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Available online at www.pelagiaresearchlibrary.com Pelagia Research Library Advances in Applied Science Research, 2013, 4(2):19-24 ISSN: 0976-8610 CODEN (USA): AASRFC Effect of pore-fluid on attenuation of elastic waves in rock types from southwestern Nigeria Olorode D. O. and Olatinsu O. B. Department of Physics, Faculty of Science, University of Lagos, Lagos, Nigeria _____________________________________________________________________________________________ ABSTRACT Laboratory attenuation measurements using pulse transmission coupled with spectral amplitude wave-ratio technique were carried out on three sedimentary rocks namely: shale, sandstone and glauconite from Ewekoro in Southwestern Nigeria. Attenuation coefficient (k) was measured in the frequency range of 100 Hz to 2 kHz. The rock materials were then soaked in water and kerosene (light-oil) respectively, to observe the trends in their attenuation patterns. In the natural rock samples, attenuation increases steadily with frequency for sandstone and glauconite but decreases in shale. In water–saturated rock materials, shale shows no attenuation dispersion which may be due to the pin-points getting easily disrupted by pore-fluid saturation; sandstone shows a decrease from its natural level; which implies a strong dependence of attenuation on pore-fluid; glauconite manifests a step-wise decrease and later increases around 1 kHz. The rock samples were saturated with kerosene (light oil) and their characteristic curves changed. Shale completely dissolved making it impossible to observe its attenuation pattern; sandstone attenuates more than glauconite. These results show that pore-fluid in the different rock materials have great influence on the attenuation coefficient of the materials. Key words: Attenuation coefficient, pore-fluid, pulse transmission, sedimentary rocks, seismic waves. _____________________________________________________________________________________________ INTRODUCTION The fact that elastic waves propagating through the earth are attenuated is a common observation. As these elastic waves travel deeper they lose energy unlike in spherical spreading, where energy is spread across a wider area, and reflection and transmission of energy at boundaries, where redistribution takes place in the upward or downward directions. This energy loss depends on frequency, that is higher frequencies are absorbed more rapidly than lower frequencies. In addition, attenuation appears to vary with the lithology of the medium [1]. Elastic wave attenuation has great potential as a tool to yield a better understanding of the anelastic properties, and hence the physical state, of rocks in the earth. Because of this potential, an expanding body of laboratory work has concentrated on bringing to fruition the diagnostic capabilities of attenuation measurements [2-5]. Two important reasons could be advanced for the need to investigate and understand the attenuation properties of the earth. Firstly, as elastic waves propagate through the subsurface, their amplitudes are reduced. Secondly, attenuation characteristics, when determined, could reveal useful information on the type of rock as well the presence and degree of fluid saturation of rocks. There is an appreciable overlap in the attenuation values of different rocks, but it is evident that sedimentary rocks are generally more absorptive than other types of rock. Amplitude analysis of elastic waves in sedimentary rocks is a common practice in rock Physics. Changes in reservoir seismic properties can be connected with fluid type and changes within the rock [6]. Low-frequency wave propagation in partially saturated rocks is still not well understood because of the lack of precise and reliable experimental techniques [7]. Biot theory which is the most commonly used theory for studying wave propagation in saturated porous rocks is not without its limitation. This is because the theory estimates attenuation fairly for frequencies higher than seismic frequencies. To resolve the problem of limitation of very important to develop simple and inexpensive experimental approach to measure attenuation at low 19 Pelagia Research Library Olorode D. O. et al Adv. Appl. Sci. Res., 2013, 4(2):19-24 _____________________________________________________________________________ frequencies. Our studies