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Director of the Far East Geological Institute Academician Alexander I. Khanchuk Professor (Geology and Mineralogy) Tel: +7-4232-318750, +7-4232-318520 E-mail: [email protected] The current Director of the Far East Geological Institute is Academician Alexander I. Khanchuk. Alexander I. Khanchuk is recognized as a world expert in geodynamics, petrology, and mineralogy and focuses on reconstruction of geodynamic environments of Earth’s crust evolution in ocean-continent transition zone. In addition, Academician Khanchuk is a recognized authority in fundamental and applied problems of the Pacific margins geology. The Russian Far East is a territory where young geological structures extend from Asian continent to the Pacific Ocean. This relatively small region hosts different magmatic rocks and sedimentary rocks of all geological ages. Among the deposits operated in this area, those are the deposits of flour spar, boron, lead, zinc, tungsten, and other minerals generated by a diverse geological structure, there are the deposits whose reserve ranks the largest in the world. In this view, scientific activity of the Far East Geological Institute integrates fundamental and applied research of Eastern Asia and the adjacent Pacific basin geology, and coordination of all related investigations carried out at the Russian Academy of Sciences, institutions of the Ministry of Natural Resources of the Russian Federation, and other agencies. We believe that this booklet will manage to demonstrate the extensive geography of scientific interests application, diversity and specificity of research objects, and high level of investigations carried out by scientists and engineers working at the Far Eastern Geological Institute of Russian Academy of Sciences. Ekaterina A. Radkevich Valentin G. Moiseenko Aleksey D. Scheglov Ivan Ya. Nekrasov issues of geology, geochemistry, engineering geology, and geoecology of the Russian Far East. The Geological Institute’s basic scientific activities fall into three main research areas: • geology, lithosphere dynamics, magmatism and metamorphism within the Earth's crust, and studies of the mantle ocean-continent transition zone evolution; • metallogeny of typical geodynamic environments; • environmental geology, interaction between the atmosphere, hydrosphere, lithosphere, and biosphere in modern geoecological systems. The Senior Administrative Officers of the Far East Geological Institute, Far East Branch of the Russian Academy of Science (FEGI FEB RAS), with contact information, are listed below. Personnel The USSR Academy of Sciences established the Far East Geological Institute on September 4, 1959 within the Far East Branch of the Siberian Division of the USSR Academy of Sciences. The Far East Geological Institute (FEGI) is situated in the vicinity of Amursky Bay, in a wooded suburb north of Vladivostok. The Institute includes seventeen research laboratories and a museum. Recently an Analytical Center was created, furnished with up-to-date precision apparatus and sophisticated equipment. The Analytical Center conducts the full range of analytical investigations of rocks and minerals, including the delineation of light isotopes and rare earth elements. The Institute’s first Director was Ekaterina Alexandrovna Radkevich who was a Corresponding Member of the USSR Academy of Sciences, and a Hero of Socialist Labor. Director Radkevich is recognized for her decisive role in organizing and developing FEGI’s basic research. Throughout its history the Institute has been headed by renowned scientists, including Academicians V.G. Moiseenko and A.D. Scheglov, and Corresponding Member of the Russian Academy of Sciences I.Ya. Nekrasov. FEGI is a comprehensive, wide-ranging geological research institution equipped with up-to-date laboratories where scientists research the most difficult and complex The Institute employs nearly three hundred people, of whom one hundred nineteen are scientists. The staff includes one Academician, one Corresponding Member of the Russian Academy of Sciences, twenty-six Professors, and fifty-six Doctors. Three members of the staff have been granted the honorary title “Honored Worker of Russian Federation Science” and two were granted the honorary title “Honorary Geologist of the Russian Soviet Federative Socialist Republic”. The former building of the Geological Institute –– Deputy Director for scientific research Professor Oleg V. Chudaev Tel: +7-4232-318327 E-mail: [email protected] Deputy Director for scientific research Dr. Alexander V. Ignatiev Tel: +7-4232-318737 E-mail: [email protected] Scientific Secretary Dr. Natalya A. Kharitonova Tel: +7-4232-318520 E-mail: [email protected] Deputy Director for general management Sergey G. Chugainov Tel: +7-4232-318271 E-mail: [email protected] Deputy Director for Overhaul and Repair Alexander T. Lopatnikov Tel: +7-4232-317556 E-mail: [email protected] Associate Director for International Relations Elena E. Khanchuk Tel: +7-4232-317591 E-mail: [email protected] Chief Accountant Svetlana A. Stepanyuk Tel: +7-4232-321240 E-mail: [email protected] –– –– Postgraduate students FEGI FEB RAS has a successful education program for postgraduate students. Presently eighteen postgraduate students are working in ten major areas of study: • general and regional geology; • paleontology and stratigraphy; • geotectonic and geodynamics; • petrology, volcanology; • mineralogy, crystallography; • lithology; • geochemistry, geochemical methods of mineral deposit prospecting; • geology, solid minerals prospecting, minerogeny; • geoinformatics; • environmental geology. Dissertation Council The Institute has a vigorous, functional Scientific Council that awards scientific degrees in several disciplines: • general and regional geology; • petrology, volcanology; • geology, solid minerals prospecting, minerogeny. The Council consists of twenty-two renowned scientists all of whom are Professors. One member of the Council is Academician and one is a Corresponding Member of the Russian Academy of Science. The Institute’s scientific relations Cooperation with Universities and colleges in the Russian Far East Institute scientists work in close collaboration with local universities and colleges including the Far Eastern State University, the Far Eastern State Technical University, and the Vladivostok State University of Economy and Service. In addition, FEGI scientists periodically present lectures in colleges and universities of the Russian Far East. FEGI scientists supervise student scientific coursework, field work, and appraise final papers as part of the federal program, “Integration of Russian Science and Higher Education (2002-2006)”. In some cases, postgraduate students who attend the Far Eastern State Technical University (FESTU) will be hired on a part-time basis to work in FEGI research units. FESTU students enrolled in the Institute of Engineering and Social Geology, who are working towards Doctorate degrees in Geology and Ecology Department, are also eligible to be hired on a part-time basis. The Institute maintains strong scientific relations with other geological organizations in the Russian Federation and in other countries, including: Australia, Mongolia, the United Kingdom, Germany, Canada, China, South Korea, United States of America, Vietnam, India, Mexico, and Japan. The Far East Geological Institute is celebrated for its participation in many cooperative projects including undertakings sponsored by the Russian Foundation for Basic Research (RFFI), the International Association for the promotion of cooperation with scientists from the New Independent States (NIS) of the former Soviet Union (INTAS), as well as UNESCO. Recent joint projects include deep-water oceanic drilling, mineral resource surveys, metallogenesis studies, and tectonics research in North-East Asia. The Far East Geological Institute is an integral component of the Russian Academy of Sciences and is committed to achieving the goals of the Academy. The present building of the Far East Geological Institute –– Laboratory of Regional Geology and Tectonics Research Staff: Vladimir V. Golozubov, Prof., Head of Laboratory; Valentin P. Utkin, Prof., Chief Researcher (Honored Science Worker); Vladimir P. Simanenko, Dr., Leading Researcher; Boris I. Pavlutkin, Dr., Leading Researcher; Anatoly N. Philippov, Dr., Leading Researcher; Alexander I. Malinovsky, Dr., Leading Researcher; Georgy I. Govorov, Dr., Senior Researcher; Alexander N. Mitrokhin, Dr., Senior Researcher; Peter L. Nevolin, Dr., Senior Researcher; Sergei A. Kasatkin, Researcher. Technical Staff: Polina D. Gassanova, Leading Engineer; Olga M. Molibog, Leading Engineer; Tatiana M. Mikhailik, Programmer; Irina V. Smirnova, Senior Lab Technician; Tamara I. Karpenko, Technician. Contacts: Tel: +7-4232-317823 E-mail: [email protected], [email protected] Major research directions and results Since the Institute was organized, the laboratory has been working on the tectonics and metallogenic mapping of the Pacific Mobile Belt. Later investigations were concentrated on solving the problems of Pre-Cambrian geology, and since 1981, research emphasis has been on the younger Phanerozoic complexes forming the basement of the Pacific active margins. Before the Far East Geological Institute was founded in 1959, the Department of Regional Geology had been a part of the Far East Branche of the Siberian Division of the USSR Academy of Sciences and then as a member of the Institute was transformed into the Laboratory of Tectonics. The founding fathers of the laboratory were professors M.G. Organov, N.P. Vasil’kovsky (the first Head of the laboratory), A.M. Smirnov, G.M. Vlasov, V.I. Shul’diner, and G.S. Gnibidenko. For years (from 1966 to 1981) an ideological inspirer and leader of the laboratory was A.M. Smirnov. In the 1980s, when A.I. Khanchuk took charge of the laboratory, the tectonics of the Far East as a whole and of the Sikhote-Alin Mountains, in particular, was revised in the context of the lithosphere plate tectonics that gave impetus to the development of new ideas and interpretations on the tectonic history of these regions. These territories have been recognized to be a collage of terranes that differ in the history of their development and that were accreted to the eastern margin of Asia during the Upper Paleozoic, Mesozoic, and Cenozoic. We have first shown that the chaotic complexes with blocks and plates of the rocks of oceanic origin are the fragments of the Mesozoic accretionary prisms formed over the subduction zones. Deciphering the structure and development of the eastern margin of Asia in the Mesozoic-Cenozoic time has defined the episodes of predominance of the subduction regime and the transform margin setting. Vladimir V. Golozubov –– these slidings were important in the formation of orogenic belts and newly formed continental lithosphere (Golozubov, 2006; Khanchuk, Golozubov, 2008). 3. Study of the role of the geodynamic strike-slip faulting regime in the tectogenesis, magmatism, and metallogeny of the Asia eastern margin. The scientific problem was first posed by V.P. Utkin in the late 1970s while on a searching-surveying expedition for the Primorgeologiya Company. From 1981 the investigations were continued at the Laboratory of Geodynamics and Magma- and Orecontrolling Structures that was established by V.P. Utkin at the Far East Geological Institute of the FEB RAS, and since 2007 – at the Laboratory of Regional Geology and Tectonics. At different times, B.K. Sorokin, I.A. Shagvaliev, Yu.P. Yushmanov, P.L. Nevolin, A.N. Mitrokhin, S.A. Kasatkin, and others participated in the investigations. The most significant results of the work: • We have first recognized that in the Mesozoic-Ceno zoic time the Asia eastern margin was developed under the conditions of the strike-slip fault geodynamic regime controlled by the development of the East-Asia Global Strike-Slip Fault Zone (GSSFZ) with paragenetic formation of the structures of shear (system of the NE left-lateral faults), compression (imbricated-folded system), and extension (different scale pull-apart faults of the crust). The syn-strike-slip-fault destruction of the Eastern margin of Asia plays a specific role in the processes of magmatism, metallogeny, and formation of the Cretaceous-Cenozoic sedimentary basins superposed on the protostructures. Three main destructive stages without clear boundaries of their onset and completion are distinguished: 1 – Late Cretaceous (formation of volcanoplutonic belts and metallogenic provinces genetically related with them), 2 – Late Cretaceous-Paleogene (formation of the graben belts – epicontinental sedimentary basins), 3 – PaleogeneNeogene (formation of the belt of marginal seas and, first of all, deep-sea basins not supplied with sediments). The stages successively grading into each other reflect the evolutional development of the continental margin under the conditions of dominance of the left-fault geodynamic regime (Utkin, 1978, 1985, 1989, 1993, and others). Geodynamic evolution of the eastern margin of Asia from Middle Jurassic to Early Cretaceouse If the indicator complexes for recognizing the subduction regime have long been established and agreed by the scientific community, transform margin regime in the geological past remained unrevealed. The laboratory has developed this new direction in paleodynamics research, as elaborated by the work of Academician A.I. Khanchuk, Prof. V.V. Golozubov, and Dr. V.P. Simanenko. On the geodynamic reconstructions available, including the recent ones, the transform plate boundaries are simply not shown – even on the areas where the plates are sliding at an acute (less than 30o) angle or in parallel to the margins of the continental plates. On the schemes, the subduction boundaries are marked. The investigations are carred out in the following directions: 1. Elaboration of criteria for recognizing the transform margin regime in the structures of the geological past. The transform margin is characterized (Khanchuk et al., 1997; Golozubov, 2006) by: • Within the GSSFZ in the Sikhote-Alin, the NNE system of the extended fault zones controlling the distribution of ore deposits has been revealed. The hierarchic roll of the structures of strike-slip fault nature controlling the ore districts, deposits, and isolated ore bodies has been established. We have first argued an idea, according to which the available lateral (from west to east) magmatic and metallogenic zoning is vertical (upwards) based on temperature and geochronological zoning. It is demonstrated by an oblique truncation of the East-Sikhote-Alin volcano-plutonic belt submerged to the east (Utkin, 1976, 1986, 1989, 2005). a) the availability of the fault zones, active at the considered length of time, along the plate boundaries with displacements for hundreds and thousands of kilometers. b) the formation of pull-apart basins that were filled with terrigenous and volcanic material in the continental margin and with avalanche sediments near the continent on the oceanic basement. c) the manifestations of volcanism with mixed subduction and intraplate characteristics that are restricted to the pull-apart basins and are irregularly distributed along the margins. • In the Primorsky sector of the GSSFZ, the recognition of the azimuthal annexations of structural planes allowed the conclusion about a periodical change of the lateral compression of the crust: 1) in the Proterozoic time – meridional; 2) at the Proterozoic-Mesozoic boundary, 2. Study of the processes that took place under the conditions of transform sliding of the plate showed that –– • The wrench-fault rifting-graben nature of the Jurassic-Early Cretaceous sedimentary basins of South-East Russia, with possible participation of the mantle convective currents and plume diapirism, has been justified. The wrench-fault displacements of crust blocks along the subhorizontal surfaces occurred without frontal subduction and obduction, so this process was called rectaduction (lat. Recta – straight; ductus – conducting) (Utkin, 1996, 1997, 1999). meridional compression was changed for a latitudinal one; 3) at the Paleozoic-Mesozoic boundary, latitudinal compression was again changed for almost meridional one. In our opinion, change of the compression vectors was governed by the change of the lateral displacement directions, first of all, the Asian continent (Utkin, Nevolin, Mitrokhin, 2003, 2007; Utkin, 2008). • We have first established the critical role of the activization of deep faults of the oceanic lithosphere in the formation of the transvolcanic belts of the Pacific Ocean. The geodynamic conditions of their development have been justified (Utkin, 2006). • The rotation model of the tectogenesis, transformation of geodynamic regimes of the continental margins, and disintegration of the Laurasia and Gondwana supercontinents has been elaborated. The global processes resulted from the combined effect of the steadily oriented meridional pole-running and latitudinal inertial forces whose vector was periodically changed depending on the acceleration or deceleration of the Earth rotation (Utkin, 1979, 2007). Rotation model of GSSFZ formation (I-IV) and transformation of geodynamic regimes of the continental margins 4. Analysis of the influence of fault displacements on the formation and filling of the intracontinental and margin-continental Cretaceous and Cenozoic sedimentary basins. It has been established that these basins are the structures of extension on the joints, curvatures, or branching of the fault zones (Golozubov, 2006; Golozubov et al., 2007). 