 5. Very visible stain Visible stain Slightly visible stain Hint of stain No visible stain. The results are valid for the tested material only Contract No. 11-2010-11/09/129 5(50) Test report no. 12-2011 3.3 Soil repellence Soil repellence was studied in order to see whether is it possible to get rid of the soiling before it causes permanent staining. Resistance to wetting and thereby soiling is indicated by a clear, well-rounded drop with high contact angle, figure 3. This kind of liquid droplets may touch lightly on the surface and easily roll off before being absorbed into the fabric. This allows time for liquid spills to be wiped from fabric before they can cause permanent staining. To investigate this phenomenon, three types of liquid soiling, red wine, coffee and hot chocolate, that had showed some resistance to wetting in the stain removal test were selected. 22 specimens, included different types of wool, synthetics, silk and fiber mixtures, that were washed 10 times before the test were soiled. Soiling was conducted at 23°C and 55 % RH the soil was at room temperature 23°C when applied on the textiles. The test specimens were placed on a smooth horizontal surface with the face-side up. Small drops of soil, 200 µl, were placed carefully on the fabric surface using a micropipette. After about 5 seconds, paper towels were used to wipe and soak up as much of spilled liquids as possible. Two observers rated the specimens independently according to the procedure described in the stain removal test. Figure3. Left panel shows red wine droplets on knitted wool and right panel shows coffee droplets on woven wool The results are valid for the tested material only Contract No. 11-2010-11/09/129 6(50) Test report no. 12-2011 Table 1: Washing conditions Washing Miele Novotronic W 307 machines Washing Wool wash 30°C , tap water, inlet temperature 15± 2 °C procedure Detergent Milo wool wash detergent 50 ml Wool Wool specimens Polyester After soiling. specimens A B washed with specimens All samples in washed with other textiles washed with one washing wool ballast and polyester polyester ballast with polyester ballast ballast Number of washes Ballast type and amount. Total weight 5 5 Wool textile Polyester textile base load. base load. 1.984 kg 1.956 kg After soiling. All samples A in one washing with polyester ballast three cycles with detergent and the last without 4 5 1 Polyester textile base load. 1.997 Polyester textile Polyester textile base load. base load. 2.025 kg 2.012 kg 1.264 kg Sample 0.332g weight. (Total weight of all samples) 0.354 0.029 kg Number of 6 test specimens 01A, 10A, Specimens no. 18A, 19A, 20A, 22A 36 01B, 10B, 18B, 19B, 20B, 22B, 02, 03, 04, 05, 06, 08, 09, 10, 11, 12, 13, 14, 15, 17, 21 Wool textiles were flat dried. Other textiles mixes were line dried 2 43 09 specimen C and All samples 15 specimen C except sample 15 22 All samples labeled A, inclusive 23,24 and 25,except sample 15 Line dried Line dried. Sample 23,24 and 25 flat dried Drying Flat dried procedure. (After one wash and after five washes) The results are valid for the tested material only Contract No. 11-2010-11/09/129 Line dried 0.548 kg 7(50) Test report no. 12-2011 4. RESULTS 4.1 Results pilling and fuzzing Results for wool specimens after washing them either with wool or with other textiles presented in table 2 and results for polyester specimens presented in table 3. Pilling were assessed on a scale from 1-5 5 no pilling 4 slight pilling 3 moderate pilling 2 severe pilling 1 very severe pilling Table 2: Pilling results for wool specimens after washing them either with wool or with other textiles. Results after 1st and 5th washing cycle are given in pilling grade as a mean value. No Fibre content 01 Wool merino 10 wool 18 wool 19 wool 20 wool merino 22 wool 1st wash 5th wash Washed Washed Washed Structure Washed Comments with with with with other other wool wool materials materials 5 5 5 5 Slightly woven surface fuzzing 5 5 5 5 Slightly woven uneven appearance 5 5 5 5 Uneven woven structure, more felted 5 5 5 5 Uneven woven structure, more felted 5 5 5 5 Some surface knitted fuzzing, wrinkled 5 5 5 5 Some surface knitted fuzzing The results are valid for the tested material only Contract No. 11-2010-11/09/129 8(50) Test report no. 12-2011 Table 3: Pilling results for polyester specimens, after washing them either with polyester or with other textiles. Results after 1st and 5th washing cycle are given in pilling grade as a mean value. 1st wash 5th wash No Fiber content Structure 09 polyester 15 polyester woven Washed with polyester 5 Washed with other materials 5 Washed with polyester 5 knitted 5 5 5 Comments Washed with other materials 5 The fabric was uneven before wash 5 Hint of surface fuzzing 4.2 Results dimensional change Results for dimensional change in percent after 1st and 5th washing cycle are presented in Table 4 to 6 Table 4: Dimensional change results for wool specimens after washing them either with wool or with other textiles Results after 1st and 5th washing cycle are given as an average of length and width dimensions. Negative result indicates shrinking. 1st wash [%] 5th wash [%] Washed Washed Washed No Fibre content Structure Washed with with other with other with wool wool materials materials woven -2.3 -2.3 -2.9 -2.8 01 wool merino wool woven -1.8 -1.1 -2.8 -2.7 10 woven -2.8 -3.6 -5.8 -6.5 18 wool woven -3.2 -4.2 -7.1 -8.6 19 wool knitted -1.7 -2.8 -2.3 -2.6 20 wool merino knitted -2.1 -2.8 -2.4 -3.8 22 wool -2.3 -2.8 -3.9 -4.5 Average all -2.5 -2.8 -4.6 -5.1 Average woven -1.9 -2.8 -2.4 -3.2 Average knitted -2.0 -2.5 -2.6 -2.7 Average merino -2.5 -2.9 -4.5 -5.4 Average wool The results are valid for the tested material only Contract No. 11-2010-11/09/129 9(50) Test report no. 12-2011 Table 5: Dimensional change results for wool specimens after washing them either with wool or with other textiles. Mean value after one wash. Negative result indicates shrinking. Mean value after 1 wash No Fiber Structure Length (%) Width (%) content Washed Washed Washed Washed with wool with other with wool with other materials materials -2.2 -1.9 -2.5 -2.7 01 wool merino woven woven -1.5 -1.0 -2.0 -1.2 10 wool woven -6.5 -6.8 0.8 -0.5 18 wool woven -7.8 -8.8 1.3 0.4 19 wool -5.7 -5.5 2.3 -0.1 20 wool merino knitted knitted -3.2 -3.2 -1.1 -2.5 22 wool -4.5 -4.5 -0.2 -1.1 Average all -4.5 -4.6 -0.6 -1.0 Average woven -4.4 -4.3 0.6 -1.3 Average knitted -3.9 -3.7 -0.1 -1.4 Average merino -4.7 -4.9 -0.2 -1.0 Average wool Table 6: Dimensional change results for wool specimens after washing them either with wool or with other textiles. Mean value after five washes. Negative result indicates shrinking. Mean value after 5 washes Fiber content Structure No Length (%) Width (%) A B A B Wool with Wool with Wool with Wool with wool other wool other woven -2.7 -2.1 -3.0 -3.5 01 wool merino wool woven -3.4 -2.9 -2.1 -2.4 10 woven -9.9 -10.2 -1.6 -2.8 18 wool woven -12.8 -14.3 -1.3 -2.8 19 wool knitted -6.2 -5.1 1.6 0.0 20 wool merino knitted -4.5 -4.7 -0.4 -2.9 22 wool -6.6 -6.6 -1.1 -2.4 Average all -7.2 -7.4 -2.0 -2.9 Average woven -5.3 -4.9 0.6 -1.5 Average knitted -4.4 -3.6 -0.7 -1.8 Average merino -7.7 -8.0 -1.4 -2.7 Average wool The results are valid for the tested material only Contract No. 11-2010-11/09/129 10(50) Test report no. 12-2011 Table nr 7: Difference in shrinkage when washed with other materials (B minus A). 01 10 18 19 20 22 wool merino wool wool wool wool merino wool Structure woven woven woven woven knitted knitted Dimensional change (%) Sample 01. 100% merino wool. -4,0 -2,5 -2,0 A B -3,0 -3,5 -2,0 0,0 Length A B Dimensional change (%) Sample 10 . 100% wool. -4,0 -8,0 -1,5 -3,0 0,0 B Length -3,0 -2,0 -2,5 -2,0 0,0 A B A B Width Figure5 Sample 10. Dimensional change Sample 19. 100% wool. -10,0 -10,0 -4,0 -3,5 Length Sample 18. 100% wool. A 5th wash Length Width 0.6 -0.5 0.5 -0.3 -0.3 -1.2 -1.5 -1.5 1.0 -1.6 -0.2 -2.5 Width Figure4 Sample 01. Dimensional change -12,0 Dimensional change (%) Fiber content A B Width Figure 6 Sample 18. Dimensional change The results are valid for the tested material only Contract No. 11-2010-11/09/129 Dimensional change (%) No 1st wash Length Width 0.3 -0.2 0.6 0.8 -0.3 -1.3 -1.0 -0.9 0.2 -2.4 0.0 -1.5 -16,0 -12,0 -8,0 -4,0 0,0 -13,0 -14,5 A B Length -1,5 -3,0 A B Width Figure 7 Sample 19. Dimensional change 11(50) Sample 20. 100% merino wool -8,0 -4,0 0,0 4,0 -6,0 -5,5 0,0 A B Length 1,5 A B Width Figure 8 Sample 20. Dimensional change The results are valid for the tested material only Contract No. 11-2010-11/09/129 Dimensional change (%) Dimensional change (%) Test report no. 12-2011 Sample 22. 100% wool -6,0 -4,0 -2,0 0,0 -4,5 -4,5 -3,0 -0,5 A B Length A B Width Figure9 Sample 22. Dimensional change 12(50) Test report no. 12-2011 4.3 Results stain removal and soil repellence Average soil repellence and stain removal results for all specimens and soil types are given in Table 8 to table 15. Grade 5 is the best result with no visible stain and grade 1 lowest with very visible stain. Stain assessed on a scale from 1-5 1 very visible stain 2 highly visible stain 3 slightly visible stain 4 hint of stain 5 no visible stain. Table 8: Results of stain removal after one wash. Mean value specimens of 100 % wool. No. 01 10 18 19 20 22 Fiber contet wool merino wool wool wool wool merino wool Structure woven woven woven woven knitted knitted Red wine 3.4 2.7 2.9 2.3 1.0 1.0 Coffee 3.4 3.3 2.4 2.4 2.1 2.0 Olive oil 5.0 5.0 5.0 4.8 4.3 4.0 Hot chocolate 2.6 3.9 5.0 4.8 1.8 1.8 Tomato sauce 3.7 3.9 2.6 3.4 1.9 2.1 Banana and mango 3.7 3.5 3.5 4.0 1.6 3.4 Table 9: Results of stain removal after five washing cycles. Mean value specimens of 100 % wool. Banana No. Fiber contet Structure Red Coffee Olive Hot Tomato and wine oil chocolate sauce mango 4.1 4.0 5.0 4.5 4.3 2.8 01 wool merino woven woven 3.9 3.5 4.8 4.8 5.0 5.0 10 wool woven 2.8 2.6 5.0 5.0 5.0 2.9 18 wool woven 2.5 2.5 5.0 4.9 5.0 5.0 19 wool 1.1 2.1 4.8 2.2 3.5 2.8 20 wool merino knitted knitted 1.1 2.5 4.9 2.2 4.3 4.8 22 wool The results are valid for the tested material only Contract No. 11-2010-11/09/129 13(50) Test report no. 12-2011 Table 10: Results of stain removal by wiping off after 10 washing cycles. Mean value specimens of 100 % wool. No. Fiber contet Structure 01 10 18 19 20 22 23 24 25 wool merino wool wool wool wool merino wool wool wool wool woven woven woven woven knitted knitted knitted knitted knitted Red wine 1.0 1.0 2.5 2.8 1.0 1.0 4.0 4.0 4.0 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Coffee 2.5 2.5 4.5 4.0 1.0 1.0 4.5 5.0 5.0 Hot chocolate 1.0 1.0 1.0 2.5 1.0 1.0 4.0 4.0 4.0 14(50) Test report no. 12-2011 Table 11: Summery of stain removal after one wash. Mean value for specimens of wool mixes and other fibers No Fiber content 02 03 04 05 06 08 09 11 12 13 14 17 21 cotton silk 88 % wool, 10 % polyamide, 2 % lycra cotton polyamide acryl polyester acrylic 80 % merino wool, 20 % polyamide 80 % wool, 20 % silk 65 % acrylic, 30 % wool, 5 % angora 45 % wool, 45 % cotton, 10 % polyamide 70 % merino wool, 28 % polyamide, 2 % lycra The results are valid for the tested material only Contract No. 11-2010-11/09/129 Structure woven woven woven knitted woven woven woven knitted knitted knitted knitted knitted knitted Red wine Coffee Olive oil Hot chocolate Tomato sauce Banana and mango 1.8 1.0 3.5 1.1 3.9 3.8 4.3 3.5 1.1 1.8 2.5 1.8 1.8 2.8 1.9 4.4 2.3 4.3 5.0 4.9 5.0 1.9 2.1 3.1 1.9 2.8 5.0 3.4 4.9 4.7 5.0 5.0 5.0 5.0 5.0 4.2 4.8 4.9 5.0 1.4 1.5 3.4 1.6 3.5 3.6 2.8 4.1 2.4 2.1 5.0 2.2 2.1 3.0 4.2 2.7 1.7 4.2 5.0 2.9 3.4 2.1 2.2 3.8 2.9 3.0 3.7 5.0 2.6 2.4 3.3 3.3 3.0 3.3 3.3 2.9 3.6 3.1 2.6 15(50) Test report no. 12-2011 Table 12: Summary of stain removal after five washing cycles. Mean value for specimens of wool mixes and other fibers No 02 03 04 05 06 08 09 11 12 13 14 17 21 Fiber content cotton silk 88 % wool, 10 % polyamide, 2 % lycra cotton polyamide acryl polyester acrylic 80 % merino wool, 20 % polyamide 80 % wool, 20 % silk 65 % acrylic, 30 % wool, 5 % angora 45 % wool, 45 % cotton, 10 % polyamide 70 % merino wool, 28 % polyamide, 2 % lycra The results are valid for the tested material only Contract No. 11-2010-11/09/129 Structure woven woven woven knitted woven woven woven knitted knitted knitted knitted knitted knitted Red wine Coffee Olive oil Hot chocolate Tomato sauce