analyse wave attenuation in limestone, shale and glauconite of Ewekoro Formation, southwestern Nigeria. The frequency range is from 100 Hz to 2 kHz. 2. Theory of Attenuation in Rocks A commonly used measure of attenuation is the attenuation coefficient α , which is the exponential decay constant of the amplitude of a plane wave propagating in a homogeneous medium. The amplitude of this plane wave may be given as Ar = Ao exp(−αr ) (1) where Ar is the amplitude at any distance r from the source, attenuation coefficient. Ao is the initial or reference amplitude and α is the Attenuation coefficient is expressed as α= πf (2) Qv where Q is the wave quality factor and is the other commonly used measure of attenuation, is the frequency. v is the velocity and f The quality factor Q is defined as Q= Q= (3) 2π ∆E E (4) For a single cycle Q= π δ (5) where δ is the logarithmic decrement and is defined as the natural logarithm of the ratio of the amplitude of two consecutive cycles, i.e. δ = ln δ = αλ = (6) αv (7) f Laboratory measurements of attenuation in rocks show that Q correlates with rock type and fluid type, hence the estimation of Q can be used as a diagnostic tool for rock type discrimination and the effect of fluid. Q values for most sedimentary rocks ranges from 20 to 200 [8]. The lower value of Q indicates higher attenuation while higher Q value means the opposite. The spectral ratio technique originally developed by [9] was used to estimate P and S wave attenuation. This procedure assumes that Q is constant over the experimental frequency range and thus it is frequency independent. Hence there is no consideration for dispersion in the spectral ratio model. However, laboratory experiments conducted on several natural rocks have revealed different dispersion and attenuation mechanisms in rocks as caused by intrinsic anelasticity, scattering, and diffraction which can cause changes in velocities and attenuation and as a result affect Q estimates. The accuracy of determining Q across the frequency spectrum is a function of the dispersion characteristics of the waves, which depends on the frequency and the nature of the rocks that disperse the waves. 20 Pelagia Research Library Olorode D. O. et al Adv. Appl. Sci. Res., 2013, 4(2):19-24 _____________________________________________________________________________ Incorporating the dependence on frequency into attenuation equation (1), leads to Ar = GRAo exp(−αr ) Ar = GRAo exp(− πfr Qv (8) ) (9) where G and R are the geometric spreading factor and the energy partitioning respectively at interface. MATERIALS AND METHODS Laboratory measurements were carried out on samples of sandstone, glauconite and shale collected from Ewekoro near Abeokuta, Ogun state, Nigeria. These were made available in a prepared form with dimensions 8cm × 5cm × 3.5cm, for use in the laboratory. The experimental set-up is as shown in Figure 1. The experiment was performed using pulse transmission technique in which the amplitude decay of elastic wave signals travelling through a rock sample is measured. Only one way transmission effects were measured. For the fluid saturation measurement, the samples were immersed in the fluid for 24 hours to ensure the uniformity of saturation. The pulse transmission technique is most suited for use in saturated samples, provided correction can be made for geometric factors such as beam (waves) spreading and reflection. We used the pulse transmission technique and measure attenuation of the sample by using equation (3). Figure 1: Experimental setup. The sine-audio signal generator generates the sinusoidal wave, which is passed into the rock sample via transducers in contact with opposite faces of the rock samples. The transducer alloy pair was used to conduct signals from signal generator to the rock sample and from the other face of the rock sample to the Y channel of the oscilloscope. Each plate has a connecting wire soldered to it for wave’s transmission. Proper care was taken to insulate the rock samples from any unwanted stray signals. The rocks samples were connected electrically by gently pressing with a G-camp on the transducers for proper connection to the rock samples. A double-beam oscilloscope was used to analyze the elastic waves. Its Y1 channel was used to observe the input signal directly from the signal generator while the output from the rock sample was fed into