5. Study of the geochemistry of volcanites of the transform margins on the material of the north-west margins of the Pacific Ocean. The laboratory is actively working on this problem today. There is evidence that the volcanites of the transform margins show the geochemical characteristics of both subduction and intraplate sources (Simanenko et al., 2002). East-Asian Global Strike-Slip Fault Zone (GSSFZ). Fault parageneses: 1 – structures of shear, 2 – compression, 3 – extension –– • Formations of the West Sikhote-Alin have been distinguished and described (Philippov, 1990). • The initial sections of the sedimentary cover of the oceanic plates of the Paleopacific have been reconstructed and the settings and some events of sedimentation in the ancient oceanic basin have been established (Philippov, 2003, 2005, 2007). • In the Lower Amur region of Khabarovsky Krai, a full section of the Early Cretaceous ensimatic island-arc system has been established. We have reconstructed the paleogeographic and paleogeodynamic settings of sedimentation and mechanisms of formation of this geological structure (Markevich et al., 1997). • We have carried out the sedimentological investigations of the volcanogenic-sedimentary formations of the Early Cretaceous Moneron-Samarga ensialic volcanic arc of the East Sikhote-Alin. We have determined the structure and composition of the formations and the setting of their accumulation – at the foot of the island slope in the back arc part associated with basaltic volcanism (Malinovsky et al., 2002, 2008). Formation of Nizhnebikinsky basin within extension zone on a place of a double bending of Alchan right-lateral strike-slip fault The results of the investigations of the laboratory workers in the listed above directions have been published in monographs and articles in the domestic and foreign journals and thematic collections. A list of publications is given on the Institute’s web-site www.fegi.ru. 6. Features of the Phanerozoic sedimentation in the interaction of the Eurasia continent with the Pacific Ocean as well as the structure and composition of feeding sources of the different-type sedimentary basins were studied at the specialized Laboratory of Sedimentary Geology that was headed for many years by P.V. Markevich and then, in 2004, was incorporated into the Laboratory of Regional Geology and Tectonics at the Institute. Sedimentological research has been carried out in the Sikhote-Alin, Sakhalin, and Koryak-Kamchatka regions as well as in other districts of the Far East. In addition, the laboratory scientists participated in the marine expeditions in the Pacific Ocean and its marginal seas. The principal results of the investigations in this field are as follows: • The terrigenous and volcano-terrigenous flysch formations of the Sikhote-Alin and Kamchatka, composed for the most part of gravitation formations, have been studied (Markevich, 1970, 1985). • We have established two types of the Phanerozoic complexes in the interface of Eurasia and the Pacific Ocean: arkose – in the outer zone of the Pacific fold belt and greywacke – in the inner zone. Greywacke complexes can not transform into arkose ones nor immature oceanic crust – into mature continental granite-metamorphic one (Markevich et al., 1987). Chondrite-normalized REE patern for basaltic and andesitic rocks of Far East Sikhote Alin volcanic belt • The structure, facies and material composition, tectonic position, and settings of accumulation of molasses of the Olyutorsky terrane of Kamchatka have been studied (Malinovsky, 1992). –– Laboratory of Stratigraphy Research Staff: Igor V. Kemkin, Prof., Head of Laboratory Yury D. Zakharov, Prof., Chief Researcher Galina I. Buryi, Dr., Leading Researcher Alexander M. Popov, Dr., Senior Researcher Vladimir D. Khudik, Dr., Senior Researcher Tatyana A. Punina, Dr., Senior Researcher Olga P. Smyshlyaeva, Dr., Researcher Liana G. Bondarenko, Researcher Ekaterina N. Gaplikova, Masters Course Student Technical Staff: Lidia I. Sokur, Engineer Yana V. Losiva, Engineer Contacts: Tel: +7-4232- 317132 E-mail: [email protected] Major research directions Results The Laboratory of Stratigraphy investigates problems in paleontology, biostratigraphy, isotope biogeochemistry, paleobiogeography, and regional geology. In recent years, the laboratory has carried out the following projects: 1. Lithological-biostratigraphic study with application of radiolarian analysis helped to reveal the true structure of ancient accretionary prisms of Sikhote-Alin. Prof. Igor V. Kemkin determined that these ancient prisms, having complex tectonic structure, are composed of multiple tectonic-sedimentary complexes of different age (similar to a “multi-layered cake”). The “layers” represent regularly repeated and strongly dislocated (asymmetrically folded and multiply duplexed) fragments of the initial section of sedimentary cover made of different-age (i.e. differently remote from a spreading center) sectors of pale-oceanic plate. Each complex is composed of oceanic rocks (pelagic flints, limestone associated with basic volcanic rocks) gradually replaced by terrigene deposits (sandy schist strata and chaotic formations). Complexes differ in time of accretion and age of paleoceanic fragments, with the most ancient pale-oceanic formations and overlapping terrigene rocks making the upper structural levels of prisms, and the youngest rocks – the lowest (inversion type of section) levels. This results from a concessive accretion of pale-oceanic formations to a continent margin. • The laboratory has completed a description of a group of invertebrates and plants of Paleozoic, Mesozoic and Cenozoic deposits in the Far East. These descriptions serve as a foundation of biostratigraphical scales of Cambrian, Ordovician, Devonian, Permian, Triassic, Jurassic, Cretaceous and Neogenic periods, as well allow for paleobiogeographical and paleoclimatical reconstructions. • Based on new paleontological data, the laboratory constructed a description of typical cross-sections of the Lower Triassic strata in South Primorye. • The laboratory analyses assisted in understanding of the geomorphologic structure of the Fedorov guyot (Magellan Mountains, the Pacific Ocean), based on an analysis of fauna (bivalves and snails) from sedimentary rocks. This permitted researchers to determine the lithological and paleontological characters of rockforming complexes from the Early Cretaceous to Pleistocene, inclusive. 2. Scientists of the laboratory have described the first complete print cast of eukonodont, found in Russia by A.V. Zhuravlev in 1997 in Low Carboni-ferous deposits of the Near-Polar Urals (Korzhim River). Judging by its dimensions (length – about 4.8 mm; width near head – 0.4 mm, and 0.25 mm – closer to the tail) it was not a sexually mature animal, and the body was slightly deformed vertically and horizontally due to burring. The print reveals three segments: head, body, and tail, with the head poorly differentiated from the body. It also contains pair H-elements or rounded skeleton fasten plates. The body part contains 37 transversal muscular segments mostly perpendicular to the eukonodont animal’s body axis. The tip of the tail hosts long beams located on both sides of the anus, which are characteristic of all eukonodont animals. Several more imprints of young eukonodont animals have been found for the first time, all different in Igor V. Kemkin – 10 – Santonian – Maastrichtian ammonites from the Bystrinskaya suite (the eastern shore of the Penzhinskaya Inlet, Koryak Plateau, Kamchatka) Late Permian fern (the Pil’nikov Stream, Southern Primo- size, orientation, and conservation quality. Behind the terminal end of the described animal a head of other animal, the younger one, was also found. Detailed examination suggests the body of the younger animal curves and transits in another plane. Finding of first in Russia eukonodont animals in Low Carboniferous deposits of Kozhim River (Near-Polar Urals) has enriched the world collection of unique soft tissue prints of these extinct and still mysterious animals, which were related to many groups of fauna (Buryi and others, 2007). 4. The first investigation and description of a unique collection of bivalve mollusks and gastropods from the sediments dredged on the guyots of Magellan Rise (Pacific Ocean), during geologic-geophysical cruises of 2000-2008, was undertaken by Dr. V.D. Khudik who established 49 taxons of 27 genuses of bivalve mollusks and gastropods in the basin of guyots Alba, Govorov, Fedorov, Il’ichev, Kotsebu, Gelendzhik and Butakov, dated to be of Cretaceous-Miocene age. The study of sedimentary fauna helped to distinguish “transgressive” Cenomanian-Turonian, Late Campanian-Maastrichtian, Late Paleocene-Middle Eocene, and Late Cenozoic phases of guyots evolution. Paleoecological study of Paleogene mollusks, as well as corrals and foraminifera, provided additional reasons for the existence of relative shallowwater conditions in the area of guyots in Early Paleocene time. 3. Late Cretaceous cephalopods (belemnites and ammonoids) reported from the Govorov, Il’ichev, Kotsebu, Fedorov, Gelendzhik and Butakov guyots, Magellan Rise, were isotopicaly investigated and described for the first time. In addition, belemnites from Govorov, Gelendzhik and Butakov guyots have been described for the first time, including 80 samples from the Gelendzhik Guyot, tropical Paleopacific. Detailed isotope measurements were undertaken for successive growth portions of samples from the Late Campanian?-Maastrichtian belemnite Belemnitella? sp. rostrum. The values of δ18O and δ13C in the analyzed material fluctuate from -0.4 to +0.8‰ and from +0.1 to +3.1‰, respectively. Judging from the data obtained, the lowest paleotemperature calculated from the Belemnitella? sp. rostrum is 9.0 oC, the highest is 13.6 oC. Other paleotemperatures for the Magellan Rise were obtained from 11 Late Campanian-Maastrichtian Dimitobelidae gen. et sp. nov. rostra (15.3-17.1 oC) of the Govorov Guyot and a Dimitobelus? sp. rostrum (10.9 oC) of the Butakov Guyot. New oxygen isotopic proxies are consistent with the hypothesis suggesting a considerable vertical range of belemnites migration in seawater column. In view of new facts, bottom waters of the tropical Pacific (Southern hemisphere) were probably produced by sinking of surface waters in the polar region. The possible signs of Late Campanian?-Maastrichtian seasonal temperature fluctuation were fixed for the Belemnitella? sp. rostrum from the Gelendzhik Guyot, and very likely reflect some surface seasonal conditions in the southern polar regions in general. This interpretation suggests that the latest Cretaceous deep-ocean temperatures in the Magellan Rise area were possibly as warm as 9 to10.2 oC for the southern winter, >11.3-11.7 oC for the southern summer, with a mean annual temperature (MAT) of >11oC (Zakharov et al., 2007a,b). These results have added considerable detail to the known geological structure and geomorphological characteristics of the described guyots, and helped to determine matter and paleontological characteristics of rock complex structure from the Early Cretaceous to the Pleistocene. The obtained data describe an extensive evolution stage of malacofaunas of the Pacific Ocean near equator and detail the geological history of the Magellan Rise basin in the Late Cretaceous and Cenozoic. Rastellum (Arctostrea) zeilleri (Bayle, 1878) – 11 – Laboratory of Cenozoic Stratigraphy Research Staff: Vladimir S. Pushkar, Prof., Head of Laboratory Yury A. Mikishin, Dr., Senior Researcher Irina G. Gvozdeva, Researcher Tatyana I. Petrenko, Researcher Olesya Yu. Likhacheva, Junior Researcher Vladimir N. Shamraev, Postgraduate Student Ekaterina Elbakidze, Postgraduate Student Technical Staff: Aleksandra V. Rudenko, Laboratory Technician Contacts: Tel: +7-4232-318750 E-mail: [email protected] [email protected] Major research directions • how frequent and how quick such changes occur in spatial-temporary coordinates and how this knowledge can be used for designing high-resolution stratigraphic schemes and climate changes prediction. The laboratory studies the Cenozoic evolution of natural environments in Eastern Asia and the Northern Pacific. Research directions include the formation of Cenozoic strata, changes in the regional and global paleoclimate of the junction zone of the largest continent, Eurasia, and the largest ocean, the Pacific. In addition, the laboratory studies the comparative characteristics of paleogeographic environments of deposit formation in contrasting climatic zones. Results Stratigraphy and paleogeography results of the laboratory were used in the state programs to produce large-scale geologic maps of the Sea of Japan (Dalmorgeologia) and Sea of Okhotsk (SakhInzhGeologia) shelves. • The laboratory has obtained new data on stratigraphy and paleogeographic history of continental border and marginal seas. These data will assist in resolving various challenges related to the creation of more detailed stratigraphic schemes. Reconstruction of environmental changes, including global climate fluctuations, is based on understanding the nature of co-evolutional interactions between the biological and geological events of the Cenozoic. In this connection, to find answers on the following questions is of primary importance: • The laboratory worked out a super detailed zonal scale for diatoms of the North Pacific. • what are the causes that led to changes in paleocommunities of microorganisms and how the formers can resist and adapt to the environmental changes. • what accounts for taxonomic and ecological variabili ty, frequency of species diversity and paleoproductivity, as well as variation of intra- and infraspecific interactions. • The laboratory has specified the genesis and age of the Golovnin formation in Kunasir Island, the Marumyan Formation in Sakhalin Island, the Novokachalinsk, and the Ust-Suyfun and Suyfun Formations in the southern part of the Russian Far East. Vladimir S. Pushkar Aulacoseira praegranulata var. praeisslanica (Jouse) Moiss – 12 – Zonal scale of Pliocene-Pleistocene deposits of North Pacific (NPDZ) Neogene diatom zonal scale of Primorye (Far East of Russia) – 13 – Laboratory of Oceanic Lithogenesis and Ore Formation Research Staff: Oleg V. Chudaev, Prof., Head of Laboratory Yuri G. Volokhin, Dr., Leading Researcher Leonid B. Hershberg, Dr., Leading Researcher (Honored Geologist of Russian Federation) Eugene V. Mikhailik, Dr., Leading Researcher George A. Chelnokov, Dr., Senior Researcher Pavel E. Mikhailik, Junior Researcher Ivan V. Bragin, Junior Researcher Elena A. Vakh, Postgraduate Student Technical Staff: Natalia V. Gruda, Leading engineer Svetlana V. Mikhailova, Technician Contacts: Tel: +7-4232-318327 E-mail: [email protected] Major research directions In high pCO2 cold mineral waters of Sikhote-Alin, magmatic CO2 makes shallow ground waters slightly acid and more aggressive to the surrounding rocks. Chemical composition of these waters depends on pressure of CO2, residence time and composition of host rocks. Oxygen and hydrogen isotopes data indicate that the water of the studied high and low temperature hydrothermal systems is the most meteoric. The Laboratory of Oceanic Lithogenesis and Ore Formation studies the geochemistry of modern hydrothermal systems in the transition zone from the Asia continent to the Pacific Ocean; stratigraphy, petrology and geochemistry of Early Mesozoic siliceous formations in the Sikhote-Alin; ferromanganese crusts and nodules of the Pacific Ocean and marginal seas. Results • For the first time the detailed correlation scheme of Triassic siliceous formation of Sikhote-Alin based on biostratigraphic conodont zoning has been developed. The scheme reveals the main features of facies and the cyclical structure of the formation. • The study of high temperature hydrothermal systems of the Kuril Island arc and Kamchatka showed that the water composition of both systems is conditioned by reworking of surrounding host rocks and deep-source chemical elements from magmatic chambers. Chemical composition of water in hydrothermal systems with low temperature greatly depends on water-rock interaction. In some cases gases of deep origin may occur and mix with shallow ground water. 