Banana and mango 2.1 1.6 4.0 1.4 2.8 3.1 4.0 3.7 1.1 2.0 2.9 1.5 1.4 2.9 2.0 4.5 2.1 4.5 4.7 5.0 5.0 1.9 2.1 3.0 1.9 2.6 5.0 4.5 4.8 4.8 5.0 5.0 5.0 5.0 5.0 4.2 4.8 4.8 5.0 1.0 2.0 5.0 2.3 4.7 4.4 3.0 5.0 2.0 2.4 4.7 2.1 2.4 4.8 4.8 5.0 3.3 5.0 5.0 4.3 5.0 3.8 3.8 4.8 4.4 4.5 4.7 4.8 5.0 2.9 2.5 4.0 2.1 4.6 4.5 4.2 4.6 3.6 4.4 16(50) Test report no. 12-2011 Table 13: Summary of stain removal by wiping off after 10 washing cycles. Mean value for specimens of wool mixes and other fibers No 02 03 04 05 06 08 09 11 12 13 14 17 21 Fiber content cotton silk 88 % wool, 10 % polyamide, 2 % lycra cotton polyamide acryl polyester acrylic 80 % merino wool, 20 % polyamide 80 % wool, 20 % silk 65 % acrylic, 30 % wool, 5 % angora 45 % wool, 45 % cotton, 10 % polyamide 70 % merino wool, 28 % polyamide, 2 % lycra The results are valid for the tested material only Contract No. 11-2010-11/09/129 Structure woven woven woven knitted woven woven woven knitted knitted knitted knitted knitted knitted Red wine Coffee Hot chocolate 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.8 1.0 1.0 1.0 2.0 1.0 2.0 2.0 2.0 1.0 1.0 1.0 1.0 3.8 1.0 1.0 1.0 1.5 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.8 1.0 17(50) Test report no. 12-2011 Table 14: Average soil repellence and stain removal results for each specimen. *Specimens 23-25 only tested for soil repellence due to lack of material. Woven Woven Woven Woven Knitted Knitted Knitted Knitted Knitted Woven Knitted Woven Knitted Woven Woven Woven Woven Knitted Knitted Knitted Repellence wiping 1.5 1.5 2.7 3.1 1.0 1.0 4.2 4.3 4.3 1.0 1.0 1.3 1.0 1.3 1.3 1.0 1.8 1.0 1.0 1.0 Stain removal 1st wash 3.6 3.7 3.6 3.6 2.1 2.4 2.9 2.3 4.3 4.0 4.0 3.8 2.8 3.6 2.6 2.5 3.8 Stain removal 5th wash 4.1 4.5 3.9 4.2 2.7 3.3 3.4 2.8 4.4 4.7 4.1 3.9 3.3 4.7 3.0 3.1 4.1 Knitted 1.0 2.9 3.4 Knitted 2.8 2.8 3.0 No Fibre content Structure 01 10 18 19 20 22 23* 24* 25* 02 05 08 11 06 09 03 04 12 13 14 100% wool (merino) 100% wool 100% wool 100% wool 100% wool (merino) 100% wool 100% wool 100% wool 100% wool 100% cotton 100% cotton 100% acrylic 100% acrylic 100% polyamide 100% polyester 100% silk 88% wool, 10% polyamide, 2% lycra 80% merino wool, 20% polyamide 80% wool, 20% silk 65% acrylic, 30% wool, 5% angora 70% merino wool, 28% polyamide, 2% lycra 45% wool, 45% cotton, 10% polyamide 21 17 The results are valid for the tested material only Contract No. 11-2010-11/09/129 18(50) Test report no. 12-2011 Table 15: Average soil repellence and stain removal results divided by stain types and fibre groups. Soil type Cleaning Wool Woolmix Synthetic Cotton Red wine Coffee Olive oil Hot chocolate Tomato sauce Banana and mango Mean Wiping 1 wash 5 wash Wiping 1 wash 5 wash 1 wash 5 wash Wiping 1 wash 5 wash 1 wash 5 wash 1 wash 5 wash Wiping 1 wash 5 wash The results are valid for the tested material only Contract No. 11-2010-11/09/129 2.4 2.2 2.6 3.3 2.6 2.9 4.7 4.9 2.4 3.3 3.9 2.9 4.5 3.3 3.9 2.6 3.2 3.8 1.3 2.1 2.1 1.6 2.7 2.7 4.8 4.7 1.4 2.9 3.1 2.8 4.4 3.0 4.4 1.4 3.0 3.6 1.0 3.9 3.4 1.8 4.8 4.8 5.0 5.0 1.0 3.5 4.3 3.9 4.8 3.2 3.3 1.3 4.0 4.3 1.0 1.4 1.8 1.0 2.5 2.5 4.8 4.9 1.0 1.5 1.6 2.3 4.0 3.0 3.8 1.0 2.6 3.1 19(50) Silk Knitted Woven 1.0 1.0 1.6 1.0 1.9 2.0 3.4 4.5 1.0 1.5 2.0 4.2 4.8 5.0 4.8 1.0 2.8 3.3 1.8 1.7 1.8 2.2 2.6 2.6 4.7 4.8 1.9 2.6 2.8 2.5 4.1 2.9 4.0 2.0 2.8 3.4 1.4 3.0 3.1 2.4 3.5 3.6 4.8 4.9 1.4 3.3 3.9 3.6 4.8 3.5 3.9 1.7 3.6 4.0 Test report no. 12-2011 5. CONCLUSIONS 5.1 Pilling and fuzzing The results of pilling and fuzzing after five washes were the same for all 6 wool specimens and 2 polyester specimens: no pilling (grade 5). This was valid independent of whether the materials were washed together with similar fibers or with other materials. This result would probably have been different with materials that were more sensitive to pilling. Some fuzzing was observed, but no significant differences could be found between the two different ways of washing. Our current research did not show any additional significant danger of pilling or shrinkage during the first 5 washes. However, more research in these themes is needed with more varying materials and higher number of washing cycles in order to draw final conclusions. 5.2 Dimensional change The high shrinkage results of specimens 18 and 19 indicate that these materials are not very suitable for machine wash. When the specimens washed with wool and specimens washed with other materials are compared, we can see that on some materials there is no difference, whereas on others there are small variations in both ways. If an average value for all specimens is calculated, it indicates that there is 0.5% higher average shrinkage on specimens that are washed together with other materials. However, this is within the 95% confidence limits of the method and therefore not significant. 5.3 Stain removal and soil repellence The soil repellence results vary greatly between 1 and 4, even within the same fiber type (wool). Best repellence results are given by pure wool samples 23-25 made of crossbred wool, followed by 18 and 19, also wool. Worst repellence results can be found among all the fiber types included in the test, including cotton, synthetics, wool, silk and blends. When it comes to stain removal results, there was usually less than one grade difference between the evaluation after the first and fifth wash. Wool had best soil resistance against red wine and coffee, but if it gets soiled the stain remains visible (Table 6). Synthetic materials in test did not have good resistance against any of the soils used, but they were easier to get clean than other materials. Olive oil stains were generally not very visible, and was usually graded between 4 and 5. The exception was silk, which was graded to 3 after 1st wash, but also got better after 5 washes. Hot chocolate stains got lighter in wash on wool and synthetics, but remained quite visible on cotton and silk. However, cotton could be washed more efficiently and the result would most likely have been different after more suitable washing program and detergent. Tomato sauce stains remained partly at the surface of the fabric and were quite visible after the first wash, but