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Supplementary Material (ESI) for Journal of Materials Chemistry This journal is (c) The Royal Society of Chemistry 2010 Supplementary Information ▲ ▲ ▲ ▲ ▲ ▲ ▲ Intensity (a.u.) ▲ ● ▲ ▲ ● 150 min ▲ ▲ ▲ ▲ 120 min 90 min ● ● ● ▲ ▲ 11 20 30 40 60 min 50 60 70 80 2 Theta (degrees) Fig S1 XRD patterns of cobalt phosphide nanoparticles obtained from [Co(Se2PtBu2)2] precursor in TOP/HDA at 300 °C for different reaction times; orthorhombic Co2P (JCPDS-32-0306),▲ orthorhombic CoP (JCPDS-29-0497), ● unidentified phase