1 – sodium-chloride waters; 2 – sulphate waters; 3 – surface waters; 4 – atmospheric precipitations (Kuril Islands); 5 – Sea of Okhotsk. Oxygen-hydrogen isotopic ratio, high temperature waters of the Kuril Islands volcanoes Oleg V. Chudaev – 14 – Hot springs with ultra sulphate waters of the Mendeleev Volcano (Kuril Islands) Native sulphur of the Ebeko Volcano (Kuril Islands) • A detailed geological study of Alba, Fedorov and Gramberg guyots (Magellan Mountains) showed that the cobalt manganese crusts on apical subhorizontal surfaces, looking like narrow ribbon bodies, were confined to relief scars. The formation of these crusts is associated with the Taylor-Hogg topographic eddies (TE) above the guyots. The mechanism of topographic eddies provides a satisfactory explanation for continuous long-term evolution of cobalt manganese crusts forming at the same place. This TE mechanism also accounts for an asymmetrical structure and composition of the described crusts, as well as for deposition of convex lenses of carbonaceous silts in the center of flat tops. 1 – cobalt manganese crusts; 2 – carbonaceous sediments of flat tops; 3 – guyot brow; 4 – the Taylor-Hogg topographic eddy; 5 – directions and intensity (depends on arrow thickness) of top currents; 6 – directions and intensity (depends on arrow thickness) slope currents; 7 – currents along isotherms, isohalines, isopicnic lines and other see water parameters. Dashed-lines demonstrate backside currents. Helium-neon isotopic ratio, thermal waters of the Kuril Islands volcanoes A model of Taylor-Hogg topographic eddy over the Magellan Mountains guyots – 15 – Laboratory of Gemmology Research Staff: Vera A. Pakhomova, Dr., Head of Laboratory Boris L. Zalishchak, Dr., Leading Researcher Vitaliya B. Tishkina, Dr., Junior Researcher Ella G. Odarichenko, Dr., Researcher Olga A. Karas, Postgraduate Student Yulia A. Shabanova, Postgraduate Student Svetlana Y. Buravleva, Postgraduate Student Vladimir A. Kamynin, Laboratory Assistant Dmitriy G. Fedoseev, Laboratory Assistant Technical Staff: Sergey Yu. Zharchenko, Technician Yury S. Chikharev, Technician Contacts: Tel: +7-4232- 317604 E-mail: [email protected] Major research directions The laboratory tries to maintain contacts with gemologists abroad. International links with scientists from Australia (Dr. Grahame Brown and Dr. Lin Sutherland), the United States (Gemological Institute of America) and Thailand (Asian Institute of Gemological Sciences) help the laboratory researchers to take part in international conferences, to stay abreast of state-of-the-art methods of analysis and to publish in the international gemologyoriented journals. • Geology, mineralogy and geochemistry of precious stone deposits. • Genesis and composition of minerals. • Study of minerals and mineral associations of magmatic rocks, primarily granitoids, including alkaline and alkaline-granite rocks, pegmatite, skarns and greisens. • Relationships between the genetic processes of semi-precious stone deposits and ores in terms of different geodynamic settings of the Sikhote-Alin Ridge. • Scientific aspects on the distribution, formation and prediction of precious stone occurrences and deposits. • Development and application of instrumental techniques for diagnosis, analysis and evaluation of minerals, aggregates, inclusions and structure of mineral raw materials (natural, synthetic or organic). • Applied gemology for consultants or contractors, including: lectures on the history and culture of precious stones and on methods to examine and evaluate gems and jewelry. The exchange of gemology expertise with the neighboring countries of the Asia-Pacific Region can be very useful for the comparative study of the gemological objects of Russia and foreign countries; for developing better methods of studying gemstones and gem material and for developing innovative technologies for upgrading the precious stones of Russia and the Russian Far East. Fluid inclusion in quartz of crystal-bearing pegmatites, the Verkhne-Shibanovskoye deposit Vera A. Pakhomova – 16 – Noble opals from Raduzhnoe Deposit, Primorye Corundums from placer deposit, Western Sikhote-Alin Results • The laboratory has discovered new shows of corundum (sapphires and garnets) and rare earth (RE) mineralization within the Sikhote-Alin. Comparative study of characteristic distribution and conditions of formation of the precious stone deposits and RE minerals in different ore complexes of Sikhote-Alin showed that formation controlling factors were contact syenitization, as the alka lizing process, in the presence of limestone- and high aluminiferous strata. and from the Raduzhnoe deposit of Primorye. Study of the opal structure confirmed that there is a direct relation between the diffracted light beam wave length and globules size. It is known that the color of opalescence is in close relation with the light beam wave length. For more than half a century, precious opals have been successively synthesized in different countries all around the world since the discovery of the opalescence. The laboratory has defined a group of admixture elements “responsible” for the precious opal color, with Fe, Mn, Ti, and Ni being the main responders. Strongly colored opals are characterized by maximum content of Fe. According to the electron paramagnetic resonance (EPR) data, yellow-, brown- and red-colored opals have Fe3+, while those with different tints of green have Fe2+. • The laboratory has summarized the results of longterm studies of the geology, ore mineralization and gene sis of the zoning of alkaline ultrabasic complexes found in the southern part of the Russian Far East. • The laboratory studied opals from the Raduzhnoe deposit. Researchers investigated the composition, physical and optical properties of opal from this deposit and compared its gemological characteristics with Mexican and Australian minerals. According to petrochemical characteristics, structure position and thermobarogeochemistry, opal mineralization is related to andesitic volcanism of the California-type transform margin. The origin of the opal is a result of filling fractures in andesites with a metasomatic silica colloid solution (maximum temperature – 160° C, with increasing alkalinity from pH 7.5 to 9.5). • The laboratory studied and has determined physical and chemical parameters of the formation of boron minerals (datolite, danburite and axinite) from the Dal’negork borosilicate deposit, minerals of crystal-bearing pegmatite and syenite from the Upper-Shibanovkoye Deposit (smoky quartz, cassiterite, beryl and REE: monazite, xenotime, deliite, cheralite and brabantite) and topazes from the Zabytoe deposit. The precious stones of those deposits have been also thoroughly investigated for gemological characteristics inclusive of their estimated value in jewelry. • The laboratory has performed a comparative study of ordinary and precious opals from Australia opal deposits Ilvaite with pseudohexagonal crystal of prase grew above. Dal’negorsk, Primorye NIKON E-600 POL Optical Microscope for Geological Studies, Jeol (Japan) – 17 – Laboratory of Metamorphic and Metasomatic Formations Research Staff: Oleg V. Avchenko, Prof., Head of Laboratory; Valentin O. Khudolozhkin, Dr., Leading Researcher; Rostislav A. Oktyabrsky, Dr., Leading Researcher; Mikhail A. Mishkin, Prof., Senior Researcher; Igor A. Tararin, Prof., Senior Researcher; Galina A. Valuy, Prof., Senior Researcher; Alexander M. Lennikov, Prof., Senior Researcher; Ziniyat G. Badredinov, Dr., Senior Researcher; Sergei N. Lavrik, Dr., Senior Researcher; Alexander N. Solyanik, Dr., Senior Researcher; Oksana I. Sharova, Junior Researcher; Elena Yu. Moskalenko, Junior Researcher; Vera L. Ivanova, Dr., Researcher; Igor A. Alexandrov, Researcher. Technical Staff: Lyudmila I. Grabko, Leading Engineer; Konstantin G. Sterkhov, Leading Engineer; Galina G. Zubkova, Senior Lab Technician; Raisa A. Gerasimenko, Technician. Contacts: Tel: +7-4232-312960 E-mail: [email protected]; [email protected] Major research directions genesis of platinum-bearing basic and ultrabasic intrusive complexes from the southern Far East; and the interaction between the hydro- and lithospheres in natural and anthropogenic environments. The Laboratory of Metamorphic and Metasomatic Formation studies the role of magmatic and metamorphic processes in the Earth’s crust and mantle evolution of the Asian-Pacific transition zone. This area of study includes geochemical modeling of fluid and mineral equilibrations during metamorphic and magmatic rock formation; petro- Results 1. The laboratory has studied the petrographic and mineralogical factors of the unique concentrically-zonal Konderskiy alkaline-ultrabasic massif which has a dunite core and related platinum and gold mineralization. The predominant mineral of platinum group is isoferroplatinum (Pt3Fe); gold is present in high-grade cupriferous (generally, CuAu and CuAu3) and silver-containing varieties. 2. Discovery of a noble metal mineralization in Lantar skiy massif, part of the Dzhugdzhurskiy anorthosite massif of autonomous type. The mineralization is related to the massive pyrrhotine ore bodies with small amounts of chalcopyrite, pyrite and pentlandite. The mineral phases of the platinoid are generally presented by platinumpalladium telluride (PtPdTel5) and sperrylite (PtAs2). Gold varies from cupriferous-platinum to relatively high-grade platinum- and silver- solid solutions with palladium. Oleg V. Avchenko – 18 – Facies diagram with suggested areas of P-T metamorphism of the Dzhugdzhur-Stanovoy fold area-related rocks. Dotted lines are geotherms typical for: 1 – island arcs and zones of “hot” rifting; 2 – stable continental crust; 3 – subduction zones of melted oceanic crust; 4 – subduction zones of cooled oceanic crust. Encircled letters indicate indexes of metamorphic facies Galina A. Valuy established that metamorphism of the amphibolite facies of the Dzhugdzhur-Stanovaya fold area proceeded at a significant variation of pressure – from 7 to 13 kbar but under close temperatures – 620-730o C, and the metamorphogene fluid contained much water. The highest-pressure rocks of the amphibolite facies of the Dzhugdzhur-Stanovaya fold area are comparable in depth of occurrence with granulites of the South Aldan Shield. 3. The laboratory developed a petrologic model of Early Pre-Cambrian crust-formation of the Aldan Shield. Geological data and regularities of distribution of main petrogenic elements and admixture elements show that the granulite protoliths of the South Aldan Shield are the volcanites of the calc-alkaline and komatiite-tholeiitic series as well as terrigenous-sedimentary rocks. Basing on the mechanism of plume tectonics we propose petrological models of formation of the volcanites of the calc-alkaline and komatiite-tholeiitic series. 8. The laboratory discovered a new petrologic province of layered granites in the coastal zone of Primorye. 9. The laboratory has found numerous areas of therapeutic mud along the western coast of Amursky Bay and Peter the Great Bay. This mud originated at the geochemical barrier of salinity and alkalinity occurring at the boundary of marine and fresh water mixing. Additional factors of the therapeutic mud’s formation are the closed character of the coastal marine basins and the specific composition of their sediments. 4. The laboratory found that the most highly metamorphosed paragenesis of metamorphic rocks in zonal metamorphic complexes of island arcs of convergent margins characterizes the conditions of the kyanite mineral subfacies of the amphibolite facies. Higher-temperature associations are contact reacting rocks forming in contact zones of gabbro-granitoid massifs. 5. The laboratory completed longstanding studies of the geology, magmatism and the ore-petrology of the Ulkanskiy volcanogenic depression. This area is a new rare-metal province characterized by rare-metal, rareearth, and uranium-molybdenum mineralization associated with the emplacement of the Ulkanskiy rapakivi granite pluton. 6. Based on computer-modeling, phase accordance, thermo degassing, electrochemistry and electronic microscopy methods, the laboratory defined the petrologic evidence for infiltration of reduced fluid in metamorphic rocks. A new way to solve the problems of thermobarometry and oxygen fugacity of mineral association was proposed. 7. Using the method of minimization of the GibbseKorzhinsky thermodynamic potentials the laboratory demon-strates the fundamental possibility of computer modeling of real mineral associations in rocks of any composition with any phases and components. We have Alexander N. Solyanik – 19 – Laboratory of Volcanic Formations Petrology Research Staff: Vladimir. F. Polin, Dr., acting Head of Laboratory Vladimir G. Sakhno, Corresponding Member of RAS, Prof., Chief Researcher Sergei O. Maximov, Dr., Leading Researcher Vladimir K. Popov, Dr., Leading Researcher Andrei V. Grebennikov, Dr., Senior Researcher Technical Staff: Ludmila S. Tsurikova, Leading Engineer Valentina G. Sudzelovskaya, Technician Elena N. Dynda, Technician Contacts: Tel; +7-4232-320560 E-mail: [email protected], [email protected] The Laboratory of Volcanic Formations Petrology became independent in April 1975 when it branched off from the Laboratory of Magmatic Rocks Petrology. The organizer and first head, Prof. Vladimir G. Sakhno, directed the laboratory for twenty-seven years. From 2002 to 2007, the laboratory was headed by Dr. V.K. Popov. Since 2007, the head is Dr. Vladimir F. Polin. – island arcs: Kamchatka, Kuril Islands, the Tonga and Kermadek Archipelago; Major research directions 1. Three types of genetically and structurally related volcanic belts and zones have been identified for the first time for continental East Asia: continental margin, intra-continent and zones of plume volcanism. All types differ in geodynamic regime, deep structure, volcanic evolution, petro- and geochemical composition of rocks, conditions of origin and metallogenic specialization. – marginal seas: Sea of Japan, Philippine Sea, Tasman Sea and others; – islands and sea-bed structures of the Pacific Ocean. Results • Petrology, geochemistry, mineralogy and criteria of ore content of Mesozoic-Cenozoic volcanism at the East Asia continental margin. • Intra-plate volcanism and mantle plumes of the Far East continental lithosphere. • Explosive volcanism and its influence on the environment. 2. A new genetic type of diamondiferous rocks has been identified in microcratones of the Far East, for example, the Kurkhansk diamondiferous diatreme of the Khanka massif. Defined rocks are distinct from kimberlites in specific chemistry and mineral composition and appear to have commercial importance. • Mantle-crust interaction: petrogenetic models. Areas of field work are: – continental part of the Russian Far East (Chukchi Peninsula, Priokhotye, Yakutia, Khabarovk Territory, Amur Region and Primorye) and Northern China; 3. It was determined by thermodynamic calculations that diamonds and native elements could possibly crystallize in the mantle under low P-T parameters and with reduced endogenic fluid involvement. 