significantly improved on all materials after 5 washes. Also the structure of material was of importance. Woven fabrics had in general higher stain removal results than knitted fabrics. This may be explained by the denser structure that did not allow the soils enter in to a same degree as on knitted fabrics. However, soil repellence properties are easily affected by surface treatments and can therefore be modified for the different fiber and fabric types. The results are valid for the tested material only Contract No. 11-2010-11/09/129 20(50) Test report no. 12-2011 Soiling of textiles may occur in a number of ways including accidental spillage of liquids, static attraction of dirt and dust, and re-deposition of soils during laundering. Especially untreated woolen fabrics showed good soil repellence against water based soils. Goods made from wool are naturally water repellent. This is because the surface of wool has a very thin waxy, lipid coating chemically bonded to the surface. However, if the staining occurred it was more difficult to get wool clean than synthetic fabrics. Cotton materials got even more soiling, but they tolerate more efficient washing and detergents than wool does. The results are valid for the tested material only Contract No. 11-2010-11/09/129 21(50) Test report no. 12-2011 ANNEX 1: Quality documentation of tested Wool fabrics Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen a Top Specimen a Middle Specimen a Bottom Specimen b Top Specimen b Middle Specimen b Bottom Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation 09/129-01 Fabric 100% Merino Wool Woven White Superfine all wool merino 23.02.2011 Visual assessment of soil stains after one wash 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango 3.3 3.4 5.0 3.3 1.1 1.6 3.3 3.4 5.0 2.6 3.5 1.0 3.3 3.4 5.0 2.6 1.0 5.0 3.6 3.4 5.0 2.5 1.0 1.0 3.6 3.4 5.0 2.5 4.3 1.0 3.6 3.4 5.0 2.4 4.3 4.9 3.4 3.3 5.0 2.1 5.0 5.0 3.4 3.3 5.0 2.5 5.0 5.0 3.4 3.3 5.0 2.8 4.6 4.9 3.4 3.3 5.0 2.3 5.0 4.9 3.4 3.3 5.0 3.0 4.9 4.9 3.4 3.3 5.0 3.0 4.9 4.9 3.4 3.4 5.0 2.6 3.7 3.7 0.546 0.394 0.000 0.595 0.906 1.018 Visual assessment of soil stains after five washes. Specimens Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango Specimen A Top 4.1 4.0 5.0 4.6 5.0 1.9 Specimen A Middle 4.1 4.0 5.0 4.6 5.0 1.9 Specimen A Bottom 4.1 4.0 5.0 4.4 3.0 4.8 Mean 4.1 4.0 5.0 4.5 4.3 2.8 Standard deviation 0.226 0.739 0.000 0.450 1.073 1.513 The results are valid for the tested material only Contract No. 11-2010-11/09/129 22(50) Test report no. 12-2011 Sample No. 09/129-01 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 2 2.5 5 1.0 Specimen A drop 2 1.0 2 2.5 5 1.0 Mean 1.0 2.5 1.0 Standard deviation 0.000 0.000 0.000 Test date Washing condition Measurement points Length 1 Length 2 Length 3 Mean, length Standard deviation Width 1 Width 2 Width 3 Mean, width Standard deviation Comments Dimensional change 01.03 – 08.03.2011 See table 1 and table 2 Dimensional change Specimen A After After one wash five washes -2.0 % -2.3 % -2.6 % -2.8 % -2.0 % -2.8 % -2.2 % -2.7 % 0.329 0.329 -2.3 % -3.1 % -2.6 % -2.8 % -2.6 % -3.1 % -2.5 % -3.0 % 0.167 0.167 Abs.time in sec 5 5 - Dimensional change Specimen B After After one wash five washes -1.4 % -2.0 % -2.3 % -2.0 % -2.0 % -2.3 % -1.9 % -2.1 % 0.436 0.161 -2.6 % -3.4 % -2.9 % -3.7 % -2.6 % -3.4 % -2.7 % -3.5 % 0.165 0.165 Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 2 Number of observers 3 after one wash and 4 after five washes Results Pilling grade after 1 wash Pilling grade after 5 washes: Assessed on a scale from 1-5 5 5 (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) Changes in appearance Remarks Slightly surface fuzzing The results are valid for the tested material only Contract No. 11-2010-11/09/129 23(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen a Top Specimen a Middle Specimen a Bottom Specimen b Top Specimen b Middle Specimen b Bottom Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 09/129-10 Fabric 100% Wool Woven White Ullstandardväv ISO 105 style 537 23. 2.2011 2.9 2.9 2.9 2.9 2.9 2.9 2.6 2.6 2.6 2.6 2.6 2.6 2.7 0.521 2.9 2.9 2.9 3.1 3.1 3.1 3.5 3.5 3.5 3.5 3.5 3.5 3.3 0.477 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 3.8 3.8 3.8 3.4 3.4 3.4 4.3 4.3 4.0 4.1 4.4 4.1 3.9 0.542 1.3 4.6 1.3 4.4 4.9 5.0 5.0 5.0 5.0 1.0 4.8 4.9 3.9 1.632 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A. Top Specimen A. Middle Specimen A. Bottom Mean Standard deviation 3.9 3.9 3.9 3.9 0.747 3.5 3.5 3.5 3.5 0.522 The results are valid for the tested material only Contract No. 11-2010-11/09/129 4.8 4.8 4.8 4.8 0.452 4.8 4.8 4.8 4.8 0.452 5.0 5.0 5.0 5.0 0.000 Banana and mango 1.8 5.0 5.0 5.0 5.0 5.0 3.5 2.8 5.0 1.3 1.3 1.3 3.5 1.502 Banana and mango 5.0 5.0 5.0 5.0 0.000 24(50) Test report no. 12-2011 Sample No. 09/129-10 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 2 3.0 5 1.0 Specimen A drop 2 1.0 5 2.0 5 1.0 Mean 1.0 2.5 1.0 Standard deviation 0.000 0.577 0.000 Test date Washing condition Measurement points Length 1 Length 2 Length 3 Mean, length Standard deviation Width 1 Width 2 Width 3 Mean, width Standard deviation Comments Dimensional change 01.03 – 08.03.2011 See table 1 and table 2 Dimensional change Specimen A After After one wash five washes -1.7 % -3.4 % -1.4 % -3.7 % -1.4 % -3.1 % -1.5 % -3.4 % 0.165 0.286 -1.7 % -1.7 % -2.3 % -2.3 % -2.0 % -2.3 % -2.0 % -2.1 % 0.280 0.325 Abs.time in sec 5 5 - Dimensional change Specimen B After After one wash five washes -0.9 % -2.8 % -1.1 % -3.1 % -0.9 % -2.9 % -1.0 % -2.9 % 0.164 0.162 -0.9 % -2.6 % -1.1 % -1.7 % -1.7 % -2.9 % -1.2 % -2.4 % 0.436 0.595 Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 2 Number of observers 3 after one wash and 4 after five washes Results Pilling grade after 1 wash : Pilling grade after 5 washes: Assessed on a scale from 1-5 5 5 (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) Changes in appearance Remarks Slightly uneven appearance The results are valid for the tested material only Contract No. 11-2010-11/09/129 25(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks 09/129-18 Wool blankets 100% Wool Woven White Norway Label: Lillunn. Design of Norway. Best