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Chemistry Letters CMLTAG ISSN 0366-7022 No.3 March, 2002 Copyright Ó 2002 The Chemical Society of Japan 266 Enantiopure trans- and cis-3-Aminoindan-1ols: Preparation and Application as Novel Basic Resolving Agents Kazushi Kinbara, Yoshiyuki Katsumata, and Kazuhiko Saigo 268 Fluoride Ion Abstraction of Phosphonium Cations from Their Counter Anion: A Novel Synthetic Method of Fluorophosphoranes Shohei Sase, Naokazu Kano, and Takayuki Kawashima 270 1,4-Dihydroxylation of 1,3-Conjugated Dienes Promoted by the Pt(III) Dinuclear Complex Masahiko Ochiai and Kazuko Matsumoto 272 Rhodium Catalyzed Anti-Markovnikov Addition of Triphenylphosphine to 1,3-Dienes A Novel Method to Separate Pure (Z)-1,3Alkadienes from Isomeric Mixtures Mieko Arisawa, Ryohei Momozuka, and Masahiko Yamaguchi C-32 274 Chemistry Letters No.3 2002 Solvent-Free One-Pot Reduction of Imines Generated in situ from Aldehydes and Aniline by Tributyltin Hydride on Silica Gel Ryoichi Hiroi, Norikazu Miyoshi, and Makoto Wada 276 Catalytic Asymmetric Syntheses of ICI199441 and CP-99994 Using Nitro-Mannich Reaction Natsuko Tsuritani, Ken-ichi Yamada, Naoki Yoshikawa, and Masakatsu Shibasaki 278 Enhanced Leaving Ability of Methoxy Group and Retarded Deprotonation on the Carbon Atom Linked to the 1-Position of 8-Phosphino- or 8-Amino-naphthalene Akio Toshimitsu, Tomoyuki Saeki, and Kohei Tamao 280 Synthesis of Benzocyclooctene Derivatives via Thermal Ring Expansion of Dienylbenzocyclobutenes Toshiyuki Hamura, Shinsuke Tsuji, Takashi Matsumoto, and Keisuke Suzuki 282 The 5-endo-trig Cyclization of gem-Difluoroolefins with sp3 Carbon Nucleophiles: Synthesis of 1-Fluorocyclopentenes Junji Ichikawa, Kotaro Sakoda, and Yukinori Wada Copyright Ó 2002 The Chemical Society of Japan Chemistry Letters No.3 2002 284 C-33 Catalytic Oxidation of Alcohols with Ru(Pybox)(Pydic) Complex Seiji Iwasa, Kazushi Morita, Kentaro Tajima, Ahmad Fakhruddin, and Hisao Nishiyama 286 A New Condensation Reaction for the Synthesis of Carboxylic Esters from Nearly Equimolar Amounts of Carboxylic Acids and Alcohols Using 2-Methyl-6-nitrobenzoic Anhydride Isamu Shiina, Ryoutarou Ibuka, and Mari Kubota 288 Novel Valence Expansion Reactions Using KC8 : A New Route to Hexavalent Organotellurium Compounds from Divalent Tellurium Masataka Miyasato, Mao Minoura, Yohsuke Yamamoto, and Kin-ya Akiba 290 Formation of Cyclopropanes by the Reductive Coupling of 1,3-Dihalides Promoted by Titanocene(II) Species Takeshi Takeda, Keiko Shimane, Fujiwara, and Akira Tsubouchi 292 Tooru Comparison of Cyclic and Acyclic Phosphites by Selective Phosphorylation. Synthesis of Phosphatidylinositol 4-Phosphate Yutaka Watanabe, Hirofumi Munetsugu, and Minoru Hayashi Copyright Ó 2002 The Chemical Society of Japan C-34 294 Chemistry Letters No.3 2002 Ruthenium-Mediated Domino Sequence Forming Six-Membered Ring Diene from Ene-Yne and Alkene Masahiro Murakami, Minoru Ubukata, and Yoshihiko Ito 296 Application of High Pressure Induced by Water-freezing to the Michael Reaction of Alcohols with ,-Enones Yujiro Hayashi and Koichi Nishimura 298 Catalytic, Enantioselective Propargyl- and Allenylation Reactions of -Imino Ester Hirotaka