4. The laboratory has developed a method of quantitative estimation of fugacity (fH2O, fH2, fOH, fHCl and fHF) in fluxes. Based on this method, F- and Cl-bearing magmatic complexes were distinguished, responsible for the course of evolution and ore content of the ore-magmatic systems. The use of these parameters allows researchers to consider the role of rhyolite-granite complexes for specific types of mineralization. 5. A fluid-magmatic model has been proposed for impact ignimbrite volcanism of the Earth. Petrologic and Vladimir F. Polin – 20 – geochemical studies of the impact ignimbrite complexes of the Far East suggest that they result from either explosions of a deep-seated mixture of heavy hydrocarbons, or due to a chain reaction mechanism of “oxygenhydrogen” combustible mixture. 6. The study of ultrabasic rock inclusions into alkali basalts proved the former to be of upper mantle origin, and thus initiated a new approach to mantle structure and composition research. 7. The study of marginal seafloor rocks has established their heterogenic nature. Mechanisms of marginal sea formation due to spreading, western continental margins sinking, and asthenospheric plumes activity have been investigated. 8. Based on the analysis of volcanic complexes, the concept of heterogenic seafloor structure has been proposed for the eastern and western provinces of the Pacific. Basalt typification, using geochemical characteristics, has been made with recognition of the fluid regime contribution to petrogenesis and evolution of melts and their ore content. Petrochemical and geodynamic models have been proposed for the origin of magmatic complexes within oceanic structures. Petrogenetic model of continental volcanic belts of Asia Pacific margin: A – continental margin belts; B – intra-continental volcanic belts; C – zones of plum volcanism 12. Time interval of volcanic activity of Shuphan plateau (South-Western Primorye) was determined and evolution of basaltic volcanism products was characterized in great detail. Formation of the plateau had taken a short time, less than 2 millions of years, and was disastrous. Influx of basaltic melts was accompanied by crust contamination unique in its scale. Alkaline basalt composition evidences high heterogeneity of mantle sources. 9. Carbonatite-bearing tuffs enriched in hercynite and fassaite have been revealed, being a component of products of basaltic volcanism which took place on the Primorye South-West in the Late Oligocene. A volcanic carbonatite formation model was proposed based on the mechanism of the interaction of basaltic melts and calciferous substratum. 13. SHRIMP-dating of “large volume” ignimbrites of the East Sikhote-Alin volcanic belt showed that the ignimbrites were formed over a short period of time. Explosion of huge volumes of pyroclastic materials could be the cause of disastrous effects in the Cretaceous period. 10. Changbaishan volcano structure was described in detail, along with petrochemical and isotopic geochemical characteristics of the volcanic strata. Thorough chronologic study of magmatic events was useful in determining periodicity of the disastrous volcanic explosions. 14. Geochemistry of obsidian tools from the different archeological sites in Primorye, Priamurye and Sakhalin Island have been examined. Correlation of the artifacts with volcanic glasses from local outcrops helped to determine that sources of archeological obsidian were situated in Primorye, Japan and North Korea. 11. Petrogenetic model has been proposed for the different-type magmatic formations of Ketkap-Yuna magmatic province of Aldan. Complicated order of magmatism reflects pulsating nature of fluid-thermal flux and multiplicity of melt sources. Changbaishan volcano and crater lake Tianchi – 21 – Laboratory of Experimental Mineralogy and Petrology Research Staff: Laura P. Plyusnina, Prof., Head of Laboratory George G. Likhoidov, Dr., Leading Researcher Tatyana V. Kuz’mina, Dr., Senior Researcher Technical Staff: Janetta A. Shcheka, Leading Technologist Viktor V. Svetkin, Technician Contacts: Tel: +7-4232-317601 E-mail: [email protected] Major research directions the considerable role of sulfur and arsenic due to their influence upon Pt dissolution, in a hydrothermal media. It was found that with the advent of sulfur or arsenic in the media, lower Pt solubility is limiting the stability of the hydrosulfide complexes and the precipitation of cooperite (PtS) or sperrylite (PtAs2) in spite of relatively low Pt content in the coexisting fluids. Surfaces of the Pt bulk concentration in the sulfur-bearing aqueous-chloride medium are shown in Fig. 2. Thus, in nature, sulphides and arsenides may serve as the geochemical barriers for the Pt precipitation from chloride hydrothermal solutions. The laboratory is focused on experimental and theoretical (physicochemical calculations) studies of noble metal deposits. Results 1. The laboratory examines platinum behavior in complex aqueous fluids at 300-500 oC and under 1 kb total pressure within -36 < logfO2 < 0.5 range of redox potential. This laboratory showed for the first time that high oxidizing media stabilizes Pt (IV) complexes up to 500 oC. During a set of analyses (runs), platinum content in fluids under lower temperatures (200-300 oC) was subjected to an influence of phase transformation of solid Mn oxides, which mixes were used as the oxygen buffers (Fig. 1). The well-known Pt content of extensively studied Mn-bearing sediments on the sea floor could be formed in a similar manner. 3. The study of gold and platinum chemosorption by organic matter (bitumen) at 20-500 oC and under 1 kb, revealed that thermal metamorphism of the matter resulted in its condensation, aromatization, and noble metals accumulation in kerogen. The high sorption capa city in relation to the metals was fixed at temperatures up to 500 oC. Therefore bitumen is an efficient chemical barrier favoring immobilization of the metals. 2. Experimental modeling of Pt behavior in the Pt-Fe-(Ni)-As-S-Cl-H2O system (300-500 oC, 1 kb) showed 4. High sorption capacity of graphite in relation to gold (2980 ppm) and platinum (790 ppm) was measured at 500 oC and Ptot = 1 kb in course of asphaltenes → → kerogen → graphite transformation. Distribution of the noble metals in phases coexisted in the system is summarized in Fig. 3. The results are confirmed by the discovered invisible noble mineralization in Riphean graphitebearing metamorphic complex of the Khanka terrane. 5. Experimental studies and thermodynamic modeling assigned the advent of CO2 in aqueous-sulfide-chloride solutions to negatively effect gold solubility at 300-400 oC (1 kb). Thus, the listwaenite that forms under high CO2 activity may be considered as a geochemical barrier for the gold precipitation in hydrothermal media. Laura P. Plyusnina – 22 – Fig. 1. Pt dissolution kinetic curves in complex aqueous media in the presence of unstable (200 oC / 1 kb MnO-Mn3O4) buffer mix Arrow denotes spontaneous metallic platinum crystallization at quenching time Fig. 2. The Pt bulk concentration surfaces at dissolution of Ptmet (a) and Cooperite (b) in aqueous-chloride solutions buffered by PPM Fig. 3. Sorption capacity for Au and Pt of different fractions coexisting in the system according to the temperature (Ptot = 1 kb) Metal concentration in the following: 1 – insoluble residue, 2 – soluble fraction of the organic matter, 3 – coexisting aqueous fluid – 23 – Laboratory of Mineralogy Research Staff: Sergey V. Vysotskiy, Prof., Head of Laboratory Sergey A. Shcheka, Prof., Chief Researcher (Honored Science Worker of Russian Federation) Valentina P. Zvereva, Prof., Leading Researcher Victor P. Nechaev, Dr., Leading Researcher Alexander S. Zhitkov, Dr., Researcher Anna V. Barkar, Dr., Researcher Alexander A. Vrzhosek, Senior Researcher Evgeniya V. Nechaeva, Junior Researcher Alyona M. Kostina, Postgraduate Student Technical Staff: Michail V. Mokrousov, Leading Engineer Yuriy A. Lebedev, Leading Engineer Nina A. Vasiltsova, Senior Laboratory Assistant Contacts: Tel: +7-4232-317132 E-mail: [email protected] Major research directions The laboratory studies the mineralogy and petrology of alkaline ultrabasic and boninite-komatiite volcano-plutonic complexes of the Pacific-Asia transition zone. In addition, the laboratory researches the chemical inhomogeneities of minerals as an indicator of the crystallization processes. The laboratory also studies the sapphire- and diamond-potential of basic and ultrabasic complexes and the determination of mineralogical and geochemical criteria for prospecting of the Primorye alkaline basic-ultrabasic complexes for platinoids, titanium, and gem stones. Results 1. The laboratory has discovered meymechite, an alkaline ultrabasic volcanic rock, in the Primorye region. This type of rock is wide spread around the Pacific in relationship to kimberlite and lamproite formations. Diamonds were discovered in alluvium deposits associated with the meymechite fields, while related intrusives included commercial ilmenite deposits and gold-platinum mineralization. Based on the study of microcrystalline diamonds (carbonados) discovered in Primorye, the laboratory has proposed a new model for their formation due to oxidation and recrystallization of “heavy” isotope kimberlite diamonds under low pressure and temperature and under the catalytic influence of titanium. 2. The laboratory identified a specific boninite-type ophiolite complex composed of the boninite volcanic rocks and orthopyroxene intrusions in the West Pacific island arcs. It has been found that boninite minerals are characterized by remarkable composition zoning that can be explained by sharp fluctuation of the fluid regime of melts. Sergey V. Vysotskiy – 24 – The laboratory defined the composition of boninite melt fluids in more detail than previously known as such: water is suggested to be a secondary phase resulting from oxidation of deep reduced (methanehydrogene) fluid. 3. The laboratory has discovered gem corundums (sapphires) for the first time in the Primorye region in river sediments, and later in Cenozoic alkaline-basalt volcanoes. The sapphires are revealed to be associated with alkaline basalts with relatively high sodium content. “Basaltic” sapphires are enriched in iron (0.5-3.17% FeO) with titanium being almost totally lacking, while the metamorphic and metasomatic sapphires are characterized by a higher content of Ti with minor amounts of Fe. It is suggested that this characteristic could be used to reveal the source of sapphires from alluvia deposits. 4. Five years ago the laboratory initiated a new project: “Nanosructures of natural minerals”. The laboratory initiated the study of nanostructures of natural minerals for the first time in the Russian Far East. A fractal nanostructure is a characteristic feature of all the natural minerals. For example, a single layer of the sapphire looks like as a cellular hexagonal net at all the atomic-molecular and nanno levels. 5. Between 1971 and 2007, the laboratory had developed a map of Russian Platinum Mineralization (Far Eastern Section) and published twelve monographs and more than three hundred scientific papers. Researchers have also been granted two patents. – 25 – Laboratory of Metallogeny of Precious Metals Research Staff: Vadim G. Khomich, Prof., Head of Laboratory Vladimir P. Molchanov, Dr., Leading Researcher Igor I. Fatyanov, Dr., Senior Researcher Natalya G. Boriskina, Dr., Senior Researcher Ludmila F. Simanenko, Dr., Senior Researcher Grigory R. Sayadyan, Researcher Vitali V. Ivin, Junior Researcher Evgeni I. Medvedev, Junior Researcher Technical Staff: Mikhail V. Koval, Laboratory Assistant Oleg V. Ognev, Laboratory Assistant Contacts: Tel: +7-4232-320563 E-mail: [email protected] Major research directions metasomatic alterations of the terrigenous substratum, granitoids, and volcanites are widespread (Khomich, Boriskina, 2006; Boriskina, Khomich, 2006). We have studied the features of the native gold composition and its areal distribution in gold-ore formations and products of their exogenetic destruction within the Blagodatnensky ore-placer node (Primorye). We have found an unusual association of Pd-gold with microspherules of schorlomite that is almost exclusively found in ultrabasic rocks. Presence of this association is considered an evidence of participation of platinoid-gold mineralization in placer-forming process. This minerali zation resulted from hydrothermal reworking of deepseated rocks (Medvedev, Molchanov, Khomich, 2006). We have first justified that large gold-ore districts of Transbaikal and Upper Amur areas (Lyubavinsky, Baleisky, Kariisky, and Gonzhinsky), situated near the northern boundary of the Argun superterrane and the Mongol-Okhotsk suture, belong to one-type-structure oremagmatic systems. This allows for an objective evaluation of the region’s potential for increasing the mineral resource base of precious metals (Khomich, Boriskina, 2007). We considered in succession the main features of magmatism and metallogeny of the East-Sikhote-Alin volcano-plutonic belt and the geological structure of the Dal’negorsk district and Partizansky skarn-polymetallic deposit. The results of the detailed study of mineral associations, vertical mineralogical and geochemical zonality of the deposit, and typomorphic features of silicate and ore-forming minerals have been reported. Forms of bismuth (Bi) and silver (Ag) occurrence in ores and regularities of localization of Bi and Ag mineralization in ore bodies are described. We discuss the deposit genesis in terms of the data obtained and demonstrate the possibility for using the revealed vertical zonality of mineralization in the forecasting valuation of the skarn-polymetallic deposits of the district (Simanenko, Ratkin, 2008; Simanenko, 2007). In the context of the problem of increasing of the gold raw materials resource base we have considered the criteria of searching for the Karlinsky (Nevadiisky) [Carlin, Nevada] type deposits in the region. We showed The Laboratory of Metallogeny of Precious Metals studies the formation of precious metals, the reconstruction of precious metal ore-forming systems, and location of precious metal deposits in the Russian Far East. We also estimates the potential of the Primorye Region for new gold deposits and production. These appraisals are based on analyses of the Amur Au-bearing belt and potential for noble metals of the Khanka and SouthBureya metallogenic zones. Results Our study of the geological structure and analysis of materials on gold content of four ore deposits: the Borgulikansky (gold-copper-porphyry), Pionernyi, Burindinsky, and Pokrovsky (gold-silver), found within the Late Mesozoic volcano-plutonic setting of the Pre-Cambrian Gonzhinsky protrusion, allowed us to define the main factors of localization of the precious-metal mineralization and the type elements of the structural and geological setting of the deposits. These ore-bearing areas are typically associated with zones of jointing in the volcano-tectonic depressions near the outer boundaries of granitoid massifs (remote from the Pre-Cambrian center) where the extrusive, subvolcanic bodies (necks, stocks, sills, dikes) of “mottled” composition and aureoles of hydro-thermal- Vadim G. Khomich – 26 – that the favorable indicators for the Argun superterrane to contain potential Carlin-type gold deposits were not only the extensive evidence showing its similarity to the NorthAmerican Cordillera, in particular to the Nevada State territory, where the Carlin-type deposits are widespread, but also its position over the East-Asian “hot mantle zone”. The existence of the latter is responsible for the possibility of initiation of the mantle plumes that, as in the case with the North American continent, could influence the development of ore-forming processes and concentration of gold in the Paleozoic carbonate