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Fulltext: english,
Fulltext: english,

... measurements. Furthermore, the argon gas was also passed through each sample solution for 60 s before each measurement. In each new experiment, a new bare electrode surface was used. All pH measurements were made with a Model Metrohm 744 pH meter (Herisau, Switzerland. All measurements were carried ...
Supporting Information for Angew. Chem. Int. Ed. Z52444 © Wiley
Supporting Information for Angew. Chem. Int. Ed. Z52444 © Wiley

... using freshly distilled solvents. Although we have never experienced an accident, all reactions must be performed with appropriate caution in a fume hood due to the flammable nature of mixtures of oxygen and organic solvents. Spectroscopic grade chloroform (Aldrich) or chloroform stabilized by amyle ...
Liquid chromatography: a tool for the analysis of metal species
Liquid chromatography: a tool for the analysis of metal species

... of the separating resin. Ligands are also required to avoid precipitation when an acidic eluent is not suitable for the columns selected. A low-capacity silica-based cation-exchange column was used for the separation of transition metals (Co, Cu, Fe) and coupled with post-column chemiluminescence de ...
International Journal of
International Journal of

... compound that has benzene fused with oxazole ring containing one oxygen atom and one nitrogen atom. It is a clear to yellowish low melting solid, insoluble in water. Benzoxazole finds use in research as a starting material for the synthesis of larger, usually bioactive s ...
Chromatography
Chromatography

... will be attracted or stick more to it but non-polar components will move across the surface easily.  If the stationary phase is nonpolar then nonpolar components will be more attracted to it and the polar ...
Separation and Purification Methods
Separation and Purification Methods

... are required for analyzing any number of complex mixtures—from contaminants in well water to forensic DNA samples to pharmaceutical formulations. Second, it is often necessary to purify compounds for further use—for example, the isolation of morphine from poppy seeds or the purification of intermedi ...
Paper chromatography
Paper chromatography

...  Column chromatography (CC): stationary phase is packed in a glass ...
lab-6-chrmatography
lab-6-chrmatography

... attracted differently to the porous stationary phase depending on its polarity and the polarity of the stationary phase chosen.  Remember that “Like attracts Like”.  If the stationary phase is polar then polar components will be attracted or stick more to it but non-polar components will move acro ...
Data Analysis
Data Analysis

1

Monolithic HPLC column

A monolithic HPLC column, or monolithic column, is a column used in high-performance liquid chromatography (HPLC) which contains a porous material which forms channels inside the column. In most HPLC configurations, particulate packed columns are used; in these configurations, tiny beads of an inert substance, typically a modified silica, are used inside the column.
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