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Dr. Jacob T. Klug
1. Personal details
Ben-Gurion University of the Negev, The Institutes for Applied Research
P.O. Box 1025, Beer-Sheva 84110, Israel;
Phone: 972-8-6461975
Fax No: 972-8-6472969
[email protected]
2. Education
B.Sc. 1956 – 1960: Chemistry, Technion-Israel Institute of Technology, Haifa.
M.Sc. 1960 - 1961: Chemistry, The Hebrew University of Jerusalem.
Ph.D. 1962 - 1966: Organic Chemistry, The Hebrew University of Jerusalem.
Post-Doc. 1966 – 1968: Organic Chemistry, Princeton University, Princeton, N.J.
Research Associate 1973 - 1974: Electroorganic Chemistry, Florida State University,
Tallahassee, Florida, U.S.A.
Research Associate 1975 - 1977: Electroorganic Chemistry, University of Arizona,
Tucson, Arizona, U.S.A.
3. Scientific Publication.
3.3 Refereed articles in scientific journals ( selected ):
1. R. S. Glass, J.R. Ducheck, J.T. Klug and G.S. Wilson. Facilitation of dialkyl
sulfide oxidation by neighboring group. J. Am. Chem. Soc. 99, 7349 (1977).
2. R.M. Waters, D.J. Voaden, A. Shani and J.T. Klug. The preparation of
(E)-2-pentenal. Org. Prep. Proceed. Int. 10:1-44 (1978).
3. G.S. Wilson, D. Swanson, J.T. Klug, R. S. Glass, M.D. Ryan and W. K. Musker.
Electrochemical oxidation of some mesocyclic dithioethers and compounds. J.
Am. Chem. Soc. 101, 1040 (1979).
4. A. Shani and J.T. Klug. The sex pheromone of the Egyptian cotton leafworm
(Spodoptera littoralis): Its chemical transformations under field conditions. J.
Chem. Ecol. 6, 875 (1980).
5. A. Shani and J.T. Klug. Photooxidation of (Z,E)-9,11-tetradecadienyl acetate,
the main component of the sex pheromone of the female Egyptian cotton
leafworm (Spodoptera littoralis). Tetrahedron Letters 1563 (1980).
6. D. Fishman, J.T. Klug and A. Shani. a, fl-unsaturated aldehydes;
montmorillonite clay K-10, an effective catalyst for the preparation of
unsaturated aldehydes via condensation of acetals with vinyl ethers. Synthesis
137 (1981).
7. R. Ideses, J.T. Klug, A. Shani, S. Gothilf and E. Gurevitz. Sex pheromone of
european grapefine moth, Lobesia botrana Schiff. (Lepidoptera; Tortricidae):
Synthesis and the effect of isomeric purity on the biological activity. J.Chem.
Ecol. 8, 195 (1982).
8. R. Ideses, A. Shani and J.T. Klug. Sex pheromone of European Grapevine Moth
(Lobesia botrana). Its chemical transformation in sunlight and heat. J. Chem. Ecol. 8,
973 (1982).
9. J.T. Klug, J. Skorka and A. Shani. A short synthesis of (E,E)-10,12hexadecadienal: The main component of the female sex pheromone of the spiny
bollworm (Earias insulana). Chemistry and Industry, 372 (1982) .
10. R. Ideses, A. Shani and J.T. Klug. Cyclic peroxide: An isolable intermediate in
singlet oxygen oxidation of pheromones of the furan system. Chemistry and
Industry, 409 (1982).
11. J. Almog, A. Hirshfeld and J.T. Klug. Reagents for the chemical development
of latent fingerprints: Synthesis and properties of some ninhydrin analogues. J.
Forensic Sciences 27, 912 (1982).
12. J. Halperin, Y. Golan, C. Descoins, B. Frerot, A. Shani, J. Skorka and J.T. Klug.
Preliminary trials on the attraction of Thametopoea Wilkinsoni tams to the
synthesized sex pheromone of Th. Pityocampa Schiff. La-Ya'aran 31, 24 (1981).
(In Hebrew, English summary, p. 44).
13. A. Shani, J.T. Klug and J. Skorka. A stereoselective synthesis of
(Z)-13-hexadecen-11-yn-1-yl acetate, the major component of the sex
pheromone of the pine processionary moth (Thaumetopoea pityocampa). J.
Chem. Ecol. 9, 863 (1983).
14. E. Dunkelblum, M. Kehat, J.T. Klug and A. Shani. Trimerization of Earias insulana
sex pheromone, (E,E)-10,12-Hexadecadienal, A phenomenon affecting trapping
efficiency. J. Chem. Ecol. 10, 421 (1984).
15. I. Teich, A. Shani and J.T. Klug. The role of mass trapping of the Egyptian cotton
leafworm (Spodoptera littoralis Boised) in its integrated pest control. J. Environ. Sci.
Health A20, 943 (1985).
16. Schwartz, H.; Mazor, R.; Khodorkovsky, V.; Shapiro, L.; Klug, J.T.; Kovalev, E.;
Meshulam, G.; Berkovic, G.; Kotler, Z.; Efrima, S. “Langmuir and Langmuir-Blodgett
Films of NLO Active 2-(p-N-alkyl-N-methylamino)benzylidene-1,3-indanedione-/A
Curves, UV-Vis Spectra, and SHG Behavior”. J. Phys. Chem. B 2001, 105,
17. Sawant, P.; Kovalev, E.; Klug, J. T.; Efrima, S. Alkyl Xanthates: New Capping Agents
for Metal Colloids. Capping of Platinum Nanoparticles. Langmuir 2001, 17(10),
18. Zhou, Xiaojian; Kovalev, Efim; Klug, Jacob T.; Khodorkovsky, Vladimir. An
Alternative Route for Carboni-Lindsey Reaction: N,N Cycloaddition of an Alkene to
s-Tetrazine. Org. Lett. 2001, 3(11), 1725-1727.
19. Tzhayik O, Sawant P, Efrima S, Kovalev E, Klug J.T.,
“Xanthate Capping of Silver, Copper and Gold Colloids”,
Langmuir 2001, in press.
3.4 Unrefereed professional articles and publications
1. Y. Teich, S. Newmark, M. Jacobson, J.T. Klug, A. Shani and R.M. Waters Mass
trapping of males of Egyptian cotton leafworm (Spodoptera littoralis) and
large-scale synthesis of Prodlure. In: "Chemical Ecology; Odour
Communication in Animals," pp. 343 (ed. E.J. Ritter) Elsevier, 1979.
2. A. Shani, R. Ideses, J.T. Klug, J. Skorka and R. Eliyahu. Isomerization and
oxidation of the conjugated double bonds system in pheromones.
Mediateurs Chimiques Agissant sur la Comportement des Insectes. Ed. INRA
Publ., 1982 (Les Colloques de l'INRA,7) pp. 107.
3. Goldstein, M.J., Klug, J.T., Teuerstein, A., Scharia, R., Eliahu, R. and
Mhasalkar, M. Facile Neopentyl Halide Exchange of Tribromopivalamides. In:
"Bromine Compounds; Chemistry and Application." pp. 272 (ed. D. Price, B.
Iddon and B.J. Wakefield) Elsevier, 1988.
4. Peled, M., Klug, J.T., and Scharia, R., 3,3'-Disubstituted α-lactams. In:
J.- Desmurs R.; Gérard, B., eds. Advances in Organobromine Chemistry. I.
Amsterdam: Elsevier; 1991. (Industrial Chemistry Library, vol. 3.) p.285-289
3.5 Scientific reports and research (selected )
1. Klug, J.T.; Zeigerson, E. Use of ultrasonic energy for driving chemical reactions;
annual report April 1985-March 1986, Beer-Sheva, The Institutes for Applied
Research, Ben-Gurion University of the Negev, Aug.1986. (Report No.
BGUN-ARI-53-86). (In Hebrew).
2. Klug, J.T.; Kornberg, N.; Peled, M.; Scheinhert, Y. Polymerization of
pentabromobenzyl acrylate. Report 1989. Dead Sea Bromine Group R&D
Division, Beer-Sheva.
3. Klug, J.T. Polybrominated derivatives of 5,5-dimethylhydantoin as potential fire
retardant. Report 1991. Dead Sea Bromine Group R&D Division, Beer-Sheva.
4. Klug, J.T.; Kornberg, N. Aromatic bromination of alkyl and bromoalkyl benzene.
Report 1993. Dead Sea Bromine Group R&D Division, Beer-Sheva.
5. Gorker, L.; Forgacs, C.; Klug, J. Synthesis and applications of perbromates; annual
report May 1992-May 1993. Report No. BGUN-ARI-26-93; May 1993.
6. Waldman, S.; Klug, J.T. Preparation of metal-containing phthalocyanines from
4-bromophthalic anhydride; progress report February-June 1993. Report No.
BGUN-ARI-43-93; June 1993.
7. Klug, J.T.; Ioffe, E. Benzylic bromination reactions; Report No. BGUN-ARI-55-93;
Aug. 1993.
8. Klug, J.T.; Kovalev,E. Polybrominated organic peroxides; final report. Report No.
BGUN-ARI-41-95; June 1995.
5. Lectures and presentation at conferences
5.2 Presentation of papers at conferences
Oral presentation of paper
Sept.18-19,1986 Facile Neopentyl Halide Exchange of Tribromopivalamides.
First International Symposium on The Chemistry and
Application of Bromine Compounds, University of Salford,
M. Peled, J.T. Klug, R. Scharia and M. Mhasalkar.
International Symposium on Chemistry of Orghanobrominated
compounds and their uses. ORGABROM-89 Millhouse, Thann,
France. Abstract p. 68
Poster sessions
March 1999.
Klug J.T., Kovalev E. and Skorka J., Competitive opening of spironode in
cycloaddition of s-tetrazines with anhydrobases of benzazolium salts.
The 64th Meeting of the Israel Chemical Society, March 1999.
February 2000. X. Zhou, R. Mazor, V. Khodorkovsky, E. Kovalev, J.T. Klug
The First Incorporation of a s-Tetrazine Chromophore Bridge into
Potential NLO p-System
H. Schwartz, M. Tevel, R. Mazor, V. Khodorkovsky, J.T.Klug, E, Kovalev,
G. Berkovic, Z. Kotler, and S. Efrima
LB FIims of NLO Active 1,3-Indandione Derivatives