strata of the superterrane cover (Khomich, Boriskina, 2008). This research strongly indicates the necessity of increasing the attention of prospectors and explorers to the Argun area. We have first described a unique association of natural amalgam of gold, cinnabar, native Fig. 2. Dynamic model of formation of the Mnogovershinnoe gold-silver deposit metals, cohenite, and moissanite within the Fadeevsky ore-placer district. The structure and composition of these phasexplained by the fact that the Oemku district belongs to the es have been studied using a scanning electron region with a thinner crust where the destructive processes, microscope. Cinnabar and auramalgam (Au2Hg3) demonrelated with deep dislocations in the Mesozoic-Cenozoic strate a heterogeneous composition within a grain (Fig. 1). time, were more intensive as compared with Southeast In some micronuggets of mercury-bearing gold, fractality China where deposits were formed within terranes with was found responsible for a microporous texture. The a higher thickness of continental crust (Boriskina, composition heterogeneity, microstructure fractality, and Khomich, Molchanov, 2008). presence of carbides associated with cinnabar testify We have reconstructed the hydrothermal ore-forming to the unbalanced nature of this assemblage. Native paleosystem of the Mnogovershinnoe gold-silver deposit metals are spheroids of iron and copper, practically with regard to the formation mechanisms of the strucwithout admixtures, and aggregated microplates of zinc tural-matter elements composing the ore-bearing zones, overgrown with nanospheroids of carbonaceous compo their position on the conventional chronological scale sition. We concluded that this association was crystal- of hydrothermal activity, and isotope data. Using the struclized through gas condensation of endogenous hydrogentural-matter elements in deciphering the ore genesis events hydrocarbonic fluids (Molchanov et al., 2008). made it possible to take account of both synchronously We have studied the oxygen and hydrogen stable and successively formed components of ore bodies that isotopes of minerals from eight occurrences of precioussignificantly increased the quality of the reference data metal mineralization of the Oemku ore district (Dzhegdag, in the construction of the deposit dynamic model (Fig. 2). Verkhneoemkinskoe, Molodezhnoe, Oemku, Shirokoe, The approach proposed for the reconstruction of the Gornoe, Noyabrskoe, Berezovoe) and deposits of Southhydrothermal paleosystem of the Mnogovershinnoe eastern China (Zhilingtou, Mashan, Bitian, Longtoushan). deposit can be used in constructing the models of other ore We made the inference about different water sources deposits (Fatyanov, Khomich, Boriskina, 2009). of ore-forming solutions responsible for the formation Resent accomplishments of the laboratory are: of significant concentrations of precious metals. The • the determination of the main reasons for the welldeposits of the Oemku district were, most likely, known dislocation of gold and tin mineralization: due to formed with more active participation of waters the separation of Au and Sn migration routes during magof magmatic gene matic stages as a result of different reactions to silicatesis, and the depoforming clusters of melts, oxygen, and other strong oxidants; sits of Southeast • the creation of a generalized dynamic model of inter China – waters action of juvenile solutions and infiltration therms of meteoof meteoric oriric genesis in gold-concentrating polygenic hydrothermal gin. At the deposits systems, based on analysis of the relationship between of the Oemku disthe structural elements of ore-bearing rocks and isotope trict, sulfur and research. carbon are also • the development, in collaboration with the Institute of magmatic oriof Chemistry FEB RAS, an effective technology of noble metals extraction from alluvia, based on gravitational, Fig. 1. A light film of auramalgam gin. These differon dark ilmenite. The Fadeevsky ore- ences in the source magnetic, and electromagnetic separation, demercurization placer district (Southwestern Primorye) materials can be and hydrometallurgy. – 27 – Laboratory of Metallogeny of Ore Districts Research Staff: Valery V. Gonevchuk, Prof., Head of Laboratory Vitaly I. Gvozdev, Prof., Leading Researcher Pavel G. Korostelev, Dr., Leading Researcher (Honored Geologist of Russian Federation) Galina A. Gonevchuk, Dr., Senior Researcher Boris I. Semenyak, Dr., Senior Researcher Alexander A. Orekhov, Junior Researcher Technician Staff: Tatiana M. Shamrai, Leading Engineer Dinna K. Kokorina, Dr., Leading Engineer Irina V. Sinyova, Senior Laboratory Assistant Andrei P. Zaichenko, Laboratory Assistant Contacts: Tel: +7-4232-321249, E-mail: [email protected] The Laboratory of Metallogeny of Ore Districts was initiated in 1959. Ekaterina Alexandrovna Radkevich was the Head of the laboratory until 1974. She was a Corresponding Member of the USSR Academy of Science and instigated its formation. She became the first Director of the Geological Institute and one of the recognized leaders in research of metallogeny. Most of the present researchers in the laboratory undertook postgraduate research or completed course work under her supervision. of Khabarovsk Region, and in the Armu, Kavalerovo, Furmanovo and Dal’negorsk ore districts of Primorye. Major research directions Valery G. Gonevchuk, and Galina A.Gonevchuk – orebearing magmatism and magmatism-related mineralization; The laboratory’s researchers work as a team when dealing with general problem of genesis of ore deposits and undertake research in areas of scientific interest described below. Vitaly I. Gvozdev – mineralogy and genesis of tungsten and tungsten-tin deposits; Studying the regional location and formation of tin deposits, and associated tungsten, lead, zinc mineralization forms the primary work of the laboratory. Dinna K. Kokorina – thermobaric and geochemical parameters of ore formation; The main areas of field research are the ore districts of Primorye and the southern part of Khabarovsk Region. In terms of geologic models, they are the area of juxtaposition of the ancient Proterozoic - Early Paleozoic formations of the Khanka and Bureya terranes and the Phanerozoic accretional folded complexes of the Sikhote-Alin. Among the numerous ore districts of the Sikhote-Alin, the most detailed field studies have been performed in the Khin gan-Olono, Badzhal and Komsomolsk ore districts Pavel G. Korostelev – investigation of ore paragenesises for the reconstruction of physical and chemical parameters of deposits; Alexander A. Orekhov – peculiarities of polygenic ore-magmatic systems; Boris I. Semenyak – genesis features of Sn-bearing greisens. Meeting after the route at a field camp. Kavalerovo district of Primorye Valery V. Gonevchuk – 28 – Results The laboratory has published monographs which describe the most important tin and tungsten ore districts in the Russian Federation. Publications include: Geology, Mineralogy and Geochemistry of the Komsomolsk Ore District, 1971; Metallogeny of the East of the USSR, 1976; Mineralogy and Geochemistry of Tin Deposits, 1976; Mineralogy, Petrography and Genesis of SkarnSheelite-Sulfide Deposits of the Far East, 1977; Geology, Mineralogy and Geochemistry of the Kavalerovo Ore District, 1980; Geodinamic model of ore-magmatic system of the SikhoteAlin Zoning and Depth Distribution of Tin Mineralization, 1980. (Based on the example of the Kavalerovo ore district); Deep Structure and Metallogenic Peculiarities of the South of the Far East, 1984; Tin Ore Deposits of Primorye, 1986; Metallogeny of the Main Tin Districts of the South of the Far East, 1988; Ore Deposits of Continental Margins, 2000. Issue 1. 2001. Issue 2. Volumes 1 and 2; Tin-Bearing Systems of Far East: Magmatism and Ore Genesis, 2002. The multiple investigations result in the development of graphic and descriptive models of the metallogeny for different geographical areas. A metallogenic map of the Pacific ore belt, scale 1:10 000 000, (Ed. E.A.Radke vich, 1979), is an example of a graphic model created by the laboratory. The research staff of the laboratory took part in the preparation of multi-scaled maps of the Komsomolsk and Kavalerovo ore districts. The laboratory effectively co-operates with the mining and geological industry. The benefits of this collaboration were recognized when Dr. Pavel G. Korostelev was awarded the title “Honored Geologist of Russia”. Recent scientific activity of the laboratory resulted in: • the improvment of classification of ore deposits formation; • the specifying of the geological, mineralogical and geochemical characteristics оf tin and tungsten deposits in the Russia Far East Region; • the analyzing of the regularity of distribution of different ore mineralization in the main ore districts of the Far East and the region as а whole; Sketch-map of ore districts of the southern part of the Russian Far East and main objects of fieldworks (red-colored areas) • the creation of maps, diagrams and descriptive geologic genetic models of a variety of ore systems. – 29 – Laboratory of Geochemistry Research Staff: Yury A. Martynov, Prof., Head of Laboratory Emma D. Golubeva, Prof., Senior Researcher Irina A. Tarasenko, Dr., Senior Researcher Aleksander A. Chashchin, Senior Researcher Igor Yu. Chekryzhov, Researcher Aleksey Yu. Martynov, Junior Researcher Technical Staff: Nina E. Gvozdeva, Leading Engineer Natalya N. Semenova, Leading Engineer Mariya Yu. Martynova, Engineer Lyubov A. Kariyuk, Laboratory Technician Contacts: Tel: +7-4232-318291 E-mail: [email protected] Major research directions • The laboratory defined the characteristic structures and geochemical layering of technogenic deposits resulting from progressive lithogenesis of Primorye. In addition, the laboratory identified some newly-formed mineral associations and reconstructed their formation conditions. The laboratory was able to determine the rules of techno genic transformation of the geological environment during the regressive lithogenesis of Primorye. The laboratory studies basaltic rock evolution in the continent-ocean transition environment, the relationships between the geochemistry of basalts and the geodynamic, and the geochemistry of technogenic lithogenesis. Results • The laboratory has carried out a geochemical study of the Quaternary and Miocene volcanic rocks of the Kuril Islands. The investigation included a reconstruction of the geodynamics of the subduction zone formation and of the evolution of magma. The study included the contribution of subduction and non-subduction factors (heterogeneity of subcontinental lithosphere, Kuril basin opening) in magma genesis. • The laboratory carried out mineralogical and geochemical research of the Mesozoic and Cenozoic basalts of the Russian Far East to understand mantle dynamic and lateral heterogeneity in the transition zone between Asia and the Pacific Ocean. • The laboratory reconstructed Late Cenozoic explosive volcanism and related hydrothermal mineralization in the continental basins of the Southern Primorye. VF – volcanic front RA – rear arc Th/Nd vs. 143Nd/144Nd plot for Kunashir lavas (Kuril Islands arc) and relationship to the slab components. The altered oceanic crust MORB (AOC) and AOC fluid end members are the same used in Ishizuka et al. (2006b). Sediment (SED) fluid and sediment melt components were calculated based on averaged bulk composition of sediment columns subducted at trenches of Kuril and Japan island arc systems (Plank & Langmuir, 1998). Bulk distribution coefficients between sediment and fluid (700 0C) and sediment and melt (900 0C) are from Johnson & Plank (1999) Yury A. Martynov – 30 – Computer Technology Laboratory Laboratory Staff: Vera V. Naumova, Prof., Head of Laboratory Alexander N. Chetyrbotsky, Prof., Leading Researcher Ivan N. Goryachev, Postgraduate Student Stepan A. Semenyuk, Technician Contacts: Tel: +7-4232-317850 E-mail: [email protected] The Computer Technology Laboratory was founded in 1994. The main object is development of principles and methods of computer description and analysis of geological systems. Major research directions • Development of geological data bases and geoinformation systems (GIS) for resolving problems of regional geology. • Application of mathematical methods for geological data analysis. • Computerization of scientific research. Results An example of the GIS Project Map The laboratory is a creator of the informational server of FEGI FEB RAS (http://www.fegi.ru) and a “Regional portal: Primorsky Krai of Russia” (http://www.fegi.ru/primorye), which are constantly supported in the Internet. The portal provides the worldwide on-line users with unique information about more than 100-year investigation history of the region and presents materials contributed by more than 300 researchers from 7 institutes of the Far East Branch of the Russian Academy of Sciences, and 3 Vladivostok-based universities, as well as the State Museum of Arsen’ev, the Vladivostok-Primorye Eparchy of the Russian Orthodox Church, the Society of Amur Region Study, and many other regional organizations. Over 5 000 web sites of the portal contain articles about the unique and wonderful nature of the region, its natural resources, plants and animals, inhabitants of the Peter the Great Bay, reserved territories, ecology, history, religion, science, education, culture, economics, tourism, health protection, and many other topics. There are fifty different maps of Primorye and over two thousand pictures by the famous photographers and scientists of FEB RAS, showing the unique features of the region. In 2000, the portal became a prize-winner of a contest, “Internet Access and Training Program,” conducted by the noncommercial US organization “Project Harmony” supported by the Bureau of Educational and Cultural Affairs of U.S. Government. The laboratory was succesful in development of several efficient products: • scientific information search system "Geology of the Russian Far East". The system consists of 3 data bases: "Sedimentary Formations" (used by the Geological Institute, RAS, Moscow), "Volcanic Formations", and "Intrusive Formations"; • GIS Project "Geology and Mineral Resources of Primorsky Krai” and a first version of the GIS Project “Granite Formations of the Southern Far East of Russia”; • data bases: "Mineralogical Museum of FEGI FEB RAS" and "Composition of Basalts from Different Geodynamic Settings"; • "Algorithm and Program for Calculation of Boninite Crystallization Model Composition". The laboratory designed digital version of the North East Asia Tectonic Map (scale 1:5 000 000). The GIS Project “Mineral Resources, Metallogenesis and Tectonics of North East Asia” was made in cooperation with many Russian and foreign geological surveys and scientific organizations. Vera V. Naumova http://www.fegi.ru/primorye – 31 – Interlaboratory Group for Investigation of New PGE Types and Development of Modern Processing Technologies An extensive group of noble metals remarkable by their unique characteristics, with platinum group elements (PGE) above all, is of the extreme importance for the science and technology progress of the world and economic prosperity of nations. The world PGE reserves (less Russia) make up about 52 000 t, with 96% belonging to South Africa. The most important PGE for the operat- ed objects are platinum-chromite (42%), low-sulfide platinum-metal (34.2%), and sulfide platinum-coppernickel (22.4%) deposits. In 1980-1990 Russia ranked first and second in mining of Pd and Pt, and first and second (together with South Africa) in mining of Rh and Ru correspondently. Lately these numbers noticeably dropped. In order to keep the leading positions at the market, the volume of exported PGE was compensated from the national strategic reserves. Judging by confirmed assessments, in the competition between Russia and South Africa, the latter will become the absolute leader very soon due to its intensive operation of the unique Bushveld Igneous Complex. Production of platinum group metals in Russia, actually entirely based on the ores of the sulfide copper-nickel deposits of the NorilskTalnakh ore district, is rather vulnerable due to consider able losses of PGE in course of by-production, and to modification of raw material quality with time. Fig. 2. Spheroidal microcrystal of gold with included graphite lamellas Russia obviously needs increase PGE output, and not only through operation of more deposits, moreover most of them are located in the Arctic zone remote from the main industrial districts. To gain this objective, new types of ores shall be operated and modern processing technologies shall be developed. The Interlaboratory Group was organized at FEGI, just for this purpose, as non-traditional type of platinum mineralization was found at the Russian Far East: in Primorye, Khabarovsk Province, and Jewish Autonomous Territory. The group includes FEGI director and the leader, Academician A.I. Khanchuk, Prof. L.P. Plyusnina, Drs. G.G. Likhoidov and V.P. Molchanov, and young scientists T.V. Kuzmina and E.I. Medvedev. Fig. 3. Cloddy microcrystals of gold in carbonaceous matrix and graphite nanotube framed in the upper part of the TEM micrograph Fig. 1. Graphite occurrences in northern part of the Khanka terrane – 32 – Results The northern Khanka terrane has been for the first time studied for gold and PGE content in Late Proterozoic – Lower Cambrian high-carbonaceous metamorphic rocks. Local graphite deposits of the Tamgino-Turgenevo group have been known since 1945 (Fig. 1). A complex sequence of granite-gneiss, marble, biotite-feldspar graphite, and garnet-biotite-feldspar crystalline schist with concordant lamprophyre dykes underwent regional graphitization. Gold (to 30 ppm) and platinum (to 52 ppm) contents of economic interest were measured in the all mentioned rocks by ion mass-spectrometry, neutron activation, and atomic absorption spectroscopy. Native noble metals (gold, platinum and silver), zink, copper, bismutite, and intermetallides (Cu-Sn, Cu-Zn-Fe) were found by transmission electron micro scope in association with graphite. It is noteworthy that in comparison with “visible” platinum and silver, the “visible” gold is spread better. Usually, gold forms fine spheroids and cloddy-sponge grains (0.01-2 μm) (Fig. 2, 3). Besides, aggregates of nanosized gold and silver particles are present in carbonaceous matrix (Fig. 4). Ferroplatinum and metallic platinum with minor copper admixture (< 1wt.