quality. Pure Nature. Handicraft. Only 100 % pure new wool. Marked 1. Lillunn 24.02.2011 Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 2.1 1.5 1.5 4.8 4.5 3.1 2.9 1.450 2.5 2.5 2.5 2.4 2.4 2.4 2.4 0.473 5.0 5.0 5.0 4.8 5.0 5.0 5.0 0.204 5.0 5.0 5.0 5.0 4.9 5.0 5.0 0.102 2.1 1.5 1.5 3.5 3.0 4.0 2.6 1.103 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A. Top Specimen A. Middle Specimen A. Bottom Mean Standard deviation 3.3 2.5 2.6 2.8 0.582 2.6 2.6 2.6 2.6 0.433 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 0.000 Banana and mango 2.1 1.5 2.1 5.0 5.0 5.0 3.5 1.608 Banana and mango 2.9 2.9 2.9 2.9 0.483 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot Abs.time wine in sec in sec chocolate in sec Specimen A drop 1 3.0 >5 4.5 >5 1.0 >5 Specimen A drop 2 2.0 >5 4.5 >5 1.0 >5 Mean 2.5 4.5 1.0 Standard deviation 0.577 0.000 0.000 - The results are valid for the tested material only Contract No. 11-2010-11/09/129 26(50) Test report no. 12-2011 Sample No. Test date Washing condition Measurement points Length 1 Length 2 Length 3 Mean, length Standard deviation Width 1 Width 2 Width 3 Mean, width Standard deviation Comments 09/129-18 Dimensional change 01.03 – 08.03.2011 See table 1 and table 2 Dimensional change Specimen A After After one wash five washes -6.5 % -9.5 % -6.5 % -10.0 % -6.4 % -10.3 % -6.5 % -9.9 % 0.049 0.450 +0.4 % -2.0 % +1.2 % -2.0 % +0.8 % -0.8 % +0.8 % -1.6 % 0.401 0.696 Dimensional change Specimen B After After one wash five washes -6.9 % -9.9 % -7.0 % -11.0 % -6.4 % -9.8 % -6.8 % -10.2 % 0.344 0.664 -0.8 % -3.1 % 0.0 % -1.6 % -0.8 % -3.6 % -0.5 % -2.8 % 0.457 1.040 Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 2 Number of observers 3 after one wash and 4 after five washes Results Pilling grade after 1 wash : Pilling grade after 5 Assessed on a scale from 1-5 5 washes: (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) 5 Changes in appearance Remarks Uneven structure, more felted The results are valid for the tested material only Contract No. 11-2010-11/09/129 27(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks 09/129-19 Wool blankets 100% Wool Woven White Norway Label: Lillunn. Design of Norway. Best quality. Pure Nature. Handicraft. Only 100 % pure new wool. Marked 2. Lillunn 24.02.2011 Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 2.0 2.0 2.0 2.0 3.8 2.0 2.3 0.765 2.3 2.3 2.3 2.5 2.5 2.5 2.4 0.495 4.8 4.8 4.8 5.0 4.8 5.0 4.8 0.381 4.8 4.8 4.8 4.8 5.0 5.0 4.8 0.381 3.6 3.6 4.4 3.1 2.3 3.1 3.4 0.777 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A. Top Specimen A. Middle Specimen A. Bottom Mean Standard deviation 2.5 2.5 2.5 2.5 0.369 2.5 2.5 2.5 2.5 0.369 5.0 5.0 5.0 5.0 0.000 5.0 4.8 5.0 4.9 0.289 5.0 5.0 5.0 5.0 0.000 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 3.0 >5 5.0 >5 3.0 Specimen A drop 2 2.5 >5 3.0 >5 2.0 Mean 2.8 4.0 2.5 Standard deviation 0.289 1.155 0.577 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 5.0 4.5 5.0 2.8 3.5 3.5 4.0 0.966 Banana and mango 5.0 5.0 5.0 5.0 0.000 Abs.time in sec >5 >5 - 28(50) Test report no. 12-2011 Sample No. Test date Washing condition Measurement points Length 1 Length 2 Length 3 Mean, length Standard deviation Width 1 Width 2 Width 3 Mean, width Standard deviation Comments 09/129-19 Dimensional change 01.03 – 08.03.2011 See table 1 and table 2 Dimensional change Specimen A After After one wash five washes -8.0 % -13.4 % -8.0 % -13.1 % -7.4 % -11.9 % -7.8 % -12.8 % 0.334 0.811 +1.6 % -1.2 % +1.6 % -0.8 % +0.8 % -2.0 % +1.3 % -1.3 % 0.471 0.601 Dimensional change Specimen B After After one wash five washes -9.0 % -15.4 % -8.6 % -13.6 % -8.9 % -13.8 % -8.8 % -14.3 % 0.193 0.989 0.0 % -3.6 % +0.4 % -2.9 % +0.8 % -2.0 % +0.4 % -2.8 % 0.402 0.790 Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 2 Number of observers 3 after one wash and 4 after five washes Results Pilling grade after 1 wash : Pilling grade after 5 washes: Assessed on a scale from 1-5 5 5 (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) Changes in appearance Remarks Uneven structure, more felted The results are valid for the tested material only Contract No. 11-2010-11/09/129 29(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling 09/129-20 Sweater Janus 100% Merino Wool Knitted Colour Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Use detergent for wool White L Norway Label: Janus Large, Made in Norway by Janusfabrikken AS, N-5267 Espeland Janusfabrikken AS 24.02.2011 Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango 1.0 2.1 4.5 2.1 1.1 1.0 1.0 2.1 4.5 1.9 1.6 1.6 1.0 2.1 4.3 1.5 1.0 1.0 1.0 2.0 4.3 1.5 2.4 2.9 1.0 2.0 4.3 1.9 3.6 2.3 1.0 2.0 4.3 1.6 1.5 1.0 1.0 2.1 4.3 1.8 1.9 1.6 0.000 0.169 0.319 0.571 1.013 0.770 Visual assessment of soil stains after five washes. Specimens Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango Specimen A. Top 1.1 2.1 4.8 2.4 2.9 3.6 Specimen A. Middle 1.1 2.1 4.8 2.3 3.8 3.6 Specimen A. Bottom 1.1 2.1 4.8 2.0 3.8 1.0 Mean 1.1 2.1 4.8 2.2 3.5 2.8 Standard deviation 0.226 0.226 0.452 0.334 0.782 1.340 Visual assessment of soil stains after 10 washes and wipe off. Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 2 1.0 2 1.0 Specimen A drop 2 1.0 2 1.0 2 1.0 Mean 1.0 1.0 1.0 Standard deviation. 0.000 0.000 0.000 Specimens The results are valid for the tested material only Contract No. 11-2010-11/09/129 Abs.time in sec 2 2 - 30(50) Test report no. 12-2011 Sample No. Test date Washing condition Measurement points Length 1 Length 2 Length 3 Mean, length Standard deviation Width 1 Width 2 Width 3 Mean, width Standard deviation Comments 09/129-20 Dimensional change 01.03 – 08.03.2011 See table 1 and table 2 Dimensional change Specimen A After After one wash five washes -4.0 % -4.5 % -7.0 % -7.5 % -5.9 % -6.4 % -5.7 % -6.2 % 1.500 1.496 +3.2 % +3.2 % +2.8 % +2.8 % +0.8 % -1.2 % +2.3 % +1.6 % 1.289 2.447 Dimensional change Specimen B After After one wash five washes -5.0 % -5.5 % -6.5 % -6.0 % -5.0 % -4.0 % -5.5 % -5.1 % 0.862 1.036 -0.8 % -0.8 % +0,4 % 0.0 % 0.0 % +0.8 % -0.1 % 0.0 % 0.617 0.800 Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 2 Number of observers 3 after one wash and 4 after five washes Results Pilling