the Y2 channel of the oscilloscope. The amplitudes of the incident (Ai) and transmitted (At) waves were recorded and a measure of attenuation made using the expression in Equation (3). RESULTS AND DISCUSSION Figure 2 show the plot of attenuation for the dry rock samples. It is observed that attenuation increases steadily with frequency for sandstone. For glauconite, there is a slight drop in attenuation from 100-400 Hz and thereafter 21 Pelagia Research Library Olorode D. O. et al Adv. Appl. Sci. Res., 2013, 4(2):19-24 _____________________________________________________________________________ increases with frequency. Attenuation in the dry shale sample decreases to about 1 kHz and shoots up again to 1.5 kHz and decreases further to around 2 kHz. Glauconite_dry Shale_dry sandstone_dry -0.4 -0.6 -0.8 Attenuation -1.0 -1.2 -1.4 -1.6 -1.8 -2.0 -2.2 -2.4 -2.6 0 500 1000 1500 2000 Frequency Hz Figure 2: Plots of attenuation versus frequency for the dry rocks. There is clear deviation in the behavior of the rocks from the dry condition. Shale showed no attenuation dispersion which may be due to the fact that its pin-points get easily disrupted by pore-fluid saturation. Water-saturated sandstone shows an almost opposite response (decrease in attenuation) to that in the dry condition which means a strong dependence of attenuation dispersion on pore fluids. But for glauconite, the response of the saturated sample shows a stepwise decrease and later increases around 1 kHz. Glauconite_H2O Shale_H20 Sandstone_H20 0.0 -0.2 -0.4 -0.6 Attenuation -0.8 -1.0 -1.2 -1.4 -1.6 -1.8 -2.0 -2.2 -2.4 -2.6 -2.8 0 500 1000 1500 2000 Frequency Figure 3: Plots of attenuation versusfor frequency for water-saturated samples. Plots of attenuation versus frequency water-saturated rockrock samples. 22 Pelagia Research Library Olorode D. O. et al Adv. Appl. Sci. Res., 2013, 4(2):19-24 _____________________________________________________________________________ Figure 3 represent the response of sandstone and glauconite when saturated with light oil (kerosene). Attenuation in this condition is relatively more than in dry and water-saturated conditions. This is in agreement with previous works by several authors [10-16]. It is also observed that attenuation dispersion increases for both rock types across the frequency range of measurement. Hence there is a clear discrimination in the behavior of the two rocks is in water and oil-saturated conditions. Shale completely dissolved in kerosene and as a result it was not possible to study its attenuation dispersion when saturated with this light oil. Glauconite_oil Sandstone_oil -1.3 -1.4 -1.5 Attenuation -1.6 -1.7 -1.8 -1.9 -2.0 -2.1 -2.2 -2.3 -2.4 0 500 1000 1500 2000 Frequency Hz Figure 4: Attenuation versus Frequency of light oil-saturated sandstone and glauconite CONCLUSION The attenuation characteristics of sandstone, shale and glauconite of Ewekoro were investigated in this work. The three rock types behaved differently in different pore-fluid saturation. At high frequencies, attenuation is higher than at lower frequencies. In the natural rock samples, sandstone attenuates most followed by shale and the least was glauconite. This is in agreement with the results obtained by [17] and [18]. When the rock samples were watersaturated, shale attenuates most followed by glauconite and sandstone was the least attenuated. However, when in kerosene (light oil), sandstone attenuates most, followed by glauconite while shale dissolved completely. Pore-fluid in the rock matrices has a great influence on the attenuation pattern of the rock materials. REFERENCES [1] Chopra, S., Alexev, V, First break, 2004, 22, 31-42. [2] Dutta, N.C, Odé, Geophysics, 1979, 44, 1777-1788. [3] Mavko, G.M, Nur, A, Geophysics, 1979, 44(2), 161-178. [4] Toskӧz, M.N, Johnston, D.H, Timur, A, Geophysics, 1979, 44(4), 681-690. [5] Johnston, D.H, Toskӧz, M.N, Journal of Geophysical Research, 1980, 85, 925-936. [6] Adam, L, Batzle, M, Lewallen, K.T, van Wijk, K, Journal of Geophysical Research, 2009, 114, B06208. doi: 10.1029/2008JB005890. [7] Madonna, C, Tisato, N, Boutareaud, S, Mainprice, D, A new laboratory system for the measurement of low frequency seismic attenuation, SEG Denver 2010 Annual Meeting, 2675-2680. [8] Sheriff, R.G, Geldart, L.P; Exploration Seismology Cambridge University Press, 1995. 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