%) were found by transmission electron microscope (TEM) in graphite-bearing gneiss near the rives Tamga and Ruzhinka (Fig. 5). Fig. 4. TEM micrograph of the nanoensemble of gold (light) and silver (grey) in graphite matrix (dark) The principal peculiarity of this new ore type implies that noble metals are incorporated into graphite and carbonaceous matrix as micro and nano particles, whereas sulfides, common to black shales, occur in the studied rocks in subordinate amount. Fig. 5. TEM micrograph of the ferroplatinum skeletal crystal in graphite from granite-gneiss PGE contents spread (Fig. 6) shows that PGE objects of Primorye are comparable with major deposits of the world (Bushveld, Norilsk, Great Dyke, Stillwater), whose average PGE content in raw material makes up 4-6 ppm, and rarely more. The required content standards, however, continue to decrease, and more depleted raw material is mined with each years. The above comparison, as well as abundance and bedding conditions of graphitized ores within the Russian Far East show how challenging they are for platinum group elements. Fig. 6. Spread of PGE contents in the graphitized rocks of Primorye based on ion mass spectrometry results (yellow colored area) – 33 – Mineralogical Museum Research Staff: Valentin T. Kazachenko, Prof., Head of the Mineralogical Museum Valentina A. Solyanik, Senior Researcher Elena V. Perevoznikova, Junior Researcher Natalya V. Skosareva, Junior Researcher Technical Staff: Raisa P. Shulga, Senior Laboratory Technician Contacts: Tel: +7-4232-317834 E-mail: [email protected] The Mineralogical Museum undertakes research on the geochemistry, mineralogy, mineral associations, and genesis of gold, silver, platinum and palladium metalbearing deposites of the Triassic-Jurassic carbonaceous rocks of the Sikhote-Alin. museum as a knowledge resource where lectures about geography and natural history of Vladivostok and other cities of Primorye are given by the museum scientists. Special attention is paid to ecological education and problems of the geological environment. Fifteen hundred samples are permanently on exhibit in the museum. Together with another samples under storage, the museum possesses thirteen thousand samples in total. The collection includes samples of magmatic, sedimentary and metamorphic rocks, as well as different ores, minerals and petrified remains. Annually the museum accepts around one thousand visitors, including foreigners from Japan, China, Korea, USA, Sweden, Ireland, Germany and many other countries. A real treasure is the “Stone flowers” collection composed of unique specimens of calcite, quartz, apophyllite, datolite, galena, and sphalerite druses. The well-known Dal’negorsk “calcite roses”, with their magnificent calcite crystals of different shape, resemble fragile white, yellow, and pink flowers. The museum collections illustrate the scientific work embracing a wide range of geological issues of the Far East region and are classified into 5 sections: historical geology, lithology, petrography, commercial minerals and mineralogy. Some minerals are extremely rare in nature, such as pyroxmangite, kanoite, pyrosmalite, bementite, tirodite, dannemorite, manganoan aktinolite, tin-bearing spessartite, barium rich phlogopite, pyrophanite, chromian and vanadium tourmaline, diaphorite, silver-tetrahedrite, freibergite, meneghinite, aurostibite, etc. The unique skarn of the Dal’negorsk borosilicate deposit is comparable to Ural malachite in terms of its beautiful patterns and hues of color. Skarn, sometimes called “Primorsky malachite”, display amazing patterns of apple-green datolite, pearly wollastonite, pink apophyllite, dark-green hedenbergite, and brownish garnet. This rock, characterized by diverse textural fibers, beautiful colors and by the great strength, has gained the reputation of an outstanding stone-cutting material. The museum is a significant scientific and educational center of the Russian Far East. Students of the Geological Departments of the Universities in Vladivostok use the Olenekoseras miroshnikovi (Burij & Zharnikova) (=”Keyserlingites”). Triassic (T1), Neocolumbites insignis zone (the Zhitkov Cape, Russian Island). Yuri D. Zakharov’s collection Valentin T. Kazachenko – 34 – A group of obelisk-like differently oriented red quartz crystals. Sovetsky-II Mine, Dal’negorsk, Primorye “Owl” handmade article. Obsidian and borosilicate skarn from the Dal’negorsk borosilicate deposit “Rose”-like druse of lamellar light pink calcite in a white shirt of fine-crystalline calcite. Sovetsky-II Mine, Dal’negorsk, Primorye A druse of fine laminated white calcite called “Flowered branch”. Sovetsky-II Mine, Dal’negorsk, Primorye A druse of octahedral crystals of galena. Sovetsky-II Mine, Dal’negorsk, Primorye Small crystals of pink apophyllite growing on the datolite faces. Borosilicate deposit, Dal’negorsk, Primorye Halite, skeletal crystals. California, USA Exhibition hall of Mineralogical museum – 35 – Analytical Center • Implementation of independent scientific research as well as methodological innovations that complement the institute's long-run scientific themes as well as the needs of potential clients. The Analytical Center of the Far East Geological Institute (AC FEGI) was established under the initiative of Academician A.I. Khanchuk, Director of FEGI, in 1999. The center integrates four analytical laboratories of the Institute. AC works for the needs of FEGI as well as other institutes of the Russian Academy of Sciences. It is also open for research collaboration with foreign scientific institutions. • Development, interconnecting, and application of chemical and instrumental methods of structural and compositional analysis of many naturally occurring and synthetic materials; development of novel procedures as well as adaptation and promotion of the standardized procedures for various matter analyses. The Head of AC is Prof. Alexander V. Ignat’ev, Deputy Director of FEGI. • Technical perfection and modernization of instruments and their modular systems. Structure 1. Laboratory of Precious Metal Analysis • Accumulation and systematization of analytical data and new methodological techniques. 2. Laboratory of Analytical Chemistry 3. Laboratory of Stable Isotopes • Providing a wide range of analytical services and rendering methodological help to internal users of Russian Federation and specialists of other countries; advisory activity and personnel training. 4. Laboratory of X-ray Methods Major objectives AC FEGI keeps current with key analytical advances and implements modern analytical methods and techniques, provides advanced training for analytical personnel, and keeps an eye on advances at western analytical centers. • Development of co-operation both within the framework of formal scientific programs as well as on the basis of direct bilateral agreements between cooperating groups. Participation in joint projects and scientific programs carried out in co-operation with research centers in Russia and abroad. Activities • Providing FEGI laboratories with high quality analy tical data for the programs and projects they are involved in. In AC FEGI, along with classical methods of “wet” chemistry, photometrical and electrochemical (potentiometry and potentiometric titration) quantitative analyses, there are many other modern instrumental methods and techniques to determine the composition and structure of substances. Non-destructive elemental, molecular and phase analysis Surface analysis • Inductively coupled • X-ray fluores- cence (XRF) spectroscopy • X-ray electron spectroscopy plasma atomic emission spectrometry • Arc source atomic emission spectrometry • Hydrogen background correction atomic absorption spectrometry Destructive elemental analysis • Zeeman background correction atomic absorption spectrometry • Molecular-absorption spectrophotometry – Electron microprobe analysis – Electron microscopy • X-ray difractometry – Photocolorimetry – Nefelometry and turbidimetry IR-spectroscopy Structure analysis • Inductively coupled plasma mass spectrometry (ICP - MS) • Isotopic mass spectrometry – 36 – Laboratory of Precious Metal Analysis Research Staff: Vladimir V. Ivanov, Dr., Head of Laboratory Nikolai N. Barinov, Dr., Senior Researcher Peter P. Safronov, Dr., Senior Researcher Anna A. Lotina, Junior Researcher Anna V. Ivanova, Research Assistant Technical Staff: Alexander S. Bukatin, Leading Technologist Olga F. Gurphink, Engineer Olga N. Kenya, Leading Programmer Larisa G. Kolesova, Leading Engineer Valery V. Kononov, Dr., Leading Technologist Gennadiy A. Narnov, Leading Technologist Lubov V. Simokon, Leading Engineer Svetlana F. Vasyukevich, Leading Technologist Galina S. Yagorlitskaya, Leading Technologist Valentina F. Zanina, Leading Technologist Contacts: Tel: +7-4232-317583; +7-4232-732702 E-mail: [email protected], [email protected] Chemical-analytical investigations Analytical equipment: • Atomic Absorption Spectrophotometers: Shimadzu AA-6800; Thermo Electron SolAAR M6. • FT-IR Spectrometer Thermo Scientific Nicolet 6700 with Continuum FT-R microscope. • Х-ray fluorescence Spectrometer (hand-held XRF Analyzer) Innov-X Alpha-6000. • Electric Assay Furnace DFC Ceramics DFC-810B. The laboratory pays special attention to the preparation of samples. The Sample Preparation Division provides services using the following equipment: different crushing and grinding machines, a set of sieves, ultrasonic disperser and sample classifier. The laboratory sample preparation instruments include Cem MARS 5 (microwave oven), Rocklabs Boyd, Fritsch Pulverisette -0, -1, -5, -13, -19, -23 & -25; Laborette-17, -24 & -2 and Analysette-3. There exists the possibility for separation of fine-grained platinoids, gold-, silver-bearing and some other minerals using a centrifugal concentrator for gravity concentration of fine assays. The Laboratory of Precious Metal Analysis is a unit with a broad research activity. Physical-chemical and mineralogical-geochemical studies of precious metal lode and placer deposits as well as an examination of natural mineral and synthetic materials and other substances such as mine tailings and post-processing products have been carried out for many years. With a long history of field experience in East Asia, the laboratory is a leader in supplying geological information and analytical data for research concerning a wide range of geological problems. The set of certified sample standards and procedures of quantitative analysis enables us to carry out traditional chemical analytical works as well as research on the adaptation of known analytical techniques to the individual characteristics of the matrix of study materials. Current analytical capabilities of the laboratory are primarily focused on elemental analyses of materials of natural and man-made origin using the following analytical methods: The laboratory is equipped with many specialize d instruments, similar to those of other world class chemical-analytical facilities. • Traditional fire assay with gravimetric finish and/or atomic absorption spectrometry; Our highly competent personnel is able to work on specific analytical problems and develop analytical methods to address various clients’ requirements. • Fire assay with atomic-absorption finish for determination of platinum-group elements, gold and silver at trace level. Vladimir V. Ivanov The Electron and Light Microscopy Division. A. Bukatin – 37 – Mineralogical investigations Analytical equipment: • Research-grade and laboratory microscopes: Zeiss AxioImager D1, AxioPlan2, AxioStar, SteREO Discovery V12, SteREO Lumar V12 and Stemi 2000; Nikon Eclipse LV100 Pol and SMZ 800; Leica MS5 and EZ4D. • Scanning Electron Microscopes: Zeiss EVO-50XVP with Oxford INCA Energy EDS; Jeol JSM-6490 LV with Oxford INCA Energy EDS. Research activities: The Atomic Absorption Spectrophotometry Division L. Simokon, O. Gurphink, G. Yagorlitskaya, S. Vasyukevich • A light and electron microscopic study of ores and host rocks, including a comprehensive mineral identification, phase analysis of minerals and so forth. • A complete mineralogical analysis of heavy-mineral concentrates and/or a selective particle-size analysis as well as a morphogenetic analysis for placer gold, platinum and related minerals. • Instrumental determination of major and minor elements for native gold and manufactured alloys containing precious metals. • Revealing the typomorphic characteristics of minerals that are informative with respect to their formation and transformation under various conditions. • IRS-diagnostics of minerals and thin mineral mixtures (infrared spectrometry FT-IR Spectrometer). The laboratory has a large representative collection of ores and heavy-mineral concentrates. A database on mineralogy, metallogeny, rock and mineral compositions (including data in GIS-format, which are bound to the cartographical bases) for a number regions of the Far East (Chukotka, Kolyma, Priokhotie, Koryakiya, Kamchatka, Kuril Islands, Priamurie, Primorye as well as China and Korea) is being developed. The Electron and Light Microscopy Division A. Lotina and O. Kenya. Back row: L. Kolesova For example, in close co-operation with other laborato ries of FEGI, new and interesting data on palladium- and platinum-containing copper-rich gold have been obtained. The Electron and Light Microscopy Division A. Ivanova. Back row: N. Barinov and P. Safronov Au–Cu–Ag (Pt, Pd) diagram for solid solutions of Cu and Ag-rich gold from the Konder massif 1. Au–Cu, Au–Cu–Ag, and Au–Ag; 2. Au–Cu–Pt; 3. Au–Cu–Pd; 4. Au–Cu–Pt–Pd; 5. Au–Cu–Pt with Ag; 6. Au–Cu–Pd with Ag. Reference: Nekrasov I.Ya., Ivanov V.V., Lennikov A.M. et al., Rare natural polycomponent alloys based on gold and copper...// Geology of ore deposits. 