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Delta Pressure Sensors M. Chitteboyina, D. Butler and Z. Celik-Butler, Nanotechnology Research and Teaching Facility University of Texas at Arlington http://www.uta.edu/engineering/nano/ 1 Delta Pressure Sensor Model Delta Pressure Sensor Final Model Packaged piezo resistors ~ 25 nm Unsealed cavity ~ 7.5 µm Passivation layer ~ 600 nm packaging layer ~ 1.35 µm Z-scale exaggerated 5 times Delta pressure (differential pressure) sensor is a type of pressure sensor which is used to detect pressure changes Delta pressure measures the pressure between two different points Here the pressure sensor is not sealed 2 Delta Pressure Sensor Results STRAIN YY PLOT DISPLACEMENT PLOT MISES STRESS PLOT STRAIN XX PLOT 3 Delta Pressure Sensor Fabrication STEP 1 On a clean wafer spin-coat ~ 40 µm flexible polyimide as the substrate layer followed by 600 nm passivation layer Passivation layer ~ 600 nm Piezo resistors ~ 25 nm STEP 2 Spin polyimide and cure STEP 3 Deposit ~ 2 µm membrane layer STEP 4 Deposit ~ 25 nm thick Piezoresistors Silicon nitride membrane layer ~ 2 µm Sacrificial layer ~ 7.5µm Packaged piezo resistors ~ 25 nm Unsealed cavity ~ 7.5 µm NEXT STEPS Deposit ~ 500 nm thick aluminum as the metallization layer Deposit ~ 100 nm thick packaging layer to package the pressure sensors packaging layer ~ 0.1 µm Ash the sacrificial layer using oxygen plasma to suspend the membrane Etch the silicon wafer from the back side to get access to the bond pads and characterize the delta pressure sensors Passivation layer ~ 600 nm membrane layer ~ 2 µm Z-scale exaggerated 5 times 4 Delta Pressure Sensor Fabrication Steps Membrane Layer + Packaging Layer 1.35 µm Piezoresistors Metallization Layer Aluminum 0.5 µm Polyimide completely gone Polyimide completely gone 5 Delta Pressure Sensor Characterization 4 Vin 3 Vout 2 Vin 1 Vout Vin R2 R4 R1 Vout R3 R2 R3 R4 R1 The electrical circuit is complete with two active piezoresistors (R1 and R3) and two passive piezoresistors (R2 and R4) in a Wheatstone bridge configuration The current-voltage characteristics is plotted and the true resistances are found 6 Delta Pressure Sensor Characterization IV_P1 Voltage (V) -0.6 -0.4 IV_A1 1.0E-04 8.0E-05 y = 0.0001x + 1E-07 6.0E-05 4.0E-05 2.0E-05 0.0E+00 -0.2 0.2 0.4 -2.0E-05 0.0 -4.0E-05 -6.0E-05 -8.0E-05 Current (A) Voltage (V) 0.6 -0.6 -0.4 IV_P2 Voltage (V) -0.6 -0.4 8.0E-05 y = 0.0001x - 3E-07 6.0E-05 4.0E-05 2.0E-05 0.0E+00 -0.2 0.2 0.4 -2.0E-05 0.0 -4.0E-05 -6.0E-05 -8.0E-05 Current (A) 0.6 IV_A2 8.0E-05 y = 0.0001x - 6E-08 6.0E-05 4.0E-05 2.0E-05 0.0E+00 -0.2 0.2 0.4 -2.0E-05 0.0 -4.0E-05 -6.0E-05 -8.0E-05 Current (A) 1.5E-04 1.0E-04 y = 0.0002x - 4E-09 5.0E-05 0.6 Voltage (V) -0.6 -0.4 0.0E+00 -0.2 0.0 -5.0E-05 0.2 0.4 0.6 -1.0E-04 -1.5E-04 Current (A) P1 and P2 are passive piezoresistors whereas A1 and A2 are active piezoresistors RP1=9.386 KΩ RA1=9.987 KΩ RP2=9.824 KΩ RA2=6.625 KΩ 7 İsmail Erkin Gönenli Advisor: Zeynep Çelik-Butler Department of Electrical Engineering The University of Texas, Arlington • • Membrane serves to amplify the pressure, convert into mechanical strain and then transfer it to the piezoresistor. Piezoresistors convert strain into resistance change which is transferred into electrical signal by the Wheatstone bridge. Piezoresistors Wheatstone Bridge R1 Vin Membrane R4 Vout R2 R3 Passive R4 R3 Membrane R2 Active R1 • Linear coupling between mechanical stress and change in resistivity given by: ΔR R Πlσl Π t σ t where R/R is the change in resistance, l and t and l and t are longitudinal and transverse piezoresistive coefficients and applied stresses respectively. Transverse stress t Longitudinal stress Direction of Current Flow Direction of Stress l • S. Sze, “Semiconductor Sensors” , John Wiley & Sons, Inc., New York , 1994 Direction of stress and current flow are the same Device 1 Device 2 42.43 µm x 21.21 µm 90 µm x 90 µm 35.36 µm x 21.21 µm 4.5 m x-axis 4 m Device 3 16.5 m 4.5 m 4 m Device 4 6.8 m 2.6 m 90 µm x 90 µm 16.5 m y-axis 110 µm x 110 µm Device 5 90 µm x 90 µm 3.8 m 9 m 90 µm x 90 µm 4 m 2.5 m 42.43 µm x 21.21 µm 4 m 13.5 m 35.36 µm x 21.21 µm 16.5 m 4.5 m Device 6 Device 7 42.43 µm x 21.21 µm 90 µm x 90 µm 14.14 µm x 14.14 µm 4.5 m 3.8 m Device 9 80 µm x 80 µm 80 µm x 80 µm 2.5 m 4 m Device 10 80 µm x 80 µm 21.21 µm x 14.14 µm 4 m 9 m 2.5 m 2.5 m 21.21 µm x 14.14 µm 28.28 µm x 14.14 µm 4 m 13.5 m Device 8 2.6 m 11 m 4 m 16.5 m x-axis 6.8 m 9 m y-axis 110 µm x 110 µm • Simulations were performed using CoventorwareTM • Twenty one pressure sensors with different membrane and piezoresistor dimensions and shapes were simulated among which ten showing best properties were selected. • The normalized change in resistance is found to be 0.84-3.5% assuming a gauge factor of 50. • Differential output voltages between 4.18-17.20 mV were obtained for 1 V input with a sensitivity range of 0.08 mV/kPa-0.34 mV/kPa. 50 kPa load applied to the top of the membrane fixed fixed fixed fixed a- Calculation of the Average Strain Strain AVG StrainTOTAL AreaTOTAL [ XX YY ]dxdy dxdy x xx cos2 yy sin 2 xy sin cos Axis transformation has been applied εyy used for these parts εxx used for these parts Axis transformation b- Calculation of the Output Voltage and Percent Change in Resistance R R Strain AVG * 50 where 50 is the gauge factor for polysilicon Vout R R 2 RR Vin for half bridge wheatstone structure • Si/ Si3N4 passivation layer/ flexible substrate (50 µm)/ Si3N4/ sacrificial layer/ Si3N4 membrane layer (~1.9 µm). • Deep reactive ion etch to etch Si3N4 membrane and open trenches. • Trenches on flexible substrate were fabricated by lift-off Trenches • Al layer (~0.5 µm)/ a-Si layer (~0.5 µm). • Piezoresistor fabrication. Piezoresistors • • • Al metallization layer (~0.5 µm). Patterning metallization layer. Al bond pads (~0.5 µm). Bond pads Metallization • Oxygen plasma ashing to release the structure. • Non-linear I-V characteristics with resistances tens to hundreds of k were obtained Before wire bonding After wire bonding Probe to apply pressure to the center. R1 R2 R3 R4 • A maximum differential output voltage of 13.7 mV has been obtained for 1V bias at full membrane deflection. Vout Output voltage is measured here. -Vin + Input voltage is applied here. • Four devices (Device 1, Device 2, Device 3 and Device 6) giving the highest voltage output in response to pressure were selected for determination of the actual piezoresistive gauge factor. Device 1 Device 2 Device 3 Device 6 110 µm x 110 µm 90 µm x 90 µm 90 µm x 90 µm 110 µm x 110 µm Before removal of sacrificial layer A’ A’ A A Membrane (1.9 µm) Sacrificial layer (3.1 µm) Si substrate A’ A After removal of sacrificial layer 3.1 µm gap after removal of sacrificial layer which is used to support the structure during fabrication The height given as around 5 µm includes the membrane which is around 1.9 µm thick. The remainder is the distance taken at full membrane deflection. Device 1 110 µm x 110 µm Applied Pressure: 78 MPa Device 2 90 µm x 90 µm Applied Pressure: 120 MPa Device 3 90 µm x 90 µm Applied Pressure: 128 MPa Device 6 110 µm x 110 µm Applied Pressure: 73 MPa Device 1 Results in Response to 78 MPa : Average Strain: 7.05 10-4 Change in Resistance (%) : 3.52 Output Voltage: 17.30 mV for 1 V input Device 2 Results in Response to 120 MPa : Average Strain: 9.9 10-4 Change in Resistance (%) : 4.95 Output Voltage: 24.15 mV for 1 V input Device 3 Results in Response to 128 MPa : Average Strain: 9.46 10-4 Change in Resistance (%) : 4.73 Output Voltage: 23.10 mV for 1 V input Device 6 Results in Response to 73 MPa : Average Strain: 7.53 10-4 Change in Resistance (%) : 3.76 Output Voltage: 18.45 mV for 1 V input Sample Actual Gauge Factor Type of Device 1 6.36 Device 3 2 19.998 Device 1 3 18.533 Device 3 4 24.121 Device 6 5 22.878 Device 1 6 25.764 Device 1 7 13.615 Device 6 8 17.766 Device 3 9 6.079 Device 2 10 29.366 Device 3 11 14.903 Device 3 12 7.992 Device 6