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1 MATERIALS ENGINEERING LABORATORY Most Recent Research Devices FACULTY OF TECHNOLOGY/Department of Mechanical Engineering, Materials Engineering Laboratory/ Seppo Järvenpää 7.7.2017 2 TOPICS Micro Indentation Tester 2009 NEW Thermo Mechanical Simulator (GLEEBLE 3500) 2010 Glow Discharge Optical Emission Spectrometer (GDOES) 2011 Confocal Laser Scanning Microscope 2012 Modernisation of Servo Hydraulic Test Machine (MTS) 2012 7.7.2017 MICRO INDENTATION TESTER 7.7.2017 3 MICRO INDENTATION TESTER Standard resolution of X/Y tables: 0.25 µm per axis Repositioning accuracy of standard tables: 1 µm per axis Anti-vibration table 7.7.2017 4 MICRO INDENTATION TESTER Vickers indenter Berkovich indenter Spherical indenter 7.7.2017 5 MICRO INDENTATION TESTER Fig. Schematic of a typical depthinstrumented indentation curve. 7.7.2017 6 MICRO INDENTATION TESTER Real typical depth-instrumented indentation curve. 7.7.2017 7 MICRO INDENTATION TESTER 7.7.2017 8 MICRO INDENTATION TESTER Continuous Multicycles Modes (CMC) method. 7.7.2017 9 10 THERMO MECHANICAL SIMULATOR (GLEEBLE 3800) Maximum heating rate - ca. 10.000 °C/s up to melting temperature Cooling rates - up to ca. 100 °C/s - or forced cooling by gas flow or quenching Maximum loading capacity - 200 kN of static force in compression or 100 kN in tension Max. speed of the moving anvil - 2 m/s (strain rates between 0.001 ... 50 1/s) 7.7.2017 11 THERMO MECHANICAL SIMULATOR (GLEEBLE 3800) Applications such as: - simulation of continuous casting simulation of hot rolling or forging processes hot tension or compression (axisymmetric or plane strain) tests, stress-strain curves hot ductility testing softening kinetics by stress relaxation simulation of annealing treatments simulation of welding thermocycles determination of TTT and CCT diagrams, including the effect of deformation thermal fatigue and creep deformation 7.7.2017 12 THERMO MECHANICAL SIMULATOR (GLEEBLE 3800) Hot/Warm Deformation: Plane strain compression test. In single- or multiple hit compression tests, strain and strain rate are controlled separately yet synchronously using the optional Hydrawedge® (see arrow). 7.7.2017 GLOW DISCHARGE OPTICAL EMISSION SPECTROMETER (GDOES) Model GDA 750 PMT, CCD 7.7.2017 13 GLOW DISCHARGE OPTICAL EMISSION SPECTROMETER (GDOES) Atoms are sputtered from the sample surface by a plasma (ionised argon atoms). Sputtered atoms emit photons with characteristic wavelengths. The intensities of different wavelengths are measured. 7.7.2017 14 GLOW DISCHARGE OPTICAL EMISSION SPECTROMETER (GDOES) 15 7.7.2017 GLOW DISCHARGE OPTICAL EMISSION SPECTROMETER (GDOES) BULK ANALYSIS - fast, few minutes/analysis - minimal sample preparation - pre-burn clears the surface being measured - detection limit 1…10 ppm -some knowledge of the measured sample is needed DEPTH PROFILING - analysing of surface layers up to 200 μm (coatings, films etc.) - depth resolution of 1-5 nm - intesities vs. time 7.7.2017 16 GLOW DISCHARGE OPTICAL EMISSION SPECTROMETER (GDOES) 7.7.2017 17 GLOW DISCHARGE OPTICAL EMISSION SPECTROMETER (GDOES) Analysis trace on steel plate (anode diameter 2.5 mm) 7.7.2017 18 CONFOCAL LASER SCANNING MICROSCOPE 7.7.2017 19 CONFOCAL LASER SCANNING MICROSCOPE TIEDEKUNTA TIEDEKUNTA / osasto osasto osaston osasto / Etuniminen Sukuniminen-Sukuniminen 7.7.2017 20 CONFOCAL LASER SCANNING MICROSCOPE - (confocal) Laser Scanning Microscope, (c)LSM - Confocal Scanning Microscope, CSM (white light) - Dual Core 3D Profiler (white/blue LED, confocal & interferometry) - Color 3D Laser Scanning Microscope (Laser + white light) - 3D Measuring Laser Microscope (Laser + white LED) 7.7.2017 21 CONFOCAL LASER SCANNING MICROSCOPE 7.7.2017 22 CONFOCAL LASER SCANNING MICROSCOPE 7.7.2017 23 CONFOCAL LASER SCANNING MICROSCOPE 7.7.2017 24 CONFOCAL LASER SCANNING MICROSCOPE 7.7.2017 25 MODERNISATION OF SERVO HYDRAULIC TEST MACHINE (MTS) 7.7.2017 26 MODERNISATION OF SERVO HYDRAULIC TEST MACHINE (MTS) • • • • • • Facilities: -istalled 1991, modernisation 2012 -static and dynamic force capacity ± 250kN, maximum frequency 20Hz -load cells ±15 kN and ± 250 kN -piston stroke 150 mm -extensometers ±1 mm (dynamic) and ±4 mm (static) • Applications such as: • -tensile tests, fatigue tests, fracture toughness tests (CTOD) • • • • • Coming procurements 2014: -thermal camera -optical extensometer -new (better) grips for flat and round specimens (-bending facilities (possibly)) 7.7.2017 27 MODERNISATION OF SERVO HYDRAULIC TEST MACHINE (MTS) 7.7.2017 28 MODERNISATION OF SERVO HYDRAULIC TEST MACHINE (MTS) 7.7.2017 29 MODERNISATION OF SERVO HYDRAULIC TEST MACHINE (MTS) Risks of the Fatigue? 7.7.2017 30