2001. Vol. 43. No. 5 The Infrared Spectrometry Division G. Narnov and V. Kononov – 38 – The examination of the exsolution and supergene corrosion of natural alloys of Au-Cu-Ag-Pd-Pt under the microscope in reflected light The TEM images of ultra-fine structure of low-fineness gold (electrum), using the replicas from its surface Experimental modeling of the development of anomalous thread-like hight-fineness gold crystal during solid-phase decomposition of Au-Ag telluride Metallogeny investigations According to the modern plate tectonics concept, reconstructions of the Mesozoic-Cenozoic geodynamic setting of East Asia have been carried out. It has been found that during the Mesozoic-Cenozoic evolution of East Asia an alternation of subduction and transform (Californian type) settings occurred. The Okhotsk-Chukchi, East Sikhote-Alin, KoryakKamchatka, Central Kamchatka, and Kurils-Kamchatka volcano-plutonic belts developed in a subduction environment. Later, the geological environment changed from convergent to transform margin. The transform environ ment characteristics are strike-slip movement with intru sion of asthenosphere diapirs resulting from sinking of the earlier subducted lithosphere into the mantle. A spatial distribution of over 200 mineral deposits has been analyzed. A wide variety of different ore-bearing systems, including many different geological processes linked to the accumulation of gold, is considered (Khanchuk, Ivanov, 1998-2000, 2006). Like other geological features, gold deposits belong to complexly organized systems. Hence, one of the basic methods for investigating such complex systems is modeling, which is performed in several research directions (Ivanov, Khanchuk, 1999, 2004). In connection with genetic modeling of precious metal-bearing systems, oxygen, carbon, sulphur, and lead isotope composition in gangue and ore minerals from a great number of different-type mineral deposits of East Asia (Ishikhara, Ivanov et al., 1996; Ivanov, 1998; Rasska zov, Ivanov et al. 2002, 2007) have been studied. In addition to the earlier studies on radioisotope 40 Ar/39Ar datings for gold deposits from different type volcanic-plutonic belts of the Circum-North-West Pacific region, new age determinations for ore deposits from diverse geodynamic settings have been obtained. The database contains over 50 original analyses on over 25 gold-silver deposits. – 39 – Laboratory of Analytical Chemistry Research Staff: Galina M. Vovna, Dr., Head of Laboratory; Natalya V. Zarubina, Researcher, Deputy Head of Laboratory; Galina A. Bakhareva, Dr., Leading Researcher; Vladimir I. Kisilyov, Dr., Senior Researcher; Maxim G. Blokhin, Dr., Researcher; Evgeniy V. Elovsky, Postgraduate Student. Technical Staff: Larissa A. Avdevnina, Leading Technologist; Lyudmila I. Alekseeva, Leading Technologist; Viktoria N. Zalevskaya, Leading Technologist; Lidiya S. Levchuk, Leading Technologist; Galina I. Gorbach, Leading Technologist; Vera N. Kaminskaya, Leading Technologist; Al’bina I. Malykina, Leading Technologist; Elena A. Tkalina, Leading Technologist; Natalia V. Khurkalo, Leading Engineer; Viktoria V. Gileva, Engineer; Svetlana A. Muratova, Engineer; Larissa Y. Smirnova, Programming Specialist. Contacts: Tel: +7-4232-318750 E-mail: [email protected] The laboratory activity is directed towards solving analytical problems and providing geological and geochemical laboratory services for the Far East Geological Institute, as well as other subdivisions of FEB RAS, supplying quantitative data analyses for their investigations. The laboratory uses classical methods of chemistry and instrumental tools, including inductively coupled plasma and high-performance liquid chromatograph instruments. Zirconium geochronological dating through the ICP-MS with laser ablation and a quantitative analysis of REE in accessory minerals can be accomplished. Established in 1959, the Laboratory of Analytical Chemistry presently is equipped with unique up-to-date equipment applicable for detecting and analyzing rock and mineral elements. Numerous new techniques have been developed by the highly skilled lab stuff and are being successfully applied for defining the elementary composition of rocks, sea bed sediments, ferromanganesian deposits, soils, vegetable materials, natural water and other substances. Analytical equipment 1. Ion-chromatograph LC-10A (SHIMADZU, Japan). Being a single-column modification of devises for high-performance liquid chromatography. Chromatographic column of the apparatus is adapted for sharing and determining of cations Li+, NH4+, Na+, K+, Ca2+, and Mg2+ and anions F-, Cl-, NO2-, Br-, NO3-, and SO42-. 2. Plasmaquant 110 (Analytik Jena AG, Germany) and ICAP 6500 Duo (Thermo Electron Corporation, USA) inductively coupled plasma atomic emission spectrometers. Plasma spectrometry is one of the Galina M. Vovna – 40 – Plasmaquant 110 (Analytik Jena AG, Germany) ICAP 6500 Duo (Thermo Electron Corporation, USA) Agilent 7500a with UP-213 system (Agilent Technologies, USA) Agilent 7500c (Agilent Technologies, USA) universal and advanced methods of elemental analysis of a substance. With the help of the Plasmaquant 110, numereous element content in rocks, ferromanganesian materials, ores, natural and contaminated waters and biological materials can be determined simultaneously. The ICAP 6500 Duo spectrometer is used for elemental analysis of liquid samples. It works via Echelle optic scheme and has a semi conducting CID detector and plasma discharge dual observing (in radial and axial direction) system that enables most of elements at level 1-10 ppb to be defined. Proper software ITEVA provides computer monitoring of the spectrometer. chronological and isotopic and geochemical analysis the laboratory has Agilent 7500a equipped with UP-213 system for laser ablation mass spectrometry. 4. Thermo Orion 920Aplus (Thermo Orion, USA) and И-500 (Close Joint Stock Company “Alvilon”, Russia) ion meters are used to determine anion content of samples. 5. Mars 5 (CEM Corporation, USA) system is used to prepare samples of different composition: rocks, soils, and biological materials. Preparation of the samples to be analysed includes open decomposition in acids mix and alloying the samples with different fusions in a muffle furnace and a microwave decomposition system. 3. Agilent 7500c (Agilent Technologies, USA) inductively coupled plasma mass spectrometer is used for mass-spectral studies. The laboratory analyzes samples of different natural materials (rocks, sea bed sediments, water, and biological matter). For geo Ion-chromatograph LC-10A (SHIMADZU, Japan) Mars 5 (CEM Corporation, USA) – 41 – Laboratory of Stable Isotopes Research Staff: Tatyana A. Velivetskaya, Dr., Head of Laboratory Victoria V. Yakovenko, Junior Researcher Technical Staff: Vera M. Avchenko, Leading Engineer Elena S. Ermolenko, Leading Engineer Nina P. Konovalova, Leading Engineer Irina V. Borovik, Leading Engineer Sergei Yu. Budnitsky, Engineer Ekaterina Yu. Kovaleva, Engineer Sergei S. Gussev, Laboratory Technician Contacts: Tel: +7-4232-318548 E-mail: [email protected] identified in various natural formations, including the conditions of genesis. At present, this laboratory is one of few laboratories in Russia that possesses great opportunities in research of light stable isotopic relationships. The laboratory has preparative and mass spectrometry facilities for determining the stable isotope ratios, at natural abundance levels, of the important light elements: 2H/1H, 13C/12C, 15 N/14N, 18O/16O, and 34S/32S. These isotope studies are carried out for a wide range of natural materials, depending on the tasks to be solved in various areas of scientific researches, including geology, biology, ecology and medicine. The laboratory has a variety of methods for 13C/12C and 18O/16O analysis of carbonates. The high-precision analysis of microquantities of organogenic carbonates (e.g., 0.025-0.040 milligrams or 6-10 foraminiferas), which is very important for the interpretation of paleorecords, has been established at the laboratory and is considered a routine capability. In addition, an easy and economic method has been successfully applied to 13C/12C analysis of organic carbon in sediments and soils, which also can be applied to the analyses of dispersed forms of carbon in rock. The laboratory provides high accuracy 18O/ 16O analysis of silicates and oxides by fluoridation, to answer questions connected with determining formation temperatures of various minerals. The production of 2H/1H and 18O/16O analyses of water and hydrogenous minerals makes it possible to provide valuable information about the genesis of formational water and its mineralogical effects on country rocks. For studying the biological processes connected with nutrient transfer, the laboratory has the capability to analyze 13C/12C and 15N/14N total and component-wise structure of organic substance by using a mixture of adaptable “off-line” techniques, depending upon high vacuum gas preparation lines. There are also fully automated “on-line” techniques used in the laboratory. For measurement of stable isotope ratios, the laboratory is equipped with three mass spectrometers. For investigations of geochemical processes in the hydrosphere and atmosphere, the laboratory produces high-precision 2H/1H, 18O/16O and 13C/12C analyses of liquid (Н 2О) and gaseous (СО 2, СН 4) samples. High-precision 34S/32S analysis is used when studying sulphur deposits and when a source of sulphur is to be Thermo Finnigan МАТ 252 (Germany) mass spectrometer is used for the analysis of stable isotopes and is equipped with 8 collectors for measuring of isotopic ratios: H/D, 13C/12C, 15N/14N, 18O/16O (from СO2 and O2), and 34S/32S (from SO2) Tatyana A. Velivetskaya – 42 – Thermo Finnigan МАТ 253 (Germany) mass spectrometer. It is used for measuring of H/D, 13C/12C, 15N/14N, 18 O/16O (from СO2 and O2), and 34S/32S (from SO2 and SF6) stable isotopes ratios. H/D measuring can be conducted in helium stream. There are several peripheral sample preparation units working connectively with the mass spectrometer. They are: the high-temperature transformer TC Thermo Finnigan for measurement of hydrogen and oxygen in water samples; element analyzer EA Thermo Finnigan for measurement of carbon, sulphur and nitrogen in samples of firm organic substances; GC/C III gas chromatograph with burning micro-furnace for sample preparation of complex organic compounds for H/D, 13C/12C, 15N/14N, 18 O/16O definition in individual components Photo of high-vacuum facility with 6 ports for highvacuum systems of various modifications used in the preparation of samples for isotope analysis. “Off-line” mode is used for the reception of: SO2 from sulphides and sulphates; СO2 from samples of various organic substances, soils, sedimentary rocks, oils and volatile organic liquid compounds; water from hydrogenous minerals for the isotope analysis of hydrogen Photo of high-vacuum plant for СO2 extracting from carbonate microquantities (25-35 milligrams) using 105% phosphoric acid at 95 оС. The device is connected with a micro volume of the МАТ 252 dual inlet system Photo of high-vacuum plant for laser extraction of oxygen from silicates and oxides by fluoridation. Samples are heated up by the continuous wave laser Nd-YaG, CW 100w, wave length 1.06 micrometer Thermo Finnigan МАТ 253 mass spectrometer is used for measuring isotopic ratios: H/D, 13C/12C, 15N/14N, 18O/16O (from СO2), and also Ar. It is connected with a high-vacuum device for laser isolation of argon from samples, and with a shared system (gas chromatograph Agilent 6890N), so that the spectrometer can be used for development of methods enabling measurement of argon in a helium stream, useful for К/Ar geochronology – 43 – Laboratory of X-Ray Methods Research Staff: Alexander A. Karabtsov, Dr., Head of Laboratory Evgeny A. Nozdrachov, Dr., Researcher Tatyana A. Lotina, Junior Researcher Technical Staff: Natalya I. Ekimova, Leading Technologist Galina B. Molchanova, Leading Technologist Tamara B. Afanasyeva, Leading Technologist Lyudmila I. Azarova, Leading Technologist Victor P. Soroka, Leading Engineer Tamara K. Babova, Senior Lab Technician Valentina I. Sechenskaya, Senior Lab Technician Irina V. Zolotaryova, Technician Contacts: Tel: +7-4232-317132 E-mail: [email protected] The laboratory carries out electron probe X-ray microanalysis using a JEOL JXA-8100 electron microprobe with three wavelength dispersive spectrometers and the energy dispersive X-ray Spectrometer (INKA Co Ltd., Oxford, England). The current spectrometer crystal inventory consists of: LIF, PET, TAP, and LDE2. The X-ray Laboratory provides high quality analy tical work to support scientific activity of the scientists of FEGI. The laboratory supports several projects including: (1) Gemstones of the Far East (mineralogy and formation conditions); (2) Experimental modeling of physical and chemical conditions critical to the formation of precious metal and other deposits. In addition, the laboratory cooperates closely with scientists of the Chemical Institute, Pacific Ocean Institute, and other institutes and subdivisions of the Far East Branch of RAS. Radiographic analysis Radiographic analysis is one of the most efficient methods for researching the structure and composition of crystals. In many cases this method provides unique information about the phase composition and structural features of a given material. A special feature of X-ray analysis is its multi-purpose use in various kinds of material examination. Electron probe X-ray microanalysis Electron probe X-ray microanalysis (EPMA) is used for qualitative and quantitative analysis of elements within samples at concentrations from 0.01 to 100 wt %. A very small amount of material is used for an electron microprobe measurement with the required sample size for complete analysis ranging from 10-13-10-16 g. Elements from B to U can be analyzed. The laboratory carries out X-ray diffraction studies at the DRON-3 diffractometer (Russia) with monochromatic X-ray radiation. When dealing with a very small amount of material, the staff uses an IRIS-3 X-ray source (Russia) as well as Debye-Scherrer and Gandolfi powder cameras. Phase identification is performed with the use of the software program PDF2, a database which includes information on 75 000 compounds. Both minerals and synthetic compounds can be analyzed, as well as micro inclusions from an uncovered surface of 1-5 microns in diameter. The laboratory began using the multipurpose X-ray diffractometer D8 DISCOVER with GADDS (Bruker AXS GmbH, Germany) in 2007. The minimum analysis area is 50 microns. X-Ray Fluorescence Analysis S4 Pioneer sequential X-ray spectrometer (Bruker AXS GmbH, Germany) is available for the X-ray fluores cence analysis. The device has an X-ray tube, capacity 4 kW, with Rh-anode and a thin (75 micron) beryllium window. The spectrometer has the following configuration: five analyzing crystals (LiF200, LiF220, Ge, PET, and OVO-55); two collimators with divergence to be 0.23 and 0.46 ; and eight primary X-ray filters: Cu (1000, 300, and 200 microns) and Al (800, 500, 200, 100, and 12.5 microns). Alexander A. Karabtsov – 44 – JXA-8100 Electron Microprobe (JEOL Co. Ltd., Japan) PGS-II diffraction spectrograph (Germany) The laboratory performs quantitative determinations on the concentrations of petrogenetic elements Na, Mg, Al, Si, P, K, Ca, Ti, Mn, Fe and microelements S, Cl, V, Cr, Co, Ba, Rb, Sr, Y, Zr, Nb, As, Pb, Th, U, Ni, Cu, Zn, Ga in various rocks, minerals, ores and soils. For these purposes compressed tablets and fused disks are used. Emission spectral analysis Qualitative and semi-quantitative spectrographic analysis of rocks and minerals is performed by using the PGS-II (Germany) and DFS-8 (Russia) diffraction spectrographs which evaporate samples in the alternating current arc (30 mg in 5 min). Sensitivity of this method is in range of 10-2 to 10-4 %. The laboratory applies three techniques for the qualitative analysis of rocks and minerals: 1. Simultaneous analysis on twelve elements (B, Ni, Co, Cr, V, Mo, Zn, Ga, Sn, Cu, Pb, Ag) through the evaporation of 400 mg sample in an AC arc; 2. Analysis of impurity elements (Ni, Co, Cr, V, Zr, Sc, Mn, Bi, In, Sb, Be, Y, Yb, Nb, Pb, Cd, and others) through the evaporation of 10-100 mg probe put in a channel drilled inside the carbon electrode. Test sensitivity is in range of 10-2 to 10-5% with reasonable error between 