Kagoshima, Tetsumaru Uzawa, and Takahiko Akiyama 300 Diastereoselective Additions of Ethynyl Grignard Reagent to Erythrulose Derivatives Shoji Kobayashi, Parthasarathi Das, Guang Xing Wang, Takashi Mita, Martin J. Lear, and Masahiro Hirama 302 Catalytic Asymmetric 1,3-Dipolar Cycloaddition of a Nitrone Bearing a Bulky Amide Moiety to -Substituted Allylic Alcohols Xia Ding, Yutaka Ukaji, Shuhei Fujinami, and Katsuhiko Inomata Copyright Ó 2002 The Chemical Society of Japan Chemistry Letters No.3 2002 304 C-35 First Aggregation of L-Cysteinato Cobalt(III) Octahedrons Assisted by Trigonal-Planar Silver(I) and Trigonal-Prismatic Sodium(I) Ions Takumi Konno, Tatsuya Kawamoto, Rie Kuwabara, Takashi Yoshimura, and Masakazu Hirotsu 306 Chemoselective Substitution Reaction of 2Bromo-3-methoxy-1,4-naphthoquinone Bryanne L. Stills, Carolyn B. Lauzon, and Tetsuo Otsuki 308 Electrochemical Oscillation in the Oxidation of Tritolylamines Using YBa2 Cu3 O7 Ceramics Electrode in Oxygen Atmosphere Masakazu Tatsumi, Yutaka Isida, Takayuki Ariyama, and Masafumi Yano 310 Synthesis of Ultrathin Films of Prussian Blue by Successive Ion Adsorption Technique Isamu Moriguchi, Haruna Kamogawa, Kaori Hagiwara, and Yasutake Teraoka 312 Molecular Assembly of Bachteriochlorophyll a Using Light-harvesting Model 1-Helix Polypeptides and 2-Helix Polypeptide with Disulfide-linkage Mamoru Nango, Ayumi Kashiwada, Hiroyuki Watanabe, Shuhei Yamada, Taku Yamada, Makiko Ogawa, Toshiki Tanaka, and Kouji Iida Copyright Ó 2002 The Chemical Society of Japan C-36 314 Chemistry Letters No.3 2002 Conversions of Thiirene 1-Oxides to Iminothioketones or Oxazoles through Probable Intermediates Sulfilimines Yutaka Ono, Yoshiaki Sugihara, Akihiko Ishii, and Juzo Nakayama 316 Pressure-induced Metamagnetic Behavior in a Quasi-One-Dimensional Molecule-based Ferrimagnet Kentaro Suzuki, Yuko Hosokoshi, and Katsuya Inoue 318 Sc(OTf)3 Catalyzed Electrophilic Amination of Arenes: An Expeditious Synthesis of Aryl Hydrazides J. S. Yadav, B. V. S. Reddy, G. Veerendhar, R. Srinivasa Rao, and K. Nagaiah 320 Liquid-Crystalline Assemblies Containing Ionic Liquids: An Approach to Anisotropic Ionic Materials Masafumi Yoshio, Tomohiro Mukai, Kiyoshi Kanie, Masahiro Yoshizawa, Hiroyuki Ohno, and Takashi Kato 322 In Situ Insertion of Poly(aniline) into Molybdenum Oxide Layers Ke Shao, Ying Ma, Zhao-hui Chen, Xue-hai Ji, Wen-sheng Yang, and Jian-nian Yao Copyright Ó 2002 The Chemical Society of Japan Chemistry Letters No.3 2002 324 C-37 Photorefractive Properties of the Isotropic Phase of Cyanobiphenyl Side-chain Liquid Crystalline Polymers Takeo Sasaki, Teruyuki Shimada, and Koji Tachibana 326 Circular Dichroism Measurement of a Protein in Dried Thin Films Takunori Harada and Reiko Kuroda 328 High Sensitive DNA Detection Amplified by Enlarging Au-Nanoparticles in situ Zhanfang Ma, Jinru Li, Long Jiang, Mengsu Yang, and Sen-fang Sui 330 A Novel Shape-Selective Catalyst, Pt-Promoted Rb2:1 H0:9 PW12 O40 , for Hydrogenation of Aromatic Compounds Miki Yoshimune, Yusuke Yoshinaga, and Toshio Okuhara 332 An Electrochemical Quartz Crystal Microbalance Study of the Electrochemical Oscillation in H2 O2 -Reduction Reaction Xiaqin Wu, Fang Wang, Long Jin, Hexing