grade after 1 wash : Pilling grade after 5 washes: Assessed on a scale from 1-5 5 5 (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) Changes in appearance Remarks Some surface fuzzing, wrinkled The results are valid for the tested material only Contract No. 11-2010-11/09/129 31(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation 09/129-22 Jacket 100% Wool Knitted White with pink pattern Norway Norwegian wool. The product is not on the marked (not for sale) Dale of Norway 28.02.2011 Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango 1.0 2.0 4.0 1.6 2.5 4.3 1.0 2.0 4.0 1.6 2.3 4.3 1.0 2.0 4.0 1.6 1.0 3.3 1.0 2.0 4.0 2.0 2.3 3.5 1.0 2.0 4.0 2.0 2.3 3.9 1.0 2.0 4.0 2.0 2.3 1.3 1.0 2.0 4.0 1.8 2.1 3.4 0.000 0.000 0.626 0.355 0.584 1.132 Visual assessment of soil stains after five washes. Specimens Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango Specimen A. Top 1.1 2.5 4.8 2.0 4.4 4.8 Specimen A. Middle 1.1 2.5 5.0 2.4 4.5 5.0 Specimen A. Bottom 1.1 2.5 5.0 2.1 3.9 4.8 Mean 1.1 2.5 4.9 2.2 4.3 4.8 Standard deviation 0.226 0.369 0.289 0.326 0.500 0.389 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 1-2 1.0 1-2 1.0 Specimen A drop 2 1.0 1-2 1.0 1-2 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Abs.time in sec 4 4 - 32(50) Test report no. 12-2011 Sample No. Test date Washing condition Measurement points Length 1 Length 2 Length 3 Mean, length Standard deviation Width 1 Width 2 Width 3 Mean, width Standard deviation Comments 09/129-22 Dimensional change 01.03 – 08.03.2011 See table 1 and table 2 Dimensional change Specimen A After After one wash five washes -3.0 % -4.5 % -3.5 % -5.5 % -3.0 % -3.5 % -3.2 % -4.5 % 0.288 0.986 -2.4 % -2.4 % -0.4 % +1.2 % -0.4 % 0.0 % -1.1 % -0.4 % 1.144 1.823 Dimensional change Specimen B After After one wash five washes -3.5 % -4.0 % -3.0 % -4.0 % -3.0 % -6.0 % -3.2 % -4.7 % 0.279 1.160 -0.8 % -1.2 % -2.0 % -2.0 % -4.8 % -5.6 % -2.5 % -2.9 % 2.044 2.333 Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 2 Number of observers 3 after one wash and 4 after five washes Results Pilling grade after 1 wash : Pilling grade after 5 washes: Assessed on a scale from 1-5 5 5 (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) Changes in appearance Remarks Some surface fuzzing The results are valid for the tested material only Contract No. 11-2010-11/09/129 33(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date 09/129-23 Handmade sample, knitted rib 100% Norwegian crossbreed sheep wool White UK Curtis 17.3.2011 Visual assessment of soil stains after 10 washes and wipe off. Test date 30.03.2011 Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 4.0 >5 4.5 >5 4.0 Mean 4.0 4.5 4.0 Standard deviation 0.000 0.000 0.000 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Abs.time in sec >5 - 09/129-24 Handmade sample, knitted flat 100% Norwegian crossbreed sheep wool White UK Curtis 17.3.2011 Visual assessment of soil stains after 10 washes and wipe off. Test date 30.03.2011 Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 4.0 >5 5.0 >5 4.0 Mean 4.0 5.0 4.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Abs.time in sec >5 - 34(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date 09/129-25 Handmade sample, knitted flat 100% Norwegian crossbreed sheep wool White UK Curtis 17.3.2011 Visual assessment of soil stains after 10 washes and wipe off. Test date 30.03.2011 Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 4.0 >5 5.0 >5 4.0 Mean 4.0 5.0 4.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Abs.time in sec >5 - 35(50) Test report no. 12-2011 ANNEX 2: Quality documentation of wool mix fabrics and fabrics other than wool Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation 09/129-02 Fabric 100% Cotton Woven White. 23.02.2011 Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce 1.8 2.8 5.0 1.4 3.0 1.8 2.8 5.0 1.4 3.3 1.8 2.8 5.0 1.4 3.0 1.8 2.9 5.0 1.4 2.9 1.8 2.9 5.0 1.4 2.9 1.8 2.9 5.0 1.4 2.8 1.8 2.8 5.0 1.4 3.0 0.442 0.567 0.000 0.423 0.641 Banana and mango 1.9 5.0 4.4 1.4 4.4 5.0 3.7 1.579 Visual assessment of soil stains after five washes Specimens Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango Specimen A. Top 2.1 2.9 5.0 1.0 4.8 4.8 Specimen A. Middle 2.1 2.9 5.0 1.0 4.8 4.6 Specimen A. Bottom 2.1 2.9 5.0 1.0 4.8 4.6 Mean 2.1 2.9 5.0 1.0 4.8 4.7 Standard deviation. 0.226 0.226 0.000 0.000 0.452 0.444 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 0 1.0 0 1.0 Specimen A drop 2 1.0 0 1.0 0 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Abs.time in sec 0 0 - 36(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation 09/129-03 Fabric 100% Silk Woven White. 23.02.2011 Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive Hot Tomato Banana wine oil chocolate sauce and mango 1.0 1.9 3.4 1.5 4.3 5.0 1.0 1.9 3.4 1.5 4.3 5.0 1.0 1.9 3.4 1.5 4.3 5.0 1.0 1.9 3.4 1.5 4.1 5.0 1.0 1.9 3.4 1.5 4.1 5.0 1.0 1.9 3.4 1.5 4.1 5.0 1.0 1.9 3.4 1.5 4.2 5.0 0.000 0.221 0.663 0.361 0.247 0.000 Visual assessment of soil stains after five washes. Specimens Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango Specimen A. Top 1.6 2.0 4.5 2.0 4.8 4.8 Specimen A. Middle 1.6 2.0 4.5 2.0 4.8 4.8 Specimen A. Bottom 1.6 2.0 4.5 2.0 4.8 4.8 Mean 1.6 2.0 4.5 2.0 4.8 4.8 Standard deviation 0.433 0.000 0.369 0.000 0.452 0.452 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 3 1.0 5 1.0 Specimen A drop 2 1.0 3 1.0 5 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Abs.time in sec 5 5 - 37(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 09/129-04 Fabric 88 % Wool, 10 % Polyamide, 2 % Lycra Woven White. 23.02.2011 3.5 3.5 3.5 3.5 3.5 3.5 3.5 0.361 4.4 4.4 4.4 4.5 4.5 4.5 4.4 0.473 5.0 5.0 5.0 4.8 4.8 5.0 4.9 0.282 3.1 3.6 3.1 3.5 3.6 3.5 3.4 0.408 2.8 2.8 2.8 2.6 2.6 2.6 2.7 0.507 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A. Top Specimen A. Middle Specimen A. Bottom Mean Standard deviation 4.0 4.0 4.0 4.0 0.640 4.5 4.4 4.5 4.5 0.891 4.8 4.8 4.8 4.8 0.452 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 0.000 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 2.0 5 2.0 5 1.5 Specimen A drop 2 2.0 1-2 2.0 1-2 1.5 Mean 2.0 2.0 1.5 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 1.0 1.0 5.0 2.8 1.3 4.9 2.6 1.809 Banana and mango 5.0 5.0 5.0 5.0 0.000 Abs.time in sec 5 5 - 38(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 09/129-05 Tube. 100% Cotton Knitted White. Dovre interlock. 