6 and 30%; 3. Determination of As, Sb, Pb, Cu, Bi, Ni, Co, Pt, Mn, Zn, Fe, Pd, and Te content in native gold, 15 g weight sample. Sensitivity and error appearance depend on sample composition. DRON-3 diffractometer (Russia) S4 PIONEER sequential X-ray Spectrometer (Bruker AXS GmbH, Germany) D8 DISCOVER with GADDS (Bruker AXS GmbH, Germany) – 45 – Workshop for Preparation of Samples and the Production of Thin and Polished Sections Workshop Staff: Ivan I. Ivan’kov, Head of the Workshop Antonina P. Lyakhova, Grinder Natalia A. Kazanova, Grinder Olga V. Doronina, Grinder The Workshop for Preparation of Samples and the Preparation of Thin and Polished Sections is оnе of the oldest industrial subdivisions of the Far East Geological Institute. The first grinding machine, built in the mechanical workshops of the academic institute IGEM (Moscow), was confidentially delivered to Vladivostok in the 1950s to the Geological Department of the Far East Branch of the USSR Academy of Sciences as а hand luggage in а passenger carriage (passengers then were not allowed to transport more than 30 kg). Accutom-50 (Struers Co., Denmark) – universal machine for treatment of stone Today the Workshop is supplied with modern machines and equipment that make it possible to perform а whole cycle of crushing and grinding of rocks, to produce thin sections, double-side-polished transparent plates, polished sections, polished lumps, to cut stones of а given size, and to drill holes in samples for taking kern of 3 to 7 mm in diameter. SimpliMet 1000 (Struers Co., Denmark) – press for construction of synthetic grains The equipment supplied recently (machines for semi-automatic production of thin and polished sections) significantly increases the productivity and decreases production time and allows the laboratory to assist other organizations. The Workshop staff consists of four workers who have extensive experience in grinding and stonecutting works. RotoPol -35 (Struers Co., Denmark) – mаchine for producing of polished sections DiscoPlan-TS (Struers Co., Denmark) – mаchine for producing of transparent polished sections Ivan I. Ivan’kov – 46 – Geology Department Faculty: Galina M. Vovna, Dr., Dean of Department Igor V. Kemkin, Professor Vladimir S. Pushkar, Professor Liana G. Bondarenko, Senior Lecture Contacts: Tel: +7-4232-317554 E-mail: [email protected] the Gamov and Krabbe Peninsulas and on the scientific campus of the Far East Geological Institute. The second level students go to the unique educational campus of the Novosibirsk State University – the training ground “Shira”, near the Shira village in Khakassiya. In addition, with the assistance of the Far East Geological Institute, during the academic year students are taken on field excursions to look at key stratigraphic sections and interesting geological objects of Primorye. Owing to the fact that many special lectures at the department are given by the leading researchers of the Geological Institute, students acquire a good knowledge of general geology and have a basic foundation concerning geophysics and modern methods of electronic data processing. This training gives the student a quality university education which will allow them to work as specialists in all spheres of geology in a university environment or even as head of a private firm or joint venture company. In 2005, for first time in the history of the Far Eastern State University (FESU) a Geology Department was added to its academic program. The addition of the Geology Department was the joint initiative of Academician A.I. Khanchuk, Director, Far East Geological Institute and Academician V.A. Akulichev, Director, Pacific Oceano- logical Institute, the two largest scientific institutes of the Far East Branch of the Russian Academy of Sciences (FEB RAS). Chancellor of the FESU Prof. V.I. Kurilov has approved and the Presidium of the FEB RAS has confirmed this initiative. The department forms part of the Scientific Education Center “Physics of the Earth”, in the FESU Institute of Physics and Information Technology, under the leadership of Prof. Valery I. Belokon. First Dean of the department was A.I. Khanchuk, who was then succeeded by Galina M. Vovna. Staff of the department consists of highly skilled specialists: professors and doctors from the Geological Institute and leading researchers from other institutes of the FEB RAS. Since 2005, the department has given a course of lectures on geodynamic geology. Students will be qualified as experts in general and regional geology, geotectonics and geodynamics, geological surveying and structural geology, earth disasters prediction and mathematical modeling of geological processes. In future, the department plans to give lectures on groundwater, marine geology and geochemistry. The geological education process includes two-levels at the department. Students of the first (so called “basic”) level learn geology for four years and receive a higher education and B.S. degree in geology. Graduating students can choose then either to get a job or to continue their education at the department. The second level lasts for two years and ends by receiving a Master’s degree and fundamental knowledge for those who want to pursue science in the future. The department provides students a full-time tuition only. The graduate program is in Geology but there are several specializations: Regional Geology, Geological Surveying and Stratigraphy. After the graduating, the first level students have an opportunity to practice in geo logy within the Primorye region: on the coastal areas of – 47 – Laboratory of Avalanche and Mudflow Processes Research Research Staff: Nikolay A. Kazakov, Dr., Head of Laboratory Yury V. Gensiorovskiy, Researcher Mikhail V. Mikhalev, Junior Researcher Technical Staff: Valentina K. Stavniychuk, Leading Engineer Darja A. Bobrova, Engineer Svetlana V. Rybal’chenko, Engineer Ekaterina N. Kazakova, Laboratory Assistant Valentina A. Lobkina, Laboratory Assistant Contacts: Sakhalin Branch of Far East Geological Institute Far East Branch, Russian Academy of Sciences 25, Gorky Street, Yuzhno-Sakhalinsk, 693023, Russia Tel: +7-4242-751335; Fax: +7-4242-751336 E-mail: [email protected] Nikolay A. Kazakov The Laboratory of Avalanche and Mudflow Processes Research was formed in 2002. Since the laboratory’s inception it has been run by Dr. Nikolay A. Kazakov. dynamics in different landscapes complementing the methods of crystal-morphological analysis of snow thickness structure. Major research directions • The laboratory has developed quantitative descriptions of avalanche, debris-flow and mudflow as solitare waves – solitons. The laboratory researches evolution of nival, avalanche, and mudflow complexes in geoecological systems of the Russian Far East, as well characteristics of related processes and their influence on geoecological systems. • The laboratory has researched nival-glacier processes found in the mid- and low-mountain relief of the Russian Far East. Results • The laboratory has created physical and mathematical models of nival, avalanche, and mudflow processes; avalanche and mudflow wave dynamics; and avalanche and mudflow front as wave solitons. Specifically, the following topics have been analyzed: • Investigations has been carried out into the gene sis and dynamics patterns of snow cover, avalanches, mudflows, and other exogenous geodynamic processes found in the mid- and low-mountain relief of the Russian Far East. These studies have resulted in a method to quantitatively describe snow thickness texture as a deterministic fractal. This approach of describing snow thickness texture through fractal dimensionality permits mathematical modeling in order to elaborate methods of forecasting snow thickness characteristics of strength snow cover as an electrodynamic system; the fractal dimensionality of snow cover texture; • avalanche and mudflow complexes as trigger geosystems; • snow cover metamorphism as an energy-informational process; • the self organization of dissipative structures in forming and developing of nival, avalanche, and mudflow complexes. • • – 48 – • The laboratory has developed methods for mapping nival, avalanche, and mudflow processes and methods of building up mid-scale maps showing the intensity of nival, avalanche, and mudflow processes in unstudied regions for application in engineering research and construction projects. • The laboratory has determined the theoretical bases and methodological principles of avalanche and mudflow processes control, as well as long-term forecasting principles for determining the intensity or degree of avalanche and mudflow events. These permit setting up zones predicting intensity of expected avalanche and mudflow based solely on geological, geomorphological and landscape structure and climate data of the region. • The laboratory has developed theoretical bases and methods for calculating the dynamic characteristics of catastrophic avalanches and mudflows as they apply to engineering and construction. • The laboratory has studied anthropogenic transformations and their impact on nival, avalanche, and mudflow complexes and subsequent influence on the evolution of geoecological systems. • The laboratory has been able to describe the formation of hill mountains of Sakhalin Island as the result of extreme volumes of debris-flow activity (more than 300 000 m3). – 49 – Laboratory of Monitoring of Natural Processes and Geoinformation Technologies Research Staff: Vyacheslav A. Melkiy, Prof., Head of Laboratory Vladimir M. Pishchalnik, Prof., Leading Researcher Oleg V. Zenkin, Dr., Senior Researcher Aleksey A. Galtsev, Junior Researcher Elisaveta V. Nikonova, Postgraduate Student Technical Staff: Inna I. Lobishcheva, Leading Engineer Valeriy A. Sakharov, Leading Engineer Valeriy A. Romanyuk, Laboratory Researcher Contacts: Sakhalin Branch of Far East Geological Institute Far East Branch, Russian Academy of Sciences 25, Gorky Street, Yuzhno-Sakhalinsk, 693023, Russia Tel: +7-4242-265046 E-mail: [email protected] Vyacheslav A. Melkiy Major research directions • The laboratory developed techniques for computer processing of satellite data from Moderate Resolution Imaging Spectroradiometer (MODIS) to estimate anthropogenous pollution of the Sea of Okhotsk. The degree of pollution was measured by analyzing the biooptical properties of waters from different parts of the sea. The laboratory studies natural interactions occurring at the boundaries between the lithosphere, hydrosphere, atmosphere and biosphere in modern geoecological systems of transition continent-ocean zone. The laboratory develops methods of monitoring these natural processes, including remote sensing data from earth satellites, remote sounding, and geoinformation technologies. • On a northeast shelf of Sakhalin Island, the laboratory developed the technology and methodologies for modeling ice conditions in the Sea of Okhotsk. These techniques are designed to forecast ice conditions to enhance safety in an oil-and-gas complex. Results • The laboratory developed theoretical bases and principles to construct a uniform system of monitoring an environment and the technosphere of a region. • The laboratory developed a technology for monitoring volcanic, seismic and landscape hazards from space. • The laboratory was able to determine the rules of transformation of the geological environment in the modern geoecological systems of the Sea of Okhotsk shelf zone. – 50 – International Department Department Staff: Andrei V. Grebennikov, Dr., Head of Department Valentina A. Piskunova, Senior Interpreter Inessa G. Strelchenko, Leading Interpreter Valentina I. Nikiforova, Technician Contacts: Tel: +7-4232-317591 E-mail: [email protected] [email protected] The International Department co-ordinates the international activities of FEGI scientists, including: The International Department is an independent unit of the Institute. It operates under the immediate supervision of the Director. The International Department is instrumental in the intense development of Far East Geological Institute (FEGI) co-operation with foreign scientific organizations that results in an increasing number of international agreements signed by the Institute. Moreover, every year FEGI scientists expand their contacts with colleagues from other countries; foreign scientists now visit the Institute more often, and more of our experts travel abroad. • systematizing information concerning the international activities of FEGI; • organizing and conducting international meetings, conferences, and workshops; • coordinating the preparation of reports about the Institute's international activities; • consulting employees in compiling, registering and realizing international agreements; The department was founded by Lidia I. Kovbas who had worked in the Institute for twenty years. Thanks to her professional skills and personal charm, the Institute managed to gain international standing and has become a respected scientific organization in the Russian Far East. Following the untimely passing of L.I. Kovbas, V.P. Nechaev and S.V. Vysotsky consolidated the department’s position and significantly extended its field of interest. • searching for international projects of interest to FEGI researchers and identifying international sources of funding for scientific projects. The International Department also performs the following operations: • represents FEGI interests in certain Russian governmental bodies, including the Far Eastern Customs Headquarters, and the Regional Branch of Foreign Ministry; in addition to various international organizations; • provides assistance with the translation of various kinds of print material: government documents, patent descriptions, references, international correspondence, as well as materials from conferences, meetings, and workshops; • prepares annotations and summaries of foreign scientific publications; • prepares visa documents to make possible travel to Russia for invited foreign experts, and prepares documents to facilitate foreign travel by FEGI scientists. The staff of the International Department is always ready to step forward with help and assistance. Andrei V. Grebennikov – 51 – Economic Planning Office. Personnel Department Accounting Department. Chancery Office Maintenance and Supply Department Back row: Tatiana N. Samokish, Engineer of Personnel Department; Tatiana V. Fedorovskaya, Chief Economist; Ludmila V. Bystrushkina, Leading Engineer; Vladimir I. Bityukov, Master Mechanic; Tatiana I. Leontieva, Main Specialist to Labor Protection; Elena V. Solomakha, Deputy Chief Accountant; Tatiana N. Belikova, Leading Accountant; Svetlana N. Bondar, Leading Accountant; Tatiana N. Kamynina, Leading Accountant Front row: Ol’ga V. Kasatkina, Secretary-Referent; Tatiana I. Karchevskaya, Engineer of Chancery Office; Elena A. Konovalova, Leading Accountant; Maria A. Ushkova, Leading Engineer of Supply Department; Galina S. Sorokovykh, Chief of Security Service Office; Anna I. Striyuk, Chief of Personnel Department • The Economic Planning Office and Accounting Department oversees financial and economical activities of the Institute and controls the studied application of material, manpower, and financial resources of the Institute. • The Personnel Department is responsible for salary concerns, and personnel management. • The Chancery Office has a number of important duties, including: – timely handling of incoming and outgoing correspondence, and its delivery to the point of destination; – record keeping, as well as maintaining and filing correspondence with different organizations; – systematic control and facilitating documentation necessary to operations of the Institute. • The Maintenance and Supply Department ensures that the Institute’s infrastructure is kept in good condition and is responsible for the routine upkeep and repair of the Institute’s premises and equipment. The Maintenance and Supply Department supplies the Institute with all the necessary material resources. Specialists of these departments are involved with a wide circle of responsibilities as outlined below. Mikhail I. Kuts, Leading Engineer; Natalia V. Khmelnitskaya, Leading Engineer; Alexander S. Khapersky, Chief of Supply Department – 52 –