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12th International Conference on Fracture Study of crack propagation by infrared thermography during very high cycle fatigue regime N. RANC*, D. WAGNER**, L. ILLOUL*, PC. PARIS***, C. BATHIAS** *Laboratoire PIMM, ENSAM-ParisTech, FRANCE **LEEE, University of Paris X, FRANCE ***LAMEFIP, ENSAM-ParisTech, Bordeaux FRANCE Introduction • Many elements of mechanical structures can be loaded beyond 107 cycles : ⇒ Very high cycle fatigue regime (VHCF) or gigacycle fatigue regime • Fracture mechanisms associated with the VHCF are different from those known in high cycle fatigue (HCF) : • Fatigue failure can occur at values of cycle exceed 107 cycles and for stress level below the conventional high cycle fatigue limit. • In high yield strength steels the fracture does not occur on the surface but rather internally in the materials : formation of a fish eye 2 Experimental study of the crack propagation in the VHCF regime • Experimental difficulties : – High frequency : In gigacycle fatigue test is carried out at ultrasonic frequency (20kHz) one cycle : 50µs – Test duration : 14 hours for 109 cycles – Internal crack initiation Ö Is it possible to use pyrometry to understand and to study the fatigue initiation in VHCF regime? • Advantage of pyrometry technique: – – – – Good spatial and time resolutions It allows to obtain field measurements on the surface of the specimen The dissipated power is higher than at low frequency It allows to detect the thermal effects associated with an internal crack propagation (the fish eye formation, i.e. crack propagation , inside the material in the gigacycle fatigue regime is related to a local increase of the temperature due to plasticity on the crack tip.) 3 Experimental device : ultrasonic fatigue test with measurement of temperature fields Experimental device : ultrasonic fatigue test • Ultrasonic fatigue machine • Geometry of the specimen R1=1.5mm R2=10mm L1=16mm L2=10mm 5 Experimental device : temperature field measurement • Temperature measurement by infrared pyrometry: – MCT detector – Wavelength range : 3.7µm – 4.9µm – Aperture time : 100µs-1500µs – Refresh time : 16ms – 40ms – Spatial resolution : 0.12mm/pixel Experimental device : test with R=0.01 6 Temperature evolution during an ultrasonic fatigue test • Case of a high-strength steel : (0.22% of C; 1.22% of Mn; 1% of Cr; 1% of Ni); UTS = 950MPa Exothermic Martensitic transformation Fracture 260 200 240 180 220 160 200 140 Temperature in °C Temperature variation in °C Case of another high-strength steel : (0.22% of C; Mn, Cr, Si: less than 1%); UTS ≈ 1700MPa • 120 100 80 100 MPa 200 MPa 275 MPa 300 MPa 325 MPa 60 40 20 180 160 140 315MPa 120 100 80 60 40 0 20 0.0 5.0x10 7 1.0x10 8 1.5x10 Cycle 8 2.0x10 8 2.5x10 8 3.0x10 8 0.0 2.0x10 6 4.0x10 6 6.0x10 6 8.0x10 6 1.0x10 7 1.2x10 Cycle Specimen is cooled by an air circulation 7in order to limit its heating 7 Temperature field just before the fracture • R=-1; ∆σ=335MPa; NF=8.37x107 cycles (gigacycle domain) Temperature in °C 340 (5) Temperature in °C 320 300 (1) (2) N = 8.35890x107 cycles N = 8.36500x107 cycles (4) 280 260 (3) 240 (1) (2) 220 8.358x10 7 8.361x10 7 8.364x10 7 8.367x10 7 8.370x10 7 Cycle (3) (4) (5) N = 8.36968x107 cycles N = 8.36996x107 cycles N = 8.37000x107 cycles8 Post mortem observation of the fracture surface • Optical microscopy Observation direction • Scanning electronic microscopy rc Inclusion in the center of the fatigue crack : 0.5mm Propagation of a fish eye fatigue crack ⇒Average radius of the inclusion: aint=7.6µm ⇒Eccentricity: e=rc/R1=0.81 9 Thermal model of the crack propagation The model of crack propagation 1 • Paris-Hertzberg-McClintock crack growth rate law : ⎛ ∆K eff da = b⎜⎜ dN ⎝E b ⎞ ⎟⎟ ⎠ 3 b norm of the Bürgers vector E Young modulus • On the threshold corner da =b dN and ∆K 0 =1 E b 11 The model of crack propagation 2 ∆K eff = ∆K = 2 π Circular crack a(t) By supposing a circular crack and neglecting crack closure: ∆σ πa Cross section of the specimen