23.02.2011 1.0 1.0 1.0 1.1 1.1 1.1 1.1 0.169 2.1 2.1 2.1 2.4 2.4 2.4 2.3 0.361 4.6 4.6 4.6 4.6 4.6 4.9 4.7 0.408 1.6 1.6 1.6 1.5 1.5 1.8 1.6 0.489 1.0 1.0 2.8 1.0 1.0 3.3 1.7 1.018 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A. Top Specimen A. Middle Specimen A. Bottom Mean Standard deviation 1.4 1.4 1.4 1.4 0.433 2.1 2.1 2.1 2.1 0.226 4.8 4.8 4.8 4.8 0.452 2.5 2.1 2.1 2.3 0.399 2.9 3.4 3.8 3.3 0.537 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 1 1.0 1 1.0 Specimen A drop 2 1.0 1 1.0 1 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 2.1 2.5 3.9 1.0 1.0 3.7 2.4 1.260 Banana and mango 2.9 2.9 2.9 2.9 0.226 Abs.time in sec 4 4 - 39(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 09/129-06 Fabric 100 % Polyamide (Nylon) Woven White. Polyamidstandard väv, style 361 23.02.2011 3.9 3.9 3.9 3.9 3.9 3.9 3.9 0.731 4.4 4.4 4.4 4.2 4.2 4.2 4.3 0.660 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 3.5 3.6 3.5 3.5 3.6 3.5 3.5 0.388 2.5 5.0 3.0 4.8 5.0 5.0 4.2 1.132 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A Top Specimen A Middle Specimen A Bottom Mean Standard deviation 2.8 2.8 2.8 2.8 0.261 4.5 4.4 4.5 4.5 0.498 5.0 5.0 5.0 5.0 0.000 4.8 4.6 4.6 4.7 0.444 5.0 5.0 5.0 5.0 0.000 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 0-1 2.0 0-1 1.0 Specimen A drop 2 1.0 0-1 2.0 0-1 1.0 Mean 1.0 2.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 5.0 1.5 1.3 5.0 5.0 1.8 3.3 1.847 Banana and mango 4.8 1.8 1.1 2.5 1.698 Abs.time in sec 0-1 0-1 - 40(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 09/129-08 Fabric 100 % Acrylic Woven White. Acrylstandard väv, ISO 105, style 864, 80 g 23.02.2011 3.8 3.8 3.8 3.8 3.8 3.8 3.8 0.571 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 3.5 3.1 3.1 4.0 4.0 4.0 3.6 0.863 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A. Top Specimen A. Middle Specimen A. Bottom Mean Standard deviation 3.1 3.1 3.1 3.1 0.569 4.8 4.6 4.8 4.7 0.450 5.0 5.0 5.0 5.0 0.000 4.2 4.6 4.6 4.4 0.595 5.0 5.0 5.0 5.0 0.000 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 0 2.0 0 1.0 Specimen A drop 2 1.0 0 2.0 0 1.0 Mean 1.0 2.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 5.0 1.0 5.0 5.0 1.0 2.5 3.3 1.871 Banana and mango 5.0 2.0 5.0 4.0 1.809 Abs.time in sec 0 0 - 41(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens Specimen A Top Specimen A Middle Specimen A Bottom Mean Standard deviation 09/129-09 Fabric 100 % Polyester Woven White. 1 m Polyester ISO 105. 107 g 23.02.2011 Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango 4.3 5.0 5.0 2.5 1.0 1.0 4.3 5.0 5.0 2.5 2.9 1.0 4.3 5.0 5.0 2.5 2.4 1.3 4.3 4.8 5.0 2.8 1.4 5.0 4.3 4.8 5.0 3.3 3.9 1.3 4.3 4.8 5.0 3.5 3.9 5.0 4.3 4.9 5.0 2.8 2.9 3.0 0.756 0.366 0.000 0.566 1.323 1.859 Visual assessment of soil stains after five washes. Red Coffee Olive Hot Tomato wine oil chocolate sauce 4.0 4.0 4.0 4.0 0.640 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 0.000 2.9 3.0 3.1 3.0 0.640 4.8 4.5 3.5 4.3 0.723 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 0 2.0 0 1.0 Specimen A drop 2 1.0 0 2.0 0 1.0 Mean 1.0 2.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 4.1 1.1 1.0 2.1 1.550 Abs.time in sec 0 0 - 42(50) Test report no. 12-2011 Sample No. 09/129-09 Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 3 Number of observers 4 Results Pilling grade after 1 wash : Pilling grade after 5 Assessed on a scale from 1-5 5 washes: (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) 5 5 5 Changes in appearance Remarks The fabric was uneven before wash The results are valid for the tested material only Contract No. 11-2010-11/09/129 43(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour 09/129-11 Sweater 100 % Acrylic Knitted use softener White. 42 Bangladesh Label: Use softener, 100 % Acrylic Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens Specimen A Top Specimen A Middle Specimen A Bottom Mean Standard deviation H & M Hennes & Mauritz 23.02.2011 Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red wine Coffee Olive oil Hot Tomato chocolate sauce 3.5 3.5 3.5 3.5 3.5 3.5 3.5 0.361 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 3.8 3.8 4.3 4.8 4.0 4.3 4.1 0.741 3.1 3.1 4.4 4.5 2.5 2.8 3.4 0.955 Visual assessment of soil stains after five washes Red Coffee Olive oil Hot Tomato wine chocolate sauce 3.8 3.8 3.6 3.7 0.257 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 0.000 5.0 5.0 5.0 5.0 0.000 Visual assessment of soil stains after 10 washes and wipe off. Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 0 1.0 0 1.0 Specimen A drop 2 1.0 0 1.0 0 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 Specimens The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 4.5 3.3 3.1 2.9 2.5 3.3 3.3 0.847 Banana and mango 4.9 4.3 4.8 4.6 0.569 Abs.time in sec 0 0 - 44(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling Colour 09/129-12 Sweater Janus, Iris 80% Merino Wool, 20% Polyamide Knitted White 46 Norway Label: Iris 46, Made in Norway by Janusfabrikken AS, N-5267 Espeland Janusfabrikken AS 23.02.2011 Size Produced in Remarks Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red wine Coffee Olive oil Hot Tomato chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B. Bottom Mean Standard deviation Specimens 1.1 1.1 1.1 1.1 1.1 1.1 1.1 0.221 1.9 1.9 1.9 1.9 1.9 1.9 1.9 0.221 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0.000 2.4 2.4 2.4 2.4 2.4 2.4 2.4 0.423 2.9 2.3 1.9 1.0 3.4 1.0 2.1 0.959 Visual assessment of soil stains after five washes. Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A Top Specimen A Middle Specimen A Bottom Mean Standard deviation 1.1 1.1 1.1 1.1 0.226 1.9 1.9 1.9 1.9 0.226 5.0 5.0 5.0 5.0 0.000 2.0 2.0 2.0 2.0 0.369 3.9 3.5 3.9 3.8 0.337 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 1-2 1.0 1-2 1.0 Specimen A drop 2 1.0 1-2 1.0 1-2 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 4.0 4.5 4.0 4.8 1.3 1.3 3.3 1.601 Banana and mango 4.3 4.8 4.5 4.5 0.674 Abs.time in sec 5 5 - 45(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling 09/129-13 T-shirt Safa 80 % Wool, 20 % Silk Knitted Colour Size Produced in Remarks Producer/Supplier/Business Received date White. XL Label: Machine wash wool program, avoid tumble dryer Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red wine Coffee Olive oil Hot Tomato chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 23.02.2011 1.8 1.8 1.8 1.8 1.8 1.8 1.8 0.442 2.1 2.1 2.1 2.1 2.1 2.1 2.1 0.221 4.2 4.2 4.2 4.2 4.2 4.2 4.2 0.708 2.0 2.0 2.0 2.3 2.3 2.3 2.1 0.495 2.9 1.4 2.1 2.3 2.3 2.3 2.2 0.567 Visual assessment of soil stains after five washes. Red wine Coffee Olive oil Hot Tomato chocolate sauce Specimen A Top Specimen A Middle Specimen A Bottom Mean Standard deviation 2.0 2.0 2.0 2.0 0.369 2.1 2.1 2.1 2.1 0.226 4.2 4.2 4.2 4.2 0.724 2.4 2.4 2.4 2.4 0.433 3.8 3.8 3.8 3.8 0.452 Visual assessment of soil stains after 10 washes and wipe off. Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 4 1.0 4 1.0 Specimen A drop 2 1.0 4 1.0 4 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 Specimens The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 4.0 2.6 3.3 1.6 2.9 2.9 2.9 0.811 Banana and mango 4.3 4.2 4.2 4.2 0.815 Abs.time in sec 4 4 - 46(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling 09/129-14 Sweater 65 % Acrylic, 30 % Wool, 5 % Angora Knitted Colour Size Produced in Remarks Producer/Supplier/Business Received date White L China - Gentle wash Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red wine Coffee Olive oil Hot Tomato chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens Vero Moda 23.02.2011 2.4 2.4 2.5 2.5 2.5 2.5 2.5 0.487 3.0 3.0 3.0 3.1 3.1 3.1 3.1 0.473 4.8 4.6 4.8 5.0 5.0 4.9 4.8 0.351 5.0 4.9 5.0 5.0 5.0 4.9 5.0 0.141 4.1 4.1 4.1 3.3 3.4 3.5 3.8 0.489 Visual assessment of soil stains after five washes. Red wine Coffee Olive oil Hot Tomato chocolate sauce Specimen A Top Specimen A Middle Specimen A Bottom Mean Standard deviation 2.9 2.9 2.9 2.9 0.226 3.0 3.0 3.0 3.0 0.000 4.8 4.8 4.8 4.8 0.452 4.8 4.6 4.8 4.7 0.450 4.8 4.8 4.8 4.8 0.452 Visual assessment of soil stains after 10 washes and wipe off. Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 5 1.0 0 1.0 Specimen A drop 2 1.0 5 1.0 0 1.0 Mean 1.0 1.0 1.0 Standard deviation. 0.000 0.000 0.000 Specimens The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 3.5 3.8 4.6 3.3 3.3 3.3 3.6 0.642 Banana and mango 4.6 4.6 4.6 4.6 0.433 Abs.time in sec 5 5 - 47(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling 09/129-15 T-shirt Nike 100 % Polyester Knitted Colour Size Produced in Remarks White. XXL Thailand Label: Wash with like colors. Do not use softeners. Remove immediately. Do not allow to lay on itself when wet. Do not iron design 24.02.2011 Producer/Supplier/Business Received date Do not use softeners Pilling after one and five washes Date of test 1.3.2011-9.3.2011 Atmosphere 20 2 C and 65 4 % RH Pre-treatment One wash and five washes Number of test specimens 3 Number of observers 4 Results Pilling grade after 1 wash : Pilling grade after 5 Assessed on a scale from 1-5 5 washes: (5 = no pilling, 1 = very severe 5 5 pilling or surface fuzzing) 5 5 5 Changes in appearance Hint of surface fuzzing Remarks The results are valid for the tested material only Contract No. 11-2010-11/09/129 48(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling 09/129-17 Sweater 45 % Wool, 45 % Cotton, 10 % Polyamide Knitted White 12 China Wash separately – inside out. We recommend detergent without optical brightener. Stretch into size when tumbling dry. Do not soak. Do not dry in direct sunlight. Claire 24.02.2011 Colour Size Produced in Remarks Producer/Supplier/Business Received date Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive oil Hot Tomato wine chocolate sauce Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation Specimens 1.8 1.8 1.8 1.8 1.8 1.8 1.8 0.442 1.9 1.9 1.9 1.9 1.9 1.9 1.9 0.221 5.0 5.0 5.0 4.8 4.8 4.8 4.9 0.338 2.1 2.1 2.3 2.3 2.3 2.3 2.2 0.487 3.0 2.9 3.0 2.9 2.9 2.9 2.9 0.408 Visual assessment of soil stains after five washes Red Coffee Olive oil Hot Tomato wine chocolate sauce Specimen A. Top Specimen A. Middle Specimen A. Bottom Mean Standard deviation 1.5 1.5 1.5 1.5 0.369 1.9 1.9 1.9 1.9 0.226 4.8 4.8 4.8 4.8 0.452 2.0 2.1 2.1 2.1 0.195 4.4 4.4 4.5 4.4 0.469 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 2.0 5 5.0 5 2.0 Specimen A drop 2 1.5 5 2.5 5 3.5 Mean 1.8 3.8 2.8 Standard deviation 0.289 1.443 0.866 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Banana and mango 2.9 3.3 3.4 3.1 3.4 2.9 3.1 0.429 Banana and mango 3.5 3.6 3.6 3.6 0.634 Abs.time in sec 5 5 - 49(50) Test report no. 12-2011 Sample No. Product Brand Fibre labelling Material Care labelling 09/129-21 Children’s dress Janus 70 % Merino Wool, 28 % Polyamide, 2 % Lycra Knitted Colour Size Produced in Remarks Producer/Supplier/Business Received date Test date Specimens Specimen A Top Specimen A Middle Specimen A Bottom Specimen B Top Specimen B Middle Specimen B Bottom Mean Standard deviation White 130 Norway Krinkelull. Label: Janus 130 Janusfabrikken AS 28.02.2011 Visual assessment of soil stains after one wash. 14.3-30.3-2011 Red Coffee Olive Hot Tomato Banana wine oil chocolate sauce and mango 1.8 2.8 5.0 2.1 3.0 3.0 1.8 2.8 5.0 2.1 3.0 1.3 1.8 2.8 5.0 2.1 2.8 1.3 1.8 2.8 5.0 2.0 3.0 4.1 1.8 2.8 5.0 2.0 3.0 3.8 1.8 2.8 5.0 2.0 3.0 2.5 1.8 2.8 5.0 2.1 3.0 2.6 0.442 0.442 0.000 0.399 0.204 1.220 Visual assessment of soil stains after five washes. Specimens Red Coffee Olive oil Hot Tomato Banana wine chocolate sauce and mango Specimen A Top 1.4 2.6 5.0 2.4 4.5 4.4 Specimen A Middle 1.4 2.6 5.0 2.4 4.4 4.3 Specimen A Bottom 1.4 2.6 5.0 2.4 4.5 4.4 Mean 1.4 2.6 5.0 2.4 4.5 4.4 Standard deviation 0.433 0.226 0.000 0.226 0.396 0.310 Visual assessment of soil stains after 10 washes and wipe off. Specimens Red Abs.time Coffee Abs.time Hot wine in sec in sec chocolate Specimen A drop 1 1.0 0 1.0 0 1.0 Specimen A drop 2 1.0 0 1.0 0 1.0 Mean 1.0 1.0 1.0 Standard deviation 0.000 0.000 0.000 The results are valid for the tested material only Contract No. 11-2010-11/09/129 Abs.time in sec 0 0 - 50(50)