Li, and Zongrang Zhang Copyright Ó 2002 The Chemical Society of Japan C-38 334 Chemistry Letters No.3 2002 Direct Electrochemistry of Cytochrome c Embedded in Membrane Films of AnionicType Lipids Prepared via Ion-Exchange Masato Tominaga, Junko Yanagimoto, and Naotoshi Nakashima 336 Rotaxane-like Characteristics of [2]Pseudorotaxane Complexes of -Cyclodextrin and Dodecamethylene Threading Chain Derivatives with Cationic End Groups Byeong-Su Kim and Jong-In Hong 338 Effects of Microwave Absorbents in NO Removal by Microwave Discharge of NO/Ar Mixture at Atmospheric Pressure Masaharu Tsuji, Kosuke Nakano, Jun Kumagae, Takeshi Tsuji, Seong-Ho Yoon, Yozo Korai, and Isao Mochida 340 Excited State Structure of N-(4-cyanophenyl)carbazole by Time-Resolved Infrared Absorption Spectroscopy Anunay Samanta, Satyen Saha, Hironori Ishikawa, and Hiro-o Hamaguchi 342 Regenerable Surface Plasmon Resonance (SPR)-based Immunosensor for Highly Sensitive Measurement of Sub-ppb Levels of Benzo(a)pyrene Norio Miura, Makoto Sasaki, Go Sakai, and K. Vengatajalabathy Gobi Copyright Ó 2002 The Chemical Society of Japan Chemistry Letters No.3 2002 344 C-39 Influences of A-site Partial Substitution for BaCo0:7 Fe0:3 O3 Oxide on Perovskite Structure and Oxygen Permeability Kazuya Kinoshita, Hajime Kusaba, Go Sakai, Kengo Shimanoe, Norio Miura and Noboru Yamazoe 346 Chiral Crystallization of a Linear Twocoordinated Palladium(0) Complex Bearing Propeller-shaped Bulky Phosphine Ligands Tsuyoshi Matsumoto, Takeshi Kasai, and Kazuyuki Tatsumi 348 Dinuclear Copper Complexes of N-(2-Hydroxybenzylidene or 5-Bromo-2-hydroxybenzylidene)-4,6-O-ethylidene--D-glucopyranosylamine: Coordination Variation and Structural Diversity Ajay K. Sah, Chebrolu P. Rao, Pauli K. Saarenketo, Kari Rissanen, G. A. van Albada, and Jan Reedijk 350 Rare Earth Ion Center in Distorted Square Anti-Prism Coordination Environment: A Novel Three-Dimensional Coordination Polymer with Channels Xu Haitao, Zheng Nengwu, Jin Xianglin, Yang Ruyi, and Li Zhengquan 352 Unusual Absorption Spectra Found for Some Phthalocyaninatozinc(II) Complexes Bearing Dendritic Substituents at Positions Kuninobu Kasuga, Noriyuki Matsuura, Koji Inoue, Makoto Handa, Tamotsu Sugimori, Kimio Isa, and Makoto Nakata Copyright Ó 2002 The Chemical Society of Japan C-40 354 Chemistry Letters No.3 2002 Cu(II) Coordination Structure in NAD Glycohydrolase from Agkistrodon acutus Venom Studied by EPR Spectroscopy Shuang Ding Wu, Xiaolong Xu, Yongshu Xie, Lixin Chen, Zhenlong Chen, and Qingliang Liu 356 Highly Ordered Coronene Adlayer on Au(111) Surface Formed in Benzene Solution: In situ Scanning Tunneling Microscopy Study Soichiro Yoshimoto, Ryuji Narita, and Kingo Itaya 358 Synthesis and Ethylene Polymerization Behavior of a New Titanium Complex Having Two Imine–Phenoxy Chelate Ligands Yasuhiko Suzuki, Norio Kashiwa, and Terunori Fujita 360 Electrochemistry in Middle Phase Microemulsion Composed of Saline and Toluene with Sodium Dodecylsulfate and n-Butanol Shinya Yoshitake, Akihiro Ohira, Masato Tominaga, Taisei Nishimi, Masayo Sakata, Chuichi Hirayama, and Masashi Kunitake 362 Synthesis, Crystal Structure and Superoxide Dismutase (SOD) Activity of Novel SevenCoordinated Manganese(II) Complex with Multidentate Di-Schiff Base Ligands Xing-Mei Ouyang, Bao-Li Fei, Taka-aki Okamura, Wei-Yin Sun, Wen-Xia Tang, and Norikazu Ueyama Copyright Ó 2002 The Chemical Society of Japan Chemistry Letters No.3 2002 364 C-41 Reactions of Silenes Produced Thermally from Pivaloyl- and Adamantoyltris(trimethylsilyl)silane with Bis(trimethylsilyl)butadiyne Akinobu Naka and Mitsuo Ishikawa 366 Application of XANES for the Determination of Oxidation States of Co and Pb in Natural Ferromanganese Nodules Yoshio Takahashi, Akira Usui, Kazu Okumura, Tomoya Uruga, Masaharu Nomura, Mio Murakami, and Hiroshi Shimizu 368 A Novel, One-Pot Synthesis of -C-Cyanohydrazines in the Presence of Lithium Perchlorate/Diethylether Solution (5.0 M) Akbar Heydari, Robabe Baharfar, Mohsen Rezaie, and Saied M. Aslanzadeh 370 Observation of a High Resolution Proton NMR with a 920 MHz Superconducting Magnet Kenjiro Hashi, Tadashi Shimizu, Atsushi Goto, Tsukasa Kiyoshi, Shinji Matsumoto, Hitoshi Wada, Teruaki Fujito, Ken-ichi Hasegawa, Masatoshi Yoshikawa, Takashi Miki, Satoshi Ito, and Mamoru Hamada 372 Fabrication of the Sponge-like Layered Silver(I)-alkylamine Complexes and Their in situ Reduction N. Ren, Y. Tang, Y. J. Wang, A. G. Dong, and W. L. Yang Copyright Ó 2002 The Chemical Society of Japan C-42 374 Chemistry Letters No.3 2002 Preparation of Boron-containing TON-Type Zeolite by Self-transformation of Porous Glass in a Vapor Phase Wei-Yang Dong, Xi-Peng Qiu, Yu Ren, and Ying-Cai Long 376 Water Accelerated Allylation of Aldehydes by Using Water Tolerant Grignard-Type Allylating Agents from Allylmagnesium Chloride and Various Metallic Salts Tomohiro Fukuma, Sandra Lock, Norikazu Miyoshi, and Makoto Wada 378 Solvent Effect on Morphology of Self-assembled Fibrous Materials Derived From an Azopyridine Carboxylic Acid Ken’ichi Aoki, Masaru Nakagawa, Takahiro Seki, and Kunihiro Ichimura 380 Direct Synthesis of Coumarins by Pd(II)Catalyzed Reaction of Alkoxyphenols and Alkynoates Juzo Oyamada, Chengguo Jia, Yuzo Fujiwara, and Tsugio Kitamura 382 Amplification of Detection Signals for Methyl Viologen by Using Supramolecular Formation of Antibody with Viologen Dimer in Surface Plasmon Resonance Sensor Hiroyasu Yamaguchi and Akira Harada Copyright Ó 2002 The Chemical Society of Japan Chemistry Letters No.3 2002 384 C-43 Preparation and Molecular Arrangement of Novel Pyrenophanes Akihiko Tsuge, Yuji Tanba, Tetsuji Moriguchi, and Kazunori Sakata 386 Syntheses of Vinyl Polymers Containing Phenylanthracene Pendants and Their Application ro Organic EL Device Satoshi Shirai and Junji Kido 388 meso-Tetraphenylporphyrin Having Hexamaltosyl and Decyl Chain as an Amphiphilic Photosensitizer toward Photodynamic Therapy Akihisa Hamazawa, Isamu Kinoshita, Brian Breedlove, Kiyoshi Isobe, Minako Shibata, Yasuko Baba, Toyoji Kakuchi, Shiho Hirohara, Makoto Obata, Yuji Mikata, and Shigenobu Yano 390 Novel Activity of SnO2 for Methanol Conversion: Formation of Methane, Carbon Dioxide, and Hydrogen Tohru Mori, Shunichi Hoshino, Arthit Neramittagapong, Jun Kubo, and Yutaka Morikawa 392 Catalytic and Stereoselective Glycosylation with a Novel and Efficient Disarmed Glycosyl Donor: Glycosyl p-Trifluoromethylbenzylthio-p-trifluoromethylphenyl Formimidate Teruaki Mukaiyama, Hiroyuki Chiba, and Setsuo Funasaka Copyright Ó 2002 The Chemical Society of Japan C-44 394 Chemistry Letters No.3 2002 Synthesis and Single Aggregate Spectroscopy of a Novel Fluorescent Dendrimer with Highly Efficient Energy Harvesting Minoru Kobayashi, Shinjiro Machida, Satoshi Takahashi, Kazuyuki Horie, Hiroyuki Yoshikawa, and Hiroshi Masuhara 396 A New Chelation-Assistance Mode for a Ruthenium-Catalyzed Silylation at the C-H Bond in Aromatic Ring with Hydrosilanes Fumitoshi Kakiuchi, Kimitaka Igi, Mitsutaka Matsumoto, Tomoo Hayamizu, Naoto Chatani, and Shinji Murai 398 Non-aqueous Synthesis and Structure of a Novel Monodimensional Zirconium Phosphate: [NH4 ]3 [Zr(OH)2 (PO4 )(HPO4 )] Dan Wang, Ranbo Yu, Takahiro Takei, Nobuhiro Kumada, Nobukazu Kinomura, Ayumu Onda, Koji Kajiyoshi, and Kazumichi Yanagisawa 400 A Novel Host-Guest Supramolecular Architecture of Dehydrocholic Acid in the Enantioselective Inclusion of R-(þ)-Methyl p-Tolyl Sulfoxide Valerio Bertolasi, Olga Bortolini, Giancarlo Fantin, Marco Fogagnolo, and Alessandro Medici 402 Structural Control in Enzymatic Oxidative Polymerization of Phenols with Varying the Solvent and Substituent Nature Naruyoshi Mita, Shin-ichiro Tawaki, Hiroshi Uyama, and Shiro Kobayashi Copyright Ó 2002 The Chemical Society of Japan Chemistry Letters No.3 2002 404 C-45 Morphological Change of Giant Vesicles Triggered by Dehydrocondensation Reaction Katsuto Takakura, Taro Toyota, Koji Yamada, Masako Ishimaru, Kenji Yasuda, and Tadashi Sugawara 406 Coordinatively Unsaturated Ru(II) Species Ru(xantsil)(CO): A New Active Catalyst for Oligomerization/Deoligomerization of HSiMe2 SiMe3 [xantsil ¼ ð9,9Dimethylxanthene-4,5diylÞbisðdimethylsilylÞ]. Isolation of a Stabilized Form of the Silyl(silylene) Intermediates Jim Josephus G. Minglana, Masaaki Okazaki, Hiromi Tobita, and Hiroshi Ogino 408 An Amorphous Nanosized Tin-Zinc Composite Oxide as a High Capacity Anode Material for Lithium Ion Batteries Zhengyong Yuan, Feng Huang, Jutang Sun, and Yunhong Zhou 410 Synthesis of a PET-Clay Hybrid Material Zhang Guozhen, Tetsuya Shichi, Tong Zhiwei, and Katsuhiko Takagi 412 High Temperature PTC Thermistor Using Ba Cobaltite Kazuya Kinoshita, Hajime Kusaba, Go Sakai, Kengo Shimanoe, Norio Miura, and Noboru Yamazoe Copyright Ó 2002 The Chemical Society of Japan C-46 414 Chemistry Letters No.3 2002 Oxidative Double Bond Cleavage of -Substituted Styrenes with Molecular Oxygen Yujiro Hayashi, Mitsuhiro Takeda, Miyamoto, and Mitsuru Shoji 416 Yuji Modulation of the Copper-Dioxygen Reactivity by Stereochemical Effect of Tetradentate Tripodal Ligands Hideki Hayashi, Kounosuke Uozumi, Shuhei Fujinami, Shigenori Nagatomo, Kazushi Shiren, Hideki Furutachi, Masatatsu Suzuki, Akira Uehara, and Teizo Kitagawa 418 A Highly Selective and Coking-Resistant Catalyst for Methane Dehydrocondensation Yuying Shu, Ryuichiro Ohnishi, and Masaru Ichikawa 420 Photoinduced Changes of Surface and Adsorbed Water in TiO2 Photocatalytic Systems as Studied by Solid State 1 H-NMR Spectroscopy Atsuko Y. Nosaka, Toshimichi Fujiwara, Hiromasa Yagi, Hideo Akutsu and Yoshio Nosaka Copyright Ó 2002 The Chemical Society of Japan