Geometry of the circular crack The crack growth rate law is thus written: ⎛a⎞ ⎛ ∆K ⎞ da ⎟⎟ = b⎜⎜ ⎟⎟ = b⎜⎜ dN ⎝ a0 ⎠ ⎝ ∆K 0 ⎠ 3 1.8 2 After integration between a0 (t=0) and a (time t): a (t ) = a0 ⎛ t ⎞ ⎜⎜1 − ⎟⎟ ⎝ tc ⎠ 2 with 2 a0 tc = bf 1.6 Crack radius [mm] 3 2.0 1.4 1.2 1.0 The crack reaches the specimen surface 0.8 0.6 tf=3.7s 0.4 0.2 0.0 0.0 0.5 1.0 1.5 2.0 Time [s] 2.5 3.0 3.5 4.0 Evolution of the crack radius12 (a0=8µm; e=0.8; tc=4.4s) Calculation of the dissipated energy during crack growth • The reverse plastic zone size in plane strain: K Kmax ∆K ry 1 ∆K 2 rR = = 4 6π (2σ y ) 2 t ry rR<0.13µm • Energy dissipated per unit length of crack: E = ηr 2 R σy K max 2πx Plastic zone (radius ry) ∆K 2πx Reverse plastic zone (radius rR) −σy rR σy − ∆K 2πx 13 Calculation of the dissipated energy during crack growth Evolution of the dissipated energy versus time: ∆K 4 2 E = ηrR = η 2 2 4 24 π σ y 36π σ 4 4 y =η 9000 8000 7000 a02 ∆σ 4 6000 ⎛ t⎞ 36π 4σ y4 ⎜⎜1 − ⎟⎟ ⎝ tc ⎠ 4 Evolution of the dissipated power versus time: P = Ef = P0 ⎛ t⎞ ⎜⎜1 − ⎟⎟ ⎝ tc ⎠ 4 with tc = P/P0 E =η a2 10000 5000 4000 3000 tf=3.7s 2000 1000 2 a0 bf P0 is a constant which is identified from experimental data 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 Time [s] Evolution of dissipated power 14 (a0=8µm; e=0.8; tc=4.4s) Modeling of the thermal problem • Thermal model assumptions: – The specimen is modeled by a cylinder with a radius of R1=1.5mm – For symmetry reasons, only one half of the specimen is consider – rR is very small (about 0.13µm) : the fatigue crack is modeled by a dissipated power along the crack tip (P is the dissipated power per unit length) 15 Heat transfer equation • Heat transfer equation: ρC ∂T P(t ) = δ (rc − a(t ))δ ( z ) + λ∆T ∂t 2 • Initial condition ℓ=5R1 T (t = 0) = T0 a(t) • Boundary condition (adiabatic conditions) ∂T ∂T ∂T ( z = 0) = 0 ( z = l ) = 0 (r = R1 ) = 0 ∂z ∂z ∂r A rc Maximum surface temperature 16 Numerical simulation of the temperature field 1 • The thermal problem is solve numerically with a finite element method: – Linear finite element – The integration scheme is implicit – The mesh is more refined in the zone close to the plan of crack propagation : 100 elements on the specimen radius • Parameters of the simulation: – Initial crack radius: a0=8µm – Eccentricity: e=0.8 – Characteristic time: tc=4.4s 17 Identification of the dissipated power P0 • Minimization of least squares method : 340 P0=2.9Wm-1 320 Temperature [°C] Minimization of least squares of the difference between the maximum temperature measured in experiments and the calculated temperature: Experiment Model 300 280 260 Crack initiation 240 220 8.358x10 7 8.361x10 7 8.364x10 7 8.367x10 7 8.370x10 Cycle number 18 7 Numerical simulation associated to the experimental configuration Temperature in °C 340 366 Temperature in °C 351 (7) 320 336 (6) 300 321 280 260 307 (5) Crack initiation 292 (4) 277 (3) (2) (1) 240 262 248 220 7 8.362x10 8.364x10 7 8.366x10 7 Cycle 8.368x10 7 8.370x10 7 (7) N = 73594 (2) (1) (3) (4) (5) (6) 69301 cycles; 67786 70530 71553 72342 73174 t = 3.68s; 3.46s; a = 0.270mm 3.39s; 3.53s; 3.58s; 3.62s; 3.66s; 0.164mm 0.142mm 0.188mm 0.210mm 0.233mm 0.256mm 19 Experimental determination of the crack initiation • Experimental crack initiation criterion: increase of 0.07◦C of the filtered temperature (a≈0.02mm) Crack propagation: between 7x104 and 9x104 cycles ⇒ very small part of the life of the specimen 240 Experimetal result Filtered curve 238 Temperature [°C] • 236 234 7x104 – 9x104 cycles Prediction of the crack initiation 232 230 8.358x10 7 8.361x10 7 8.364x10 7 8.367x10 7 8.370x10 Cycle number 20 7 Conclusion • Experimental approach : temperature measurement during ultrasonic fatigue test • Modeling of the thermal effect associated to the crack propagation : – Crack propagation – Dissipated power during crack growth – Modeling of the thermal problem and numerical solution • Results – Good correlation with the experiment